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71.
A new method is presented for preparing highly monodispersed silica particles using a two-stage semibatch/batch hydrolysis reaction of Si(OC2 H5 )4 . The slower rate of hydrolysis of the tetraethylorthosilicate (TEOS) that occurred during the semibatch process resulted in larger silica particles with a higher yield and narrower size distribution. This was in direct contrast to the batch process. In addition, the ability of four different mixed processes to produce silica particles with good packing density, narrower particle-size distribution, and higher yield were evaluated. These were batch/batch (B-B), batch/semibatch (B-S), semibatch/batch (S-B), and semibatch/semibatch (S-S) processes. The S-S system produced the largest particles with the highest yields. The size of the silica particles obtained by the S-B method decreased with increasing reaction time, while the particles obtained by the B-S process had the best particle-size distribution and packing density. In conclusion, a mixed batch/semibatch system was the best way to produce an extremely narrow particle-size distribution and a good packing density. 相似文献
72.
73.
New experimental results on pressure loss for the single and two‐phase gas‐liquid flow with non‐Newtonian liquids in helical coils are reported. For a constant value of the curvature ratio, the value of the helix angle of the coils is varied from 2.56° to 9.37°. For single phase flow, the effect of helix angle on pressure loss is found to be negligible in laminar flow regime but pressure loss increases with the increasing value of helix angle in turbulent flow conditions. On the other hand, for the two‐phase flow, the well‐known Lockhart‐Martinelli method correlates the present results for all values of helix angle (2.56‐9.37°) satisfactorily under turbulent/laminar and turbulent/turbulent conditions over the following ranges of variables as: 0.57 ≤ n′ ≤ 1; Re′ < 4000; Rel < 4000; Reg < 8000; 8 ≤ x ≤ 1000 and 0.2 ≤ De′ ≤ 1000. 相似文献
74.
丁文荣 《南水北调与水利科技(中英文)》2017,15(1):107-112
基于MODIS NDVI数据及标准气象站数据、退耕还林资料,辅以空间统计、叠置分析和趋势分析等方法,研究了金沙江下段植被NDVI时空变化特征及其影响因素,结果表明:从年内来看,金沙江下段植被NDVI变化呈单峰型,3月份为最低值0.55,而9月份为最高值0.75,年际上10年以来植被覆盖总体呈现出增长趋势,且这种增长存在显著的空间异质性;研究区植被覆盖较好,植被NDVI平均值为0.65,海拔3 850m以下植被覆盖随海拔上升而增加,超过3 850m后随海拔升高呈降低趋势;年内植被NDVI受降水量的影响较气温更为明显,对两者均有2个月的滞后期,而年际上植被NDVI则受气温变化的影响较降水量更为突出,且大规模的植被恢复工程对金沙江下段植被覆盖的增加有重要贡献。 相似文献
75.
The nano-CeO2/ZnO catalysts were prepared using a novel combination of homogeneous precipitation with micro-emulsion for oxidative coupling of methane with CO2 as an oxidant. The prepared catalysts were compared with those prepared using the conventional impregnation. The catalysts prepared in two ways were characterized with FTIR, TEM, XRD and CO2-TPD. The effects of the reaction temperature, the amount of ZnO doped in the catalysts and the average size were investigated. The experimental investigation demonstrated that methane conversion over the nano-CeO2/ZnO catalysts prepared by the combined technique was higher than that obtained over catalysts prepared by the conventional impregnation. A better low-temperature activity has also been achieved over the nanocatalysts. There was no clear trend between the average size of nano-CeO2/ZnO catalysts and their catalytic performance but methane conversion increased with increasing fractal dimension of nanocatalysts. 相似文献
76.
Ethylene–propylene–diene terpolymer (EPDM) was modified by bromination reaction. Blending the resulting brominated EPDM with natural rubber (STR5L) and blending the unmodified EPDM with STR5L at various compositions were carried out. The rheological properties of the blends were investigated using a capillary extrusion. Shear flow curves of the pure rubbers and their blends illustrated the pseudoplastic property as shear thinning behavior with a power law index n < 1. True shear viscosity of all blends showed the negative deviation in relation to their additive values. Rheological behavior and two Tg's found from the DSC thermograms at all blend compositions indicated blend incompatibility for both sets of blends. The incompatibility of the vulcanized blends was also found by measuring the spin–spin relaxation time T2 by pulsed NMR. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 89: 837–847, 2003 相似文献
77.
78.
Ping-Hua Xiang Xian-Lin Dong Chu-De Feng Yong-Ling Wang 《Journal of the American Ceramic Society》2003,86(9):1631-1634
NiO nanoparticle-coated lead zirconate titanate (PZT) powders are successfully fabricated by the heterogeneous precipitation method using PZT, Ni(NO3 )2 ·6H2 O, and NH4 HCO3 as the starting materials. The amorphous NiCO3 ·2Ni(OH)2 ·2H2 O are uniformly coated on the surface of PZT particles. XRD analysis and the selected-area diffraction (SAD) pattern indicate that the amorphous coating layer is crystallized to NiO after being calcined at 400°C for 2 h. TEM images show that the NiO particles of ∼8 nm are spherical and weakly agglomerated. The thickness of the nanocrystalline NiO coating layer on the surface of PZT particle is ∼30 nm. 相似文献
79.
超临界流体沉析制备微细颗粒的技术及其应用 总被引:11,自引:2,他引:11
快速膨胀超临界流体溶液(RESS)过程和以超临界流体为稀释膨胀剂(GAS)过程是制备微细颗粒的新技术。本文着重分析了用RESS和GAS过程制备微细颗粒的特点及影响因素,介绍了在高分子聚合物、无机盐、陶瓷材料、有机物、药物及含能材料方面的应用,提出超临界流体沉淀技术将成为制备特殊细颗粒材料、超薄膜及提纯热敏性、易氧化物质的有效手段。 相似文献
80.