Influence of isothermal aging onσprecipitation in super duplex stainless steel

The time-temperature-transformation (TTT) curve of the 00Cr25Ni7Mo4N duplex stainless steel was obtained with a Formastot-digital thermal dilatometer,and the influence of isothermal aging on σ precipitation was studied by metallographic observation,X-ray diffraction (XRD),and transmission electron microscopy (TEM).The results show that the decomposition of ferrite phase is accompanied by the formation of σ phase at 750-1000℃,especially in the range of 800-900℃.The longer the aging time,the higher the amount of σ precipitation.The area fraction of various phases remains at a certain value upon the completion of ferrite deformation.The temperature of 850℃ is the most sensitive transaction temperature,the incubation time for the formation of o precipitation is less than 1 min,and aging for 20 min leads to the complete transformation of ferrite.The o phase is formed preferentially at the α/α/γ junction,and then grows along the α/α boundary in the matrix.     

预张力悬索桥及其静力学性能分析

为从理论上获得预张力悬索桥的力学特性,利用大位移不完全广义势能变分原理,建立了预张力悬索桥的一般基础微分方程.在进一步引入假设条件下,导出了基于古典挠度理论的平衡微分方程.通过对微分方程的解析,讨论了预张力悬索桥的静力学特性及其与普通悬索桥的区别.结合算例悬索桥的数值分析表明,预张力悬索桥由于抗风索的存在,以及结构中建立的预张力,在提高结构刚度、减小加劲梁弯矩等方面具有一定的优越性.     

Preparation and sintering of nano Fe coated Si3N4 composite powders

Fe/Si₃N₄ composite powder was synthesized by the heterogeneous precipitation-thermal reduction process, and then pressed into flakes under a pressure of 10 MPa. Flakes were sintered by pressureless and hot-pressing at 1 600 °C under 0.1 MPa N₂. The chemical composition, phases and microstructure of composite powder and sintered flakes were investigated by energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results show that the structure of composite powders is Si₃N₄ coated by nano Fe. The crystal phases of sintered flakes by pressureless are Fe(Si) compound, SiC and Si₃N₄. The crystal phases of the sintered samples by hot-pressing are Fe, Fe(Si) compound and Si₃N₄. It is found that crystal phases flakes obtained by pressureless and hot-pressing are very different. Foundation item: Project(50804016) supported by the National Natural Science Foundation of China     

ENSO事件对松花江流域夏季降水的影响

对1951—2000年的ENSO事件对松花江流域夏季(6—8月)降水的影响进行了分析,结果显示:赤道中东太平洋海温异常与松花江流域夏季降水有很好的相关性,特别是ENSO事件出现后,El Nino事件影响年通常对应于松花江流域夏季降水偏多,La Nina事件影响年松花江流域夏季降水则较常年偏少,且二者通过了置信度α=0.05的显著性检验.这种相关性可用于进行松花江流域夏季降水的预测.     

基于关联与回溯的产品变异设计过程重用方法

为实现在复杂度和数量上急剧增长的产品过程模型和关联知识的重用,提出一种产品变异设计过程的重用方法.对设计系统的模块进行精细化和抽象化,建立具有规范化数据接口的产品结构变异设计的信息模型,用状态空间的带权有序检索树存储变异设计过程;将变异设计语义添加至可移植结构,当发生分割、合并和变换的变异设计行为时,对其抛弃、保持或复制等处理,实现变异设计语义随变异设计行为的继承与变迁;再通过检索变异设计语义不断获得待变异结构,将离散的设计过程关联;深度优先搜索获得把初始状态变换为目标状态的操作序列,执行可行解集,回溯变异设计过程并实现重用.以ACIS为几何造型内核开发自主原型系统,实现涡轮风扇发动机的压气机的转子叶片变异设计过程的重用.结果表明,该方法将设计重用对象由静态的孤立设计结果拓展到动态的连续设计过程,对于准确、快速地实现产品的结构变异设计具有重要意义.     

加权变分去噪模型的分裂Bregman算法

针对求解加权变分去噪模型时大量迭代导致计算速度缓慢的问题,为提高运算速度,在加权变分去噪模型中引入分裂Bregman算法.实验表明,与梯度下降法相比,该算法迭代次数少、处理过程快,极大地缩短了运算时间,并且保持了较好的去噪效果.     

Synthesis of Polycrystalline Yb:Gd_3Ga_5O_(12) Nanopowders by Homogeneous Precipitation Method

The Ytterbium doped gadolinium gallium garnet [Yb3+:Gd3Ga5O12, Yb:GGG] precursor powders were synthesized via homogeneous precipitation method using Yb2O3, Ga2O3, Gd2O3 and ammonium bicarbonate [NH4HCO3] as precipitator, and ammonium sulfate [(NH4)2SO4] as additive. The evolution of phase composition and micro-structure of the powders were characterized by TG- DTA, XRD, IR, and TEM. The results indicate that all precursor powders completely transform to Yb:GGG phase by calcining at 900 ℃ for 8 h, the resultant powders are well dispersed and have smaller particle size approximately 80 nm owing to the electrostatic effect.     

Adaptive variational models for image decomposition

Image decomposition refers to the splitting of an image into two or more components.In this paper,a clean image is separated into two parts:one is the cartoon component,consisting only of geometric structure,and the other is the oscillatory component,consisting of texture.Three parts for noisy image are considered:cartoon,texture,and noise.To better decompose an image,we propose two new variational models.In our models,two adaptive regularization terms are introduced.The two regularization terms are determined by an adaptive function which can discriminate the cartoon and texture of an image automatically.Experimental results illustrate the efectiveness of the proposed models for image decomposition.     

Fractional partial differential equation denoising models for texture image

In this paper,a set of fractional partial differential equations based on fractional total variation and fractional steepest descent approach are proposed to address the problem of traditional drawbacks of PM and ROF multi-scale denoising for texture image.By extending Green,Gauss,Stokes and Euler-Lagrange formulas to fractional field,we can find that the integer formulas are just their special case of fractional ones.In order to improve the denoising capability,we proposed 4 fractional partial differential equation based multiscale denoising models,and then discussed their stabilities and convergence rate.Theoretic deduction and experimental evaluation demonstrate the stability and astringency of fractional steepest descent approach,and fractional nonlinearly multi-scale denoising capability and best value of parameters are discussed also.The experiments results prove that the ability for preserving high-frequency edge and complex texture information of the proposed denoising models are obviously superior to traditional integral based algorithms,especially for texture detail rich images.     

Nanostructured CeO2 microspheres synthesized by a novel surfactant-free emulsion

Nanostructured CeO₂ microspheres with an average diameter of 11 μm were prepared by a novel surfactant-free emulsion for the first time. Scanning electron microscopy (SEM), X-ray diffraction (XRD) and Brunauer-Emmet-Teller (BET) measurements were used to characterize the products. The images of SEM showed that the CeO₂ microspheres consisted of petal-like nanostructures with petal thickness in a range of 60 nm to 100 nm. The BET measurements showed the specific surface area of the CeO₂ microspheres exceeded 43 m²/g. The XRD analysis indicated the nanostructured CeO₂ microspheres were of cubic lattice. A possible mechanism of an interfacial precipitation reaction with the droplets of solid-stabilized emulsion as templates was proposed.