用过滤工艺全面提高铸锭质量

探讨了过滤器孔径对6063铝合金铸锭组织和性能的影响规律。在此基础上指出,在过滤工艺恰当时,不仅可以减少铸锭中的夹杂物,而且可以有效地防止裂纹、羽毛晶等连续铸锭中的常见缺陷。     

高耸构筑物施工控制措施

通过具体工程实践,在吸收现有滑模工艺技术的基础上,对平台扭转、中心垂直度控制等关键工艺进行创新,为提高工程质量提供技术保证,达到了创省级优质工程的效果。     

Comparison of mass transfer efficiency in horizontal rotating packed beds and rotating biological contactors

In this study, the mass transfer efficiencies of a novel horizontal rotating packed (h‐RPB) bed and the conventional disc‐type rotating biological contactor (RBC) were studied at four speeds and seven submergences. Pall rings of two different sizes (25, 38 mm), superintalox saddles and a wiremesh spiral bundle were used as packings in the h‐RPB. Volumetric gas–liquid mass transfer coefficients were determined by unsteady state absorption of atmospheric oxygen in de‐aerated water. Power consumption per unit liquid volume has been found for all geometries tested. The oxygen transfer efficiency values for the h‐RPB were found to be 2–5 kg kWh^?1 and for the disc RBC were found to be 1–2 kg kWh^?1. The performance of the h‐RPB was also compared with other gas–liquid contactors such as surface aerators. The study proves that the h‐RPB is a energy efficient alternative to conventional contactors. Copyright © 2005 Society of Chemical Industry     

Final Drying of Whole Milk Powder in Vibrated-Fluidized Beds

Vibro-fluidized beds are widely used in drying sticky powders and agglomerated materials as milk powder. Using a vibro-fluidized laboratory scale dryer, this work is aiming at analyzing preliminarily the effect of its operational variables on the drying kinetics and characteristics of whole milk powder. The full-factorial design technique with three replications at the central point has been employed to generate data and correlations to quantify the effect of inlet air temperature, air flow rate, and vibration bed amplitude on the drying curves and the milk powder properties related to its faster reconstitution in water (as tapped density, Hausner cohesion ratio, agglomerate size distribution, and internal pore concentration). Results obtained are analyzed and discussed to identify the adequate operation condition for final drying whole milk powder in vibro-fluidized beds, assuring a high product quality.     

On-line mass spectrometry system for measurements at single-crystal electrodes in hanging meniscus configuration

We present the construction and some first applications of an On-line electrochemical mass spectrometry system for detecting volatile products formed during electrochemical reactions at a single-crystal electrode in hanging meniscus configuration. The system is based on a small inlet tip made of porous Teflon and a Peek holder, which is brought in close proximity (ca. 10–20 μm) to the electrode surface. The tip is connected to the mass spectrometer by glass and metal tubing. Because of the small amount of gas entering the mass spectrometer, no differential pumping is needed during the measurement. The tip construction and preparation introduced here leads to reproducible voltammetry with very good cleanliness characteristics. The presence of the tip has no significant influence on the blank voltammetry of a Pt(111) in sulfuric acid, and on voltammetric responses for CO adlayer oxidation, methanol oxidation, and hydroxylamine electrochemistry on Pt(111). The formation of gaseous products in these reactions can be followed accurately and is in good agreement with earlier results obtained by other mass spectrometric or spectroscopic techniques. The time response and tailing of the setup is on the order of seconds and mainly determined by the distance between the tip and the electrode.     

Influence of influent tributaries on water quality changes in Lake Mogan, Turkey

Lake Mogan, located in the steppes of central Anatolia, is a vital Turkish ecological system, in terms of its water resources, flora and fauna. The lake also is a unique recreational area for Ankara, the capital of Turkey. However, the lake is currently threatened by severe pollution, being under the risk of serious degradation because of (i) uncontrolled urbanization; (ii) point and non‐point source pollution; (iii) inefficient sewerage systems; (iv) sediment transportation and pollution via influent creeks to the lake; (v) uncontrolled soil erosion in its drainage basin; (vi) inappropriate flood control measures; and (vii) severe degradation of the natural wetlands within its drainage basin. This study evaluates the influence of its influent creeks on the water quality of Lake Mogan, mainly because the creeks are believed to be responsible for the major pollutant load reaching the lake, and because the extensive database documenting this situation has not previously been critically evaluated. Accordingly, this study reviews (i) change in the water quality of Lake Mogan between 1993 and 2002; (ii) the water quality classification of the major influent creeks feeding Lake Mogan; and (iii) the influence of the influent creeks on the water quality of the lake between 1993 and 2004.     

系统思考 全面优化 实现产品质量持续升级

炼钢厂在贯彻落实《做强莱钢技术支撑体系》过程中,系统思考,全面优化,多措并举,重点突破,通过工艺管理升级、工艺技术升级和装备水平升级的一揽子计划,实现了产品实物质量升级的目标。     

山东改造工程旧房质量检测

结合某成品仓库改作商业用房的工程实例,对该建筑进行了详细的检测与分析,并根据结果提出了针对性的加固方案,并对加固效果进行了探讨,为工程改造提供了依据,可供类似工程借鉴。     

世界汽车及其润滑油的发展与排放的相关性分析

介绍了美国，欧洲，日本，中国汽油机油与柴油机油的发展过程，现状，趋势及其与排放的相关性，指出：90年代美国环保要求与节能变得更加严格，美国内燃机油规格进展充分反映了这一变化；欧洲，日本进入21世纪总的方向也是如此；中国的轿车工业主要是世界知名汽车厂商合资生产，其内燃机油规格遵守世界汽车厂商的要求，基本上跟随欧洲规格。     

飞行时间二次离子质谱--强有力的表面、界面和薄膜分析手段

二次离子质谱（Secondary ion mass spectrometry，简称SIMS）是一种对表面灵敏的质谱技术，建立在表面各种类型带正、负电荷原子或分子发射的基础上。用飞行时间（Time of flight，简称TOF）仪器对这些二次离子进行质量分析，能确保并行质量登录、高质量范围、高流通率下的高分辨和精确质量测定这些优异性能。配合细聚焦扫描一次离子束，可在优于1nm的高深度分辨和优于50nm的横向分辨本领下，实现对表面优于单层ppm(百万分之一）量级的极高检测灵敏度。当今TOF－SIMS已发展为一种成熟且完善的表面分析技术。极高的灵敏度，再加上即使对大分子及不易挥发性分子都独具的敏感性，使它成为很多高技术领域不可缺少的分析手段，这些领域包括微电子学、化学和材料科学以至纳米技术和生命科学等。本文简述了TOF－SIMS的原理、仪器及其多方面的应用和展望。