Peracetic acid as a single endodontic irrigant: effects on microhardness,roughness and erosion of root canal dentin

The aim was to assess the effects of 1% peracetic acid (PAA) as a single endodontic irrigant on microhardness, roughness, and erosion of root canal dentin, compared with 2.5% sodium hypochlorite (NaOCl) and with 2.5% NaOCl combined with 17% EDTA. Forty human, single‐rooted tooth hemisections were submitted to Knoop microhardness test, before and after the following irrigation protocols: PAA = 1% PAA; NaOCl = 2.5% NaOCl; NaOCl‐EDTA‐NaOCl = 2.5% NaOCl +17% EDTA +2.5% NaOCl; and SS = saline. Another 40 roots were instrumented, irrigated with the same protocols, and sectioned longitudinally. The roughness analysis was performed on the mesial section using a confocal laser scanning microscope, whereas erosion was analyzed on each third of the distal section, using a scanning electron microscope. The data were analyzed using ANOVA and Tukey post‐tests, and Kruskal‐Wallis and Dunn post‐tests (α = .05). The PAA and NaOCl‐EDTA‐NaOCl groups showed no significant differences (p > .05); both promoted reduction in microhardness and increase in roughness, compared with the NaOCl and SS groups (p < .05). NaOCl‐EDTA‐NaOCl promoted higher erosion in the cervical and middle thirds than the other groups (p < .05); there was no difference among PAA, NaOCl, and SS (p > .05). There was also no difference among the groups regarding the apical third (p > .05). PAA used as a single endodontic irrigant caused reduction in root canal dentin microhardness and increase in roughness in a similar way to NaOCl‐EDTA‐NaOCl; however, PAA caused less erosion than NaOCl‐EDTA‐NaOCl.     

In vivo assessment of the corrosion of nickel–titanium orthodontic archwires by using scanning electron microscopy and atomic force microscopy

This study was undertaken to assess in vivo the corrosion in two commercial nickel–titanium (NiTi) orthodontic archwires removed from the oral cavity of patients using fluoride mouthwashes. Five volunteers took part in this study on the corrosion behavior of two brands of NiTi archwires (3M and AO (brand of archwire)) during use of two mouthwashes with neutral sodium fluoride 1.1%, one with acidulated fluoride 1.1%, and one with placebo and a control group. Each patient used one mouthwash in three different periods of time for 1 min a day for 30 days. The archwires were assessed with scanning electron microscopy and atomic force microscopy for qualitative and quantitative analysis. The values obtained with atomic force microscopy (AFM) were submitted to normality test, two‐way analysis of variance, and Tukey's test at a significance level of 5%. The AFM images showed a gradual qualitative increase in the roughness of both types of wire between the treatments: control < placebo < neutral fluoride < acidulated fluoride. The arithmetic average of the roughness and root mean square of the roughness were similar. As for 3M archwires, only the acidulated fluoride group differed statistically from the others. As for AO archwires, the control and placebo groups did not differ from each other, but differed from the other fluoride treatments. The group using neutral fluoride also differed significantly from the acidulated fluoride group. 3M archwires were not affected by daily oral challenges. AO archwires were not affected by daily oral challenges either; their association with fluoride, either neutral or acidulated, increased their roughness.     

磨削表面粗糙度对γ-TiAl合金抗弯强度的影响

为了研究表面加工质量对硬脆性高温合金抗弯性能的影响,对不同磨削表面粗糙度的全片层γ-TiAl(Ti-47.5Al-2.5V-1.0Cr)合金进行了抗弯性能试验,分析了表面粗糙度对其抗弯强度的影响规律。试验结果表明,随着表面粗糙度的增大,全片层γ-TiAl合金的抗弯强度明显降低。结合断裂形貌图分析了全片层γ-TiAl合金组织中裂纹的萌生、扩展及最终发生宏观断裂的方式,全片层γ-TiAl合金裂纹大多起裂于因加工纹理引起的应力集中区域附近的片层间,并优先在层间扩展,最终的断裂形式多为穿层的脆性瞬断。     

滚齿工艺对齿根粗糙度的影响

针对国内外风电和工业齿轮箱轻量化的设计趋势,较低的安全系数对齿轮齿根弯曲强度提出了更为严格的要求。研究表明,在材料技术和齿形设计难以再优化的情况下,滚齿加工的粗糙度,尤其是齿根部位的粗糙度对齿轮弯曲强度的影响尤为敏感。针对滚齿工艺过程,从滚齿加工参数、刀具前刀面粗糙度和刀具刃口圆角三方面进行分析,验证其对齿根粗糙度的影响。     

Al-Cu合金片对钢/铝异种金属激光-MIG复合焊接头组织和性能的影响

采用PLC系统控制的激光-MIG复合焊接工艺对Q890钢/6063铝合金进行异种金属焊接,研究了钢侧坡口表面添加Al-Cu合金片对接头显微组织、硬度和拉伸性能的影响。结果表明:激光-MIG复合焊接接头具有典型的熔钎焊特征;未添加Al-Cu合金片的接头界面层由舌状相Fe2Al5和粗大针状相Fe4Al13组成,厚度约18μm,添加Al-Cu合金片后由舌状相(Fe,Cu)2Al5和细小絮状相(Fe,Cu)4Al13组成,厚度约为9μm,焊缝区与热影响区的组织与未添加Al-Cu合金片时的相似;添加Al-Cu合金片的接头界面层硬度比未添加Al-Cu合金片的低约59HV;添加Al-Cu合金片的焊接接头的抗拉强度比未添加Al-Cu合金片的提高了109.8%,未添加和添加Al-Cu合金片的焊接接头均在界面层断裂。     

大口径超光滑表面粗糙度非接触检测系统

介绍了一种应用激光双焦干涉原理测量大口径超光滑表面粗糙度的检测系统。该系统采用共路干涉和电子共模抑制技术,减小了测试环境的影响,消除了激光光强波动引起的系统误差。同时,采用紧凑的光学干涉头移动的扫描方式,因此能够测量大口径光学元件。系统的横向分辨力为0.5μm,纵向分辨力为0.1nm,系统的重复性优于2%。     

表面粗糙度理论发展研究

简述了表面粗糙度理论与标准的历史 ,分析了精密加工表面性能评价对表面粗糙度理论及参数的新要求 ,对表面形貌评定的分形法、Motif法、特定功能参数集法进行了论述 ,指出了表面粗糙度理论的发展趋势     

SiC颗粒增强铝基复合材料高速铣削工艺研究

从颗粒增强金属基复合材料的应用和切削加工现状出发 ,针对SiC颗粒增强铝基复合材料的高速切削加工性能进行了试验分析。通过铣削试验 ,研究了铣削速度对铣削力、加工表面粗糙度、表面形貌以及刀具磨损的影响 ,分析了该材料的高速切削机理 ,并获得了能够保证对其进行高效高精度加工的合理工艺参数。     

微细切削的尺度效应研究

重点阐述了微切削中尺度效应对切削力和加工表面粗糙度的影响 ,通过切削试验测定了在微切削过程中切削用量对切削力和表面粗糙度的作用规律 ,并绘制了相应的曲线。在对数据分析的基础上 ,初步验证了微切削中的尺度效应理论。     

异种钢熔合区马氏体相变过程及组织

高温金相显微镜观察发现,珠光体钢（ＺＧ２０ｓＩＭｎ）与奥氏体焊材料（Ａ３０７、Ａ４５７）事区确实民氏体相,且在４００℃至室温均有相变产生。经透射电镜观察,熔合区本为低低碳梅氏体,亚条马氏体,亚结构主要是位错,有少量昌亚结构。熔龠我碳化物主要生于焊后热处理过程中,其类型主为要Ｍ２３Ｃ６,也有部分Ｍ７Ｃ３。碳化物主要在马氏体上以及马氏体或铁素体和奥氏体界面析出。马氏体带、碳化物带宽度主要受Ｎdisplay st