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51.
以醋酸铜为模板,甲醇、氯仿为溶剂,2-乙烯吡啶、丙烯酰胺为功能单体,乙二醇二甲基丙烯酸酯为交联剂,采用本体聚合法制备铜离子印迹聚合物;然后掺入到壳聚糖海绵的制备中,使壳聚糖海绵对铜离子的吸附率由27.1%提高到72.3%。制备的铜离子印迹改性壳聚糖海绵需要2d达到吸附平衡,吸附-解吸5次后,性能稳定。 相似文献
52.
Metallographic sample prepared by ion beam etching 总被引:1,自引:0,他引:1
Ion beam etching technique was used to reveal the metallograhpic microstructure and interface morphology of electroplating chromium coating, in particular, whose substrate surface layer was treated in advance by laser quenching. Chemical etchings were also conducted for comparison. The reveal microstructures were observed and analyzed by scanning electron microscopy. The results show that ion beam etching can reveal well the whole microstructures of composite coating-substrate materials. 相似文献
53.
The multi-arc ion plating technology was employed to prepare the molybdenum films with thickness of 3 μm on the AISI 1045 steel. The wear and scuffing tests were carried out on the ball-on-disc tester. AFM and SEM equipped with EDS were adopted to observe and analyze the morphologies and element compositions of surface,cross-section and worn scar of the Mo film. The phase structure was studied by XRD and the bonding strength between Mo film and substrate was measured by scratching tester. The tribological experiments show that the Mo film possesses a good wear-resistance and an excellent anti-scuffing property. The failure mechanism of Mo film under extreme condition is flaking off. 相似文献
54.
针对图像中的椒盐噪声,基于模糊理论设计了一种滤波算法。首先结合椒盐噪声特点,借助窗口进行噪声检测,其次设计了自适应的方法消除噪声,最后采用图像进行实验,定性和定量分析结果表明该方法对于椒盐噪声的消除可行有效。 相似文献
55.
三元硝酸熔盐是一种重要的传热蓄热介质,粘度物性数据对其在工业中应用非常重要.但是由于硝酸熔盐熔点高,腐蚀性强,测试条件苛刻,粘度测量结果偏差较大,故利用计算方法确定熔盐粘度.本文首先通过大量实验数据拟合了纯物质KNO3,NaNO3和NaNO2的粘度,再利用Arrhenius混合规则确定的经验公式计算三元硝酸熔盐的粘度.与前人实际测量值进行比较.结果发现:利用简单经验公式估算的结果与实际测量值比较接近,表明这种熔盐热物性变化受外界影响较小,可以利用Arrhenius简单混合规则确定熔盐粘度. 相似文献
56.
57.
Jinlong Du Zaoming Wu Yanxiang Liang Xingjun Wang Peipei Wang 《Science and Technology of Advanced Materials》2018,19(1):212-220
The mechanism of radiation-induced detwinning is different from that of deformation detwinning as the former is dominated by supersaturated radiation-induced defects while the latter is usually triggered by global stress. In situ Kr ion irradiation was performed to study the detwinning mechanism of nanotwinned Cu films with various twin thicknesses. Two types of incoherent twin boundaries (ITBs), so-called fixed ITBs and free ITBs, are characterized based on their structural features, and the difference in their migration behavior is investigated. It is observed that detwinning during radiation is attributed to the frequent migration of free ITBs, while the migration of fixed ITBs is absent. Statistics shows that the migration distance of free ITBs is thickness and dose dependent. Potential migration mechanisms are discussed. 相似文献
58.
59.
针对冻结施工法装机容量大、电能消耗高以及施工过程的阶段性特点,在分析了冻结系统螺杆盐水机组不同工况下的机械特性和在各个冻结阶段电能消耗情况下,设计了一种基于PLC的变频节能系统。该系统以PLC为控制核心,通过压力传感器、液位计等对系统工况信息进行反馈,利用PID算法控制变频器的输出频率,从而达到了调节盐水泵流量、控制供冷量的目的。实验数据论证了该系统在井筒施工中应用的可行性与高效性。 相似文献
60.
Ajit Kumar MahapatraAuthor Vitae Giridhari HazraAuthor VitaeNirmal Kumar DasAuthor Vitae Shyamaprosad GoswamiAuthor Vitae 《Sensors and actuators. B, Chemical》2011,156(1):456-462
A new triphenylamine-based fluorogenic probe bearing an indolylmethane unit (R1) was developed as a fluorescent chemosensor with high selectivity toward Cu2+ over other cations tested. The new probe R1 only sensed Cu2+ among heavy and transition metal (HTM) ions in CH3CN/H2O (70/30, v/v) solution. The capture of Cu2+ by the receptor resulted in deprotonation of the secondary amine conjugated to the triphenylamine, so that the electron-donation ability of the “N” atom would be greatly enhanced; thus sensor showed a 250 nm change in the new absorption band (from 291 nm to 541 nm) and a large colorimetric response, it also exhibited the large decrease in fluorescence intensity at 378 nm and affinity to Cu2+ over other cations such as Hg2+, Fe3+, Pb2+, Zn2+, Cd2+, Ni2+, Co2+ and Mn2+ make this compound a useful chemosensor for Cu2+ detection in CH3CN/H2O (70/30, v/v) mixture. The probe R1 (c = 1.0 × 10−6 M) displayed significant fluorescence change and colorimetric change upon addition of Cu2+ among the metal ions examined. 相似文献