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991.
992.
Single‐walled carbon nanotubes (SWCNTs) dispersed in N‐methylpyrrolidone (NMP) were functionalized by addition of polystyryl radicals from 2,2,6,6‐tetramethyl‐1‐piperidinyloxy‐ended polystyrene (SWCNT‐g‐PS). The amount of polystyrene grafted to the nanotubes was in the range 20‐25 wt% irrespective of polystyrene number‐average molecular weight ranging from 2270 to 49 500 g mol?1. In Raman spectra the ratios of D‐band to G‐band intensity were similar for all of the polystyrene‐grafted samples and for the starting SWCNTs. Numerous near‐infrared electronic transitions of the SWCNTs were retained after polymer grafting. Transmission electron microscopy images showed bundles of SWCNT‐g‐PS of various diameters with some of the polystyrene clumped on the bundle surfaces. Composites of SWCNT‐g‐PS in a commercial‐grade polystyrene were prepared by precipitation of mixtures of the components from NMP into water, i.e. the coagulation method of preparation. Electrical conductivities of the composites were about 10?15 S cm?1 and showed no percolation threshold with increasing SWCNT content. The glass transition temperature (Tg) of the composites increased at low filler loadings and remained constant with further nanotube addition irrespective of the length and number of grafted polystyrene chains. The change of heat capacity (ΔCp) at Tg decreased with increasing amount of SWCNT‐g‐PS of 2850 g mol?1, but ΔCp changed very little with the amount of SWCNT‐g‐PS of higher molecular weight. The expected monotonic decrease in ΔCp coupled with the plateau behavior of Tg suggests there is a limit to the amount that Tg of the matrix polymer can increase with increasing amount of nanotube filler. Copyright © 2012 Society of Chemical Industry 相似文献
993.
本文介绍了一起电动单梁起重机运行脱轨坠落的事故案例,分析了造成事故的直接原因和间接原因,汇总了起重机运行啃轨故障的常见致因,提出了预防起重机坠落事故的管理手段和技术措施,对预防和减少同类事故具有鼍示意义。 相似文献
994.
995.
996.
《Ceramics International》2022,48(21):31811-31817
As one of the outstanding piezoelectric materials, relaxor-PbTiO3 single crystal also exhibits promising electro-optic and nonlinear-optic properties. Therefore, it is vital to understand the domain switching kinetics not only for optimizing strain-mediated devices performance but also for fabricating optical waveguides and periodic domain structures in optical applications. In this work, domain switching kinetics in annealed and pre-poled PMN-0.38PT single crystal under different external electric field were studied. Polarization reversal can be accomplished only by c-domain nucleation and growth in the annealed sample where the formation of the ferroelastic domains is hindered. In pre-poled sample, 90° domain switching happened by 90° domain wall reorientation under low electric field while 180° domain switching is accomplished by two-step 90° domain switching and c-domain growth under high electric field. The results are important for modulating domain structure for strain mediated and optical devices. 相似文献
997.
A laser-induced NO fluorescence technique was applied to measure velocity in a hypersonic shock tunnel nozzle exit. For the application of the technique, a detailed study of the density and fluorescence lifetime of the tracer radical, flow velocity and effective test time is proposed, resulting in a methodology for the application of the technique in hypersonic pulsed facilities. The study has demonstrated that it is necessary to jointly evaluate the flow velocity, the fluorescence lifetime of the radical and the width at half height of the laser beam, resulting in a kind of indicator for the feasibility of the technique. The variation of the laser incidence time with respect to the Pitot signal showed that it is not enough to select a stable Pitot pressure signal region to define the laser incidence time, preliminary trial and error analysis are necessary for each device used. Furthermore, the analysis of the velocity values calculated from the linear fit method shows that the adoption of such a method eliminates the effect of the systematic error of the measurements. 相似文献
998.
To boost the performance of the iron‐chromium redox flow battery (ICRFB), opting an appropriate proton exchange membrane (PEM) as the core component of ICRFB is of great importance. For the purpose, in this paper, various widely adopted commercial Nafion membranes with a different thickness of 50 μm (Nafion 212, N212), 126 μm (N115), and 178 μm (N117) are chosen for the sake of evaluating the influence of membrane thickness on the ICRFB single‐cell performance. Physicochemical properties, electrolyte utilization, cell efficiency, long‐term cycling stability, and the self‐discharge process of ICRFBs based on a series of Nafion membranes are contrasted comprehensively. The cycling test of ICRFBs is carried out under the current density range of 40 to 120 mA/cm2 for the charge‐discharge process. As a result of the good equilibrium of membrane resistance and electro‐active species permeability, Nafion 212 membrane exhibits the highest electrolyte utilization and energy efficiency during the operation, accompanied by the lowest overpotential. In the final part, the selection of Nafion membrane thickness was optimized on the basis of single‐cell performance and the overall cost of the system. 相似文献
999.
火炕采暖在我国北方农村地区非常普遍,为了取得更好的采暖效果,在原有火炕的基础上,以我国北方农村地区火炕中的回风洞(俗称“狗洞”)为研究对象,通过三组实验对烟囱进口处高温烟气的温度和速度进行了测定,依据流体运动中的三大守恒定律,分别建立了三组实验中烟囱内高温烟气流动的平面二维数学模型,利用FLUENT软件对烟囱内烟气的流动状态进行数值模拟,分析了烟囱进口烟气的运动趋势以及回风洞的有无对反风时火炕采暖系统的影响,最后得出结论是回风洞能有效地减弱外界风流的反向作用,阻止了突然自然反风而造成的烟气回流,甚至是火苗外窜的安全隐患。 相似文献
1000.