Thin hard coatings fracture propagation during the impact test

One of the most significant applications of the impact test is to investigate thin hard coatings fatigue properties. Herein the test conditions and duration up to the film damage initiation, are considered in order to determine the critical stresses associated with the coating fatigue strength. Moreover, the subsequent film damage propagation is a significant mechanism as well, since it refers to the ability of the coating to withstand loads after its fatigue damage initiation. In order to describe the film fracture propagation the failed area ratio was introduced and an algorithm to determine this magnitude developed, based on the analysis of imprint scanning electron microscopy graphs. The application of the coating failed area ratio will be demonstrated in various impact test film cases, also with superficial thin layers. The top layers do not affect, in general, the failure initiation of the basic coating. However, according to the obtained results, the superficial films influence the basic coating failure propagation rate during the impact test.     

Two‐phase production of cyclohexene and cyclooctene oxides in water as an approach to pollution prevention

Liquid–liquid two‐phase epoxidation from cyclohexene and cyclooctene in aqueous potassium peroxymonosulfate (commercially available as Oxone^®) solution was studied as an application in pollution prevention. To avoid potential emissions of volatile organic compounds an aqueous solution was employed to replace the usual chlorinated solvents used in epoxide production. A droplet column reactor and stirred tank reactor were used to investigate two‐phase synthesis of epoxide. An aqueous Oxone^® solution was used to oxidize a dispersion of alkene droplets and form epoxide. The study of aqueous epoxidation in both reactors showed that the epoxidation of alkenes can be represented as a first order reaction with respect to alkene. The salting out effect of Oxone^® concentration was studied in both reactors and found to be very similar at optimal conditions. In comparing the two reactors, it was found that the droplet column reactor produces larger quantities of product per unit reactor volume for the same reaction time. The objective of this study is to provide an alternative reactor design and synthesis route that can meet pollution prevention goals. Copyright © 2004 Society of Chemical Industry     

API长圆螺纹套管抗粘结性能的试验研究

通过对国内外大量石油套管螺纹参数的测量和全尺寸的模拟试验，以及对测量和试验数据的理论分析，找出了影响国产套管发生粘扣的原因，并在实际生产中实施验证。采取相应的措施改善了套管的抗粘结性能，同时套管的密封和抗滑脱性能并未下降。     

天铁炼钢厂四流中间包流场的水模实验及优化

介绍了天铁炼钢厂中间包水模实验原理和过程，分析了斜、直、圆三种型式挡渣墙模拟结果，提出了合理的挡渣控流方案，在生产实践中使用效果良好。     

An experiment for showing some kind of artificial understanding

In this paper we design an experiment which can be depicted as a simple scenario, a very limited 'world'. In this world, there are an actor that can pursue a project and an observer that is keeping its eyes on the actor. We try to show in the experiment that the observer can to some degree understand the actor based on its knowledge and some metaphors, i.e. understand what the actor is doing and why. As the conclusion of this experiment, we try to show some features of 'understanding'. These are (1) that 'understanding' has to be based on some preliminary knowledge; (2) that 'understanding' is a process of incremental learning; (3) that, as for symbolic systems, some metaphors are necessary for mapping real entities into concepts in mind.     

Commercial Test of Multi-functional Desulfurizing Agent TS-01 for Gasoline in FCC Process

Experimental use of multi-functional desulfurizing agent TS-01 for FCC gasoline in the FCC unit of SINOPEC Jiujiang Company shows that the multi-functional desulfurizing agent can effectively remove various kinds of sulfur in FCC gasoline and diesel fuel and fulfill passivation on heavy metals.     

Active set truncated-Newton algorithm for simultaneous optimization of distillation column

An active set truncated-Newton algorithm (ASTNA) is proposed to solve the large-scale bound constrained sub-problems. The global convergence of the algorithm is obtained and two groups of numerical experiments are made for the various large-scale problems of varying size. The comparison results between ASTNA and the subspace limited memory quasi-Newton algorithm and between the modified augmented Lagrange multiplier methods combined with ASTNA and the modified barrier function method show the stability and effectiveness of ASTNA for simultaneous optimization of distillation column.     

实时多任务操作系统响应性能预估和测试

本文给出了作者开发的一个单处理机实时多任务操作系统的响应性能（响应时间，同步时间）的实验结果和／或估算。与国外同期文献发表的数据相比，指标先进。     

焊接试样的焊缝外形尺寸对爆炸试验的影响

选用水面舰艇用９４５钢和潜艇用９２１Ａ钢，研究了不同焊缝外形尺寸对爆炸试验中三缺口试样的中央缺口开裂行为的影响。通过大量的试验数据，确定了开裂判据ｅ≤ｅ_ｍ，为试验前预示中央缺口开裂与否提供了可靠的依据。     

注聚采出水分离用动态水力旋流器特性研究

原有的地面工艺和设备已不能满足聚合物驱采出水分离的要求。采用自行研制的动态水力旋流器，在增压与不增压两种工艺流程下，分别进行了流量和转数对分离效率的影响、转数与压力降的关系，以及入口压力与处理量的关系等项试验研究。试验结果表明，与静态水力旋流器相比，动态水力旋流器的分离效率明显提高，一般可提高10％左右；压力损失显著降低，约可减少0．1MPa，足见可在低压下工作，易于实现无泵运行；无泵运行明显比有泵增压运行的分离效率高，但处理量会有所降低。将动态水力旋流器应用于聚合物驱产出水的油－水分离处理是完全可行的。