稀土硝酸盐与邻香草醛缩邻氨基苯甲酸配合物的合成与表征

由邻香草醛缩邻氨基苯甲酸（以Ｈ２Ｌ表示）与稀土硝酸盐作用合成了３种新固体配合物。并对合成的配合物进行了元素分析、红外光谱、紫外光谱、差热—热重及摩尔电导分析，确定配合物的组成为〔Ｌｎ（ＨＬ）（ＮＯ３）（Ｈ２Ｏ）〕ＮＯ３（Ｌｎ＝Ｄｙ，Ｅｒ，Ｔｍ）。研究了配合物的配位方式和某些物理化学性质。     

深井重泥浆弱凝胶工艺技术初探

重泥浆强凝胶体系对钴井会产生不利影响。笔者结合川东地区的实际情况,分析了重泥浆强凝胶形成的原因和重泥浆弱凝胶的形成机制,提出了形成重泥浆弱凝胶体系的核心和设计原则,总结出了一套以正确使用泥浆添加剂并配合强有力的固控措施为主的成套深井重泥浆弱凝胶工艺技术,介绍了这套技术在川东地区的应用情况。实践证明,少用甚至不用泥浆降粘剂就可获得并维持尽可能低的静切力,使τ_s,10s为0.5—6Pα、τ_s,10min为2—12.5Pα。     

Bulk modification of styrene–butadiene–styrene triblock copolymer with maleic anhydride

The bulk modification of SBS rubber with maleic anhydride in a mixing chamber of a Haake rheomixer was studied. The effect of temperature, maleic anhydride, and benzoyl peroxide concentrations on the grafting efficiency was evaluated. High grafting efficiency was achieved when the ratio of peroxide and maleic anhydride concentration was high. On the other hand, on this condition high insoluble fraction was generated. The addition of a diamine, 4,4′‐diaminediphenylmethane to the reaction mixture minimizes the amount of insoluble polymer. However, the grafted MAH content also decreases. The graft copolymer was characterized by infrared spectroscopy and the grafting extension was determined by titration. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 2953–2960, 2002; DOI 10.1002/app.10355     

精轧油膜轴承密封失效机理的初步分析

对油膜轴承密封出现的进水、漏油现象作了大量的调查、测量和统计分析，找出了产生质量事故的根本原因，提出了解决措施。     

岳城水库供水工程贴边岔管设计

岳城水库供水工程， 邯郸、安阳两城市引水岔管均采用内、外贴边补强板型式对取水口进行局部加强。此补强方法对水流流态干扰较少， 水头损失小。设置这样的岔管对原电站压力钢管结构改动较小， 构造相对简单， 制作与安装方便， 对岳城水库供水这样的改建工程较为适用。     

红外热成象技术在股骨头坏死疾病针刺疗法中的应用

红外热成象技术可以有效地用于股骨头坏死疾病的诊断和针刺治疗效果的评价，效果优于其它常规方法。     

Plasma immersion ion implantation for SOI synthesis: SIMOX and ion-cut

We have demonstrated feasibility to form silicon-on-insulator (SOI) substrates using plasma immersion ion implantation (PIII) for both separation by implantation of oxygen and ion-cut. This high throughput technique can substantially lower the high cost of SOI substrates due to the simpler implanter design as well as ease of maintenance. For separation by plasma implantation of oxygen wafers, secondary ion mass spectrometry analysis and cross-sectional transmission electron micrographs show continuous buried oxide formation under a single-crystal silicon overlayer with sharp Si/SiO₂ interfaces after oxygen plasma implantation and high-temperature (1300°C) annealing. Ion-cut SOI wafer fabrication technique is implemented for the first time using PIII. The hydrogen plasma can be optimized so that only one ion species is dominant in concentration and there are minimal effects by other residual ions on the ion-cut process. The physical mechanism of hydrogen induced silicon surface layer cleavage has been investigated. An ideal gas law model of the microcavity internal pressure combined with a two-dimensional finite element fracture mechanics model is used to approximate the fracture driving force which is sufficient to overcome the silicon fracture resistance.     

红外光控器在蜜丸包装机上的应用

中药大蜜丸及所用包装材料软、粘、轻、小、光,较难实现机械化自动包装。通常的监控方法不适合蜜丸的自动包装。采用红外线光电控制器,解决了自动包装蜜丸时出现的瞬间无纸、无丸等自动控制。     

复合脱氧剂对纯净钢生产的影响

论述复合脱氧剂的一般化学特性，并以碳化硅和硅铝铁两种复合脱氧剂为例，讨论其对改善钢的质量，进行纯净钢生产的影响。     

含钒废水净化回收技术研究

本文讨论了五氧化二钒生产过程中所排出废水的处理方法。认为采用焦亚硫酸钠及硫酸亚铁联合还原中和法为最佳,其技术关键为联合还原剂投料比、pH值、时间及含钒污泥提钒。年处理18万吨废水,可消除80余吨Cr~(+6)、V、Cu等重金属离子污染黄浦江上游水源,能回收粗红钒和含钒污泥提钒,使金属回收率提高4％。