Measurement of metal nanolayers optical parameters using surface plasmon resonance method

The results of experimental definition of optical parameters of silver nanolayers by the method of surface plasmon resonance (SPR) are described. The goniometric installation for measurement of angular dependences of reflection of light by layered nanosructures at the attenuated internal reflection (angular spectrum of reflection) is designed. Calculation of optical parameters of nanolayers is executed taking into account the form of a curve of tin angular spectrum of reflection. The text was submitted by the authors in English.     

A study of the static and dynamic properties of side-chain liquid crystalline polymers in low molar mass mesogens

The static and dynamic properties of solutions of a side chain polysiloxane liquid crystal polymer have been studied in a cyanobiphenyl nematic host as a function of concentration and temperature. Refractive index measurements were carried out on aligned samples and the data used to determine the macroscopic order parameter, S, using Haller's method. Photon correlation spectroscopy has been used to measure ($\text{k}{}_{22}\text{γ}{}_1$) for the pure nematic solvent and the solutions. From these measurements it appears that the static properties vary slowly and linearly with increasing polymer concentration whilst the dynamic or viscoelastic properties change markedly. This change has been attributed to γ₁, the twist viscosity, and the results have been discussed in terms of the function of the siloxane polymer backbone.     

针对语音变换的语音篡改检测

针对使用语音变换技术的语音篡改,提出一种自动检测方法。在分析语音变换基本模型和变换语音失真的基础上,提取语音信号的声道参数以及相关的信号统计量,并通过支持向量机递归特征消除法,选择出对语音变换比较敏感的特征作为分类特征,使用支持向量机进行语音变换检测和变换语音的说话人性别判别。对于一种语音变换软件的实验结果表明,该方法具有较高的检测准确率,其中语音变换检测的平均准确率为94.90%,变换语音的说话人性别判别平均准确率为92.09%。     

通用视觉检测设备的专家在线平台设计

针对视觉检测设备在复杂的生产环境下存在图像处理参数设置问题,设计了一套B/S架构的通用的专家在线平台,通过在原有的视觉检测平台上增加一个普通的USB摄像头及相应的应用软件,并通过网络将出现的新问题的图像实时传输给生产厂家或外部专家,由专家通过浏览器设置合理的图像处理参数,平台综合了数据协同、远程培训等功能,达到了远程解决问题的目的。     

Delay‐dependent stability for Markovian genetic regulatory networks with time‐varying delays

This paper is concerned with the problem of stochastic stability analysis for a class of genetic regulatory networks with Markovian jump parameters and time‐varying delays. A delay‐dependent stability criterion is derived by using a novel mode‐dependent Lyapunov functional. The derived stability criterion is expressed in terms of linear matrix inequalities and is less conservative than the existing ones in the literature. A numerical example is provided to demonstrate the effectiveness of the proposed stability criterion. Copyright © 2011 John Wiley and Sons Asia Pte Ltd and Chinese Automatic Control Society     

Feedback predictive control for constrained fuzzy systems with Markovian jumps

In this paper, a feedback model predictive control method is presented to tackle control problems with constrained multivariables for uncertain discrete‐time nonlinear Markovian jump systems. An uncertain Markovian jump fuzzy system (MJFS) is obtained by employing the Takagi‐Sugeno (T‐S) fuzzy model to represent a discrete‐time nonlinear system with norm bounded uncertainties and Markovain jump parameters. To achieve more generality, the transition probabilities of the Markov chain are assumed to be partly unknown and partly accessible. The predictive formulation adopts an on‐line optimization paradigm that utilizes the closed‐loop state feedback controller and is solved using the standard semi‐definite programming (SDP). To reduce the on‐line computational burden, a mode independent control move is calculated at every sampling time based on a stochastic fuzzy Lyapunov function (FLF) and a parallel distributed compensation (PDC) scheme. The robust mean square stability, performance minimization and constraint satisfaction properties are guaranteed under the control move for all admissible uncertainties. A numerical example is given to show the efficiency of the developed approach. Copyright © 2011 John Wiley and Sons Asia Pte Ltd and Chinese Automatic Control Society     

Effect of deposition conditions on the properties and annealing behavior of cold-sprayed copper

The deposition of copper by cold gas dynamic spraying has attracted much interest in recent years due to the capability to deposit low-porosity oxide-free coatings. However, it is generally found that as-deposited copper has a signicantly greater hardness, and potentially lower ductility, than bulk material. In this article, copper was deposited by cold spraying using helium as the driving gas at both 298 and 523 K. Evidence is presented indicating that the material sprayed at the lower temperature exhibits a lower dislocation density throughout the grain structure than the material sprayed at the higher temperature. The low stacking fault energy of copper restricts recovery during annealing, and thus microstructural changes during annealing only proceed once recrystallization begins. The material sprayed at low temperature (with the low dislocation density) exhibited recrystallization at annealing temperatures as low as 373 K with a corresponding reduction in hardness. However, the copper sprayed with helium at 523 K was resistant to annealing at temperatures up to 473 K where the dislocations in the structure prevented recrystallization. However, at higher temperatures, recrystallization did proceed (with corresponding reductions in hardness). The fracture behavior of the copper that was cold sprayed with helium at 523 K, both in the as-sprayed condition and following annealing, was measured and explained in terms of the annealing mechanisms proposed. The original version of this paper was published in the CD ROM Thermal Spray Connects: Explore Its Surfacing Potential, International Thermal Spray Conference, sponsored by DVS, ASM International, and HW International Institute of Welding, Basel, Switzerland, May 2–4, 2005, DVS-Verlag GmbH, Düsseldorf, Germany.     

解析参数对活性焦再生过程及再生效果的影响

 活性焦的热解析参数对再生活性焦的脱硫脱硝性能和机械强度至关重要。为了明确解析参数对活性焦再生过程和再生效果的影响规律,通过热解析试验探究活性焦硫残余比例、CO₂和CO生成量及再生活性焦脱硫脱硝性能随解析温度和解析时间的变化规律,继而明确适宜的活性焦热解析参数。结果表明,活性焦升温解析过程中,脱硫产物在317 ℃左右迅速分解,随后分解速率下降;在进入恒温解析阶段后脱硫产物分解速率先快速下降,而后进入缓慢解析状态。硫残余比例随恒温解析温度的升高而下降,在530 ℃下解析3 h可使脱硫产物完全解析;解析温度高于430 ℃后,活性焦表面的酚基、醌基、内酯基等含氧官能团分解量明显增加,并随恒温解析温度的升高而持续增加,分解所生成的CO和CO₂也随之大幅增加,这将使活性焦的孔隙结构进一步发展,继而不利于活性焦机械强度的保持;解析温度低于530 ℃时,硫残余比例随解析温度的升高而持续降低,使再生活性焦的脱硫脱硝性能持续提高;解析温度高于530 ℃后,含氧官能团分解量随解析温度的升高而持续增加,这将有利于提高活性焦表面SO₂氧化反应速率,继而使再生活性焦的脱硫性能持续升高,但酚基、内酯基等酸性含氧官能团的分解使再生活性焦对NH₃的吸附性能降低,进而使其脱硝性能降低。在兼顾再生活性焦脱硫脱硝性能、机械强度和生产效率等多方面因素时,430 ℃恒温解析3 h是相对较优的解析参数。在此解析条件下,再生活性焦的硫残余比例仅为1.8%,含氧官能团尚未发生大量分解,脱硫脱硝性能相对较为优良。     

离心泵性能参数的自动测定和自动控制

通过将计算机技术应用于离心泵性能参数的研究，实现了离心泵性能参数的自动测定和自动控制。     

Determination of the solubility parameter of poly(ethylene oxide) at 25°C by gas-liquid chromatography

The solubility parameter of poly(ethylene oxide) at 25°C has been determined using the method developed by DiPaola-Baranyi and Guillet, by the extrapolation of the values of the interaction parameter χ, at high temperatures, ranging from 70°–90°, 90°–110° and 110°–130°C down to 25°C. The values of the solubility parameter obtained, depending on the temperature ranges employed, are 9.8, 9.9 and 10.1, respectively.