压力容器用钢和舰船钢平面应变止裂韧度KIa的行为表征

针对几种常用的压力容器用钢和舰船钢介绍了平面应变止裂韧度试验的全过程,得到了几种材料不同温度下的平面应变止裂韧度值。同时观察了止裂韧度试验的特征断口,并对试验结果进行了分析讨论。     

多晶体钛拉伸变形表面褶皱的形成及晶粒变形

用原子力显微镜对多晶体钛拉伸塑性变形中表面褶皱的形成及单个晶粒的变形进行了连续观察和测量.结果表明,表面褶皱随着应变量的增加而增大,而凹凸的相对位置关系不随变形的进行而变化.从单个晶粒来看应变量在0.1附近时由于孪晶的形成产生了新的凹凸,但对整体的表面褶皱凹凸位置关系没有大的影响.表面平均粗糙度和表面最大高低差随应变量的增加近似呈直线性增大,应变量在0.1左右时由于孪晶的形成,使粗糙度有较明显的增大.     

XPS characteristics of sulfur of bio-oxidized arsenic-bearing gold concentrate and changes of surface nature of bio-oxidation residue

During bio-oxidation of sulfides, the chemical state change of sulfur is a complex and key factor. It is not only an indicator of the extent and intensity of the bio-oxidation, but also controls the property of bio-leaching medium and the period of oxidation. The chemical state of sulfur in sulfides oxidized by leaching bacteria was studied with XPS. Sulfide minerals in the arsenic-bearing gold concentrate consist of pyrite, arsenopyrite, chalcopyrite, galena, sphalerite and so on. In order to probe the pattern of the chemical state change of sulfur in the bio-oxidation residue of arsenic-bearing gold concentrate, the structure of the grains, and the surface nature of the residue, XPS test was carried out through different sputtering duration. The study of XPS clearly shows that: sulfides is progressively oxidized from the surface of minerals to the core by leaching bacteria; the chemical valence of sulfur changes from S^2- or [S2]^2- to [SO4]^2- ; sulfur in the core is in a reduction state, S^2- or [S2]^2- , but exists in an oxidation state S^6 on the surface; due to the chemical state change of sulfur, mineral phase of the bio-oxidation residue is also changed(sulfides inside, while sulfates outside); the layered structure is found in the grains of the bio-oxidation residue.     

金刚石钻磨头超声振动钻磨硬脆材料表面质量的试验研究

硬脆材料以其优良的性能在生产实践中得到了广泛应用，但其低塑性、易脆性及不导电性等使得加工十分困难，尤其是超精密表面制作更加困难。为此，本文将超声振动引入普通钻磨中，介绍了超声振动切削原理，通过超声与普通两种方式下的表面粗糙度试验和微观形貌观察得出以下结沦：1）不同加工参数时，超声振动钻磨时的工件表面粗糙度值均低于普通钻磨时的表面粗糙度值；2）随着进给量、工件转速和输入功率的增加，超声和普通钻磨时的表面粗糙度均呈上升趋势；3）普通钻磨加工后孔壁表面有宽度和间距不均匀的沟槽，并且沟槽较宽，而超声钻磨加工后表面沟槽（划痕）较浅且均匀。     

液态铝合金表面张力快速检测新方法与装置

表面张力是液态合金的重要物性参数之一,铝合金表面张力与其变质处理效果及充型能力等质量参数密切相关,研究铸造铝合金表面张力快速检测方法及装置,对于开发铝合金熔炼质量炉前实时评价系统具有非常重要的实际意义.介绍了一种液态铝合金表面张力快速测试的新方法和新装置,新方法以固定时间内吹入被测液体的气泡个数以及气泡在生长过程中内部压差变化为信息参数,通过回归公式求解表面张力.基于该方法研制的表面张力新型测试装置由单片机测控单元、探头及其锁紧和升降机构、供气单元等部分构成.采用新装置可在5 s内测得铝合金表面张力,且具有较高的测试精度.     

NH_3 Plasma Surface Treatments of Engineering Fluoropolymers: A Way to Enhance Adhesion of Ni or Cu Thin Films Deposited by Electroless Plating

FLUOROPOLYMERS(FPs)are thermoplasticmaterials which exhibit a number of unique chemicaland physical characteristics that no other man-madeplastic product gets together.For example,FPs showvery good resistance to almost all chemicals,excellentwater vapor barrier properties,high thermal stability,outstanding electrical insulation properties(lowdielectric constant and dissipation factors),extremelylow frictional coefficient giving them high auto-lubrication properties,high resistance to rad…     

复杂型面的复合光整加工实验研究

利用电火花-超声和脉冲电化学复合加工工艺对三维复杂型面的光整加工进行了研究,论述了电火花超声复合加工的原理及超声装置的设计,进行了工艺参数实验研究,通过Master CAM软件实现型面的造型、编程,进行了三维型面的精密成形加工,经过脉冲电化学抛光后使型面达到镜面效果.     

精密分度装置中蜗轮副的啮合分析

对新型蜗轮剐齿面啮合进行理论分析，指出它的一些特性：齿面容易获得较高精度；接触线走向容易形成油膜；齿面诱导曲率小，可承受较大载荷，使用寿命长。     

Preparation of flee-standing diamond films for high frequency SAW devices

Free-standing diamond films were prepared by hot filament chemical vapor deposition （HFCVD） method under different conditions. Inter-digital transducers （IDTs） were formed on the nucleation sides of free-standing diamond films by photolithography technique. Then piezoelectric ZnO films were deposited by radio-frequency（RF） reactive magnetron sputtering to obtain the ZnO/diamond film structures. Surface morphologies of the nucleation sides and the IDTs were characterized by means of scanning electron microscopy （SEM）, atomic force microscope （AFM） and optical microscopy. The results indicate that the surfaces of nucleation sides are very smooth and the IDTs are of high quality without discontinuity and short circuit phenomenon. Raman spectra show the sharp diamond feature peak at about 1 334 cmI and the small amount of non-diamond carbon in the nucleation side. X-ray diffraction （XRD） patterns of the structure of ZnO/diamond films show a strong diffraction peak of ZnO （002）, which indicates that as-sputtered ZnO films are highly c-axis oriented.     

激光熔覆钴基合金时的钢基表层结晶机制

采用激光熔覆工艺在 2 0钢基体上获得了 2 0 4Co合金涂层。应用剥离法借助光镜、电镜、波谱仪及X射线衍射仪对基体表层及相关部位的组织及成分分布进行了分析研究。结果表明 :在本试验条件下 ,钢基表层的结晶机制为平面外延方式生长和胞状螺型位错方式生长 ;增加能量输入有利于向后一方向发展 ,并使热影响区组织粗化 ,甚至产生显微裂纹 ;尽管扩散层碳贫化 ,但其它合金元素的固溶和孪晶亚结构使之强化 ,而且钴、铬使之具有良好的耐蚀性。