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211.
Mesoporous GaSBA-15 molecular sieves with different nSi/nGa ratios have been directly synthesized using Pluronic 123 triblock polymer as a structure-directing agent by pH-adjusting method. The mesoporous materials have been characterized using ICP-AES, XRD, N2 adsorption, 71Ga-MAS NMR, SEM and TEM. ICP-AES studies show a high amount of gallium incorporation on the silica pore walls. The structural and textural properties of calcined GaSBA-15 are characterized by XRD and N2 adsorption. 71Ga MAS NMR results demonstrate that a high amount of tetrahedral-gallium could be substituted for Si in the framework of SBA-15. TEM and FE-SEM images show the uniform pore diameter and rope-like hexagonal mesoporous structure of GaSBA-15. These GaSBA-15 materials have been used as catalysts for vapour-phase t-butylation of 1,2-dihydroxybenzene (DHB) for selective synthesis of 4-t-butylcatechol (4-TBC) under different reaction conditions. GaSBA-15(10) gave the highest 93.2% conversion of DHB and 95.7% selectivity of 4-TBC as compared with other GaSBA-15 catalysts. 相似文献
212.
The temperature programmed (palladium) hydride decomposition appeared very effective method for diagnosing the extent of alloying in Pd-Pt/SiO2 catalysts. Introduction of Pt to Pd catalysts moves the TPHD peak gradually towards lower temperatures and the shift in hydride decomposition peak is accompanied by a decrease in the amount of released hydrogen. The catalysts prepared the direct redox method showed much better alloy homogeneity than the samples prepared by coimpregnation. The results of probing with other techniques, i.e. catalytic probing with hydrodechlorination of CCl2F2 and XRD, were in line with TPHD data. The catalytic probing showed the presence of synergistic effect, a clear indication of Pd-Pt mixing. XRD data of post-reaction samples showed carbon incorporation into Pd-rich phase, whereas separate Pt-rich phase did not experience any bulk carbiding. 相似文献
213.
WANG Ju-hui 《通讯和计算机》2008,5(11):48-52
This paper comes true a system of facial detection and location. Firstly, it realizes the facial detection of candidate region used skin color for the given image, and considers the influence of similar skin. Secondly, it realizes the location for eye region used the gray characteristic of eye and correction of central measurement, and makes further selection for facial candidate region. The end, it normalizes the facial image and makes it as front standard image, so realizes the facial characteristic location. 相似文献
214.
Calin D. Morosan 《Information Processing Letters》2006,100(5):188-193
Broadcasting is the process of spreading one piece of information among a group of individuals connected by an interconnection network. In this paper we give exact lower and upper bounds for the number of broadcast schemes in arbitrary networks. Also, we give the exact value for complete bipartite graphs and an upper bound for regular networks. Based on the counting method we describe a new random algorithm for broadcasting in networks. 相似文献
215.
Christoph Böhringer Wolfgang Wiegard Collin Starkweather Anna Ruocco 《Computational Economics》2003,22(1):75-109
The double or even triple dividend hypothesis of green tax reforms has beena major issue of dispute in both the scientific community and the politicalarena during the last decade. Theoretical analysis has provided a number ofimportant qualitative insights to the debate but lacks of actual policyrelevance due to very restrictive assumptions. Applied research that takes thestep from stylized analytical to complex numerical models usually comes as ablackbox to non-expert modelers. This paper aims at bridging the gap betweenstylized theoretical work and numerical analysis. We develop a flexible,interactive simulation model which is accessible underhttp://brw.zew.de. Users can specify their own green tax reforms andevaluate the induced economic and environmental effects. Based on illustrativesimulations, we demonstrate the usefulness of our do-it-yourself approach fora better understanding of the double (triple) dividend hypothesis. 相似文献
216.
对T形线路的故障测距,现有方法都是先判断故障支路,再将3端线路等效成2端线路进行测距。但在 T节点附近短路,尤其是经高阻短路时,现有的测距方法由于无法正确判别故障支路而存在一定范围的测距死区。针对上述缺陷,分别假设故障发生在某一支路,由假定正常的2段支路端的电压、电流推算求得 T节点电压和注入假定故障支路的电流,从而分别求得3个故障距离。经证明,求得的3个故障距离有且仅有1个在0和对应支路总长度之间,该距离就是真实的故障距离,故障发生在对应支路上。该方法无需事先判别故障支路即可测距,在 T节点附近经高阻故障时无测距死区。其测距精度理论上不受过渡电阻和故障类型影响,无需故障前数据,且对滤波无高要求。EMTP仿真结果表明该方法正确、有效,测距精度高。 相似文献
217.
通过火焰原子吸收光谱法对水中的锑量进行了测定,对影响测量结果的不确定度分量进行了量化的计算,从而得出影响锑量测量不确定的主要因素是测量样品消解液中的锑的质量浓度引起的不确定度. 相似文献
218.
219.
Failure analysis of hollow glasses The failure analysis is very important to clarify damages of hollow glasses. Damages of glass bottle through over pressure are very often linked with damages to persons. This is the reason why the causal research is from particular importance. Different surface characteristics of glass fragments as well as the fracture pattern give hints to the direction of the crack, the stress just before breakage and the reason of stress. A reconstruction of the bottle is a further helpful instrument for cause studies. The difference of the various characteristics of the surface will be explained. Further on there will be discussed different reasons and mechanism of fracture. 相似文献
220.
厦门市气源转换的技术分析 总被引:3,自引:2,他引:1
分析了气源转换时原有输配系统的管道、调压设备、计量设备、用气设备与天然气系统相适应的问题,提出了相应的措施。 相似文献