Evolution of BET internal surface area in glassy carbon powder during thermal oxidation

It is demonstrated that glassy carbon powder can be thermochemically activated. During activation, a film with open pores is created on the glassy carbon particles. This film has a large internal surface area, which is accessible to liquids and gases. A simple model for the evolution of the internal surface area in glassy carbon powder during thermochemical gas-phase oxidation is also presented and compared with experimental data. Experimental results are in qualitative agreement with the model. We found that a sharp particle size distribution is desirable with regard to potential technical applications.     

西安绿色康居小区规划设计剖析

通过对西安绿色康居小区规划设计的实例分析，阐明了小康型住宅区的标准和要求，在旧城住宅区改造中的落实和运用，试图探索下一世纪旧城住宅区的改造之路．     

一种派生式与创成式相结合的CAPP系统

本文结合为某机械厂开发的实用计算机辅助工艺设计系统(JJCAPP),论述了一种兼有派生式和创成式特点的综合式工艺自动设计方法.     

潦河灌区农业水费计收现状分析及对策

阐述了潦河灌区农业水费计收现状，对水费计收现状进行分析并提出解决办法。     

Long-term measurements of the concentrations of halocarbons in an urban area of Kraków, Poland

The results of the measurements of the concentrations of freons (F-11 and F-113), chloroform (CHCl₃), trichloroethane (CH₃CCl₃) and carbon tetrachloride (CCl₄) in air are presented. The data concern concentration measurements that have been conducted in Krakow since half way through 1997 to the end of 1999. The mean monthly values of these concentrations have been compared with the data from Mace Head, the station situated at a similar longitude as Krakow. It has been concluded that, in the observed period of time, the concentrations of the pollutants in Krakow are higher than in Mace Head. The mean monthly concentrations of F-11 and CCl₄ decrease in Krakow faster than in Mace Head (2.5 and 3.3 times, respectively). The concentrations of CHCl₃ and CH₃CCl₃ decrease at both locations, but the change is greater in Krakow. In Krakow, the observed increase of F-113 is 0.13 ppt/month and has an opposite trend than in the same period at Mace Head.     

浅论水电规划工作思路

在水电的前期设计阶段，规划专业的重要性显而易见。由于水电规划工作涉及专业很多，如果仅停留于规划专业本身，未必能解决问题。在规划工作中，既有定量的计算，也有定性的分析；既要站在国家的角度进行评价，也要进行企业的财务效益分析；既要考虑目前的现实情况，也要对未来的发展做出预测；既有企业的主观意志，也有自然、社会历史的限制。总之，规划专业是涉及多目标、多量纲的综合判断，若以局部来通观全体，则一定要流于片面的谬误。因此，水电规划工作须进行辩证的综合研究。     

Occurrence of Lawn Care and Agricultural Pesticides in the Don River and Humber River Watersheds (1998–2002)

Between 1998 and 2002, surface water samples were collected from several sites in the Don River and Humber River watersheds, both tributaries to Lake Ontario, and analyzed for a variety of pesticides, including those used for urban lawn care. Analyses included 152 pesticide active ingredients and eight metabolites. Samples were collected during base flow periods (i.e., dry events) and rainfall events (i.e., wet events). The objectives of the study were to determine which pesticides were detectable, whether there was a difference in the detection frequency between the two watersheds and between upstream and downstream in each river, and whether precipitation influenced the frequency of detection. Eleven pesticides and one metabolite were detected in surface waters of the Don and Humber rivers or their tributaries, with approximately 72% of samples containing at least one pesticide attributable to lawn care use. The pesticides and pesticide metabolite detected in this study included 2,4-D, atrazine, bromacil, carbofuran, chlorpyrifos, cypermethrin, diazinon, dicamba, MECOPROP, metolachlor, metribuzin, and an atrazine metabolite (des-ethyl atrazine). Four pesticides exceeded federal or provincial water quality guidelines/objectives. Diazinon exceeded the provincial water quality objective in 28% of the samples taken. For the three other pesticides (atrazine, carbofuran and chlorpyrifos) exceedance of a water quality criteria occurred in less than 1% of the samples.     

The amylose and lipid contents,dimensions, and gelatinisation characteristics of some wheat starches and their A- and B-granule fractions

Starches isolated from 23 bread wheats (Triticum aestivum) and 26 durum wheats (T. durum) contained 26.3-30.6% (mean 29.1%) total amylose, 19.3–25.1% (mean 22.9%) apparent amylose and 783–1144mg 100g^?1 (mean 977 mg 100g^?1) lysophos-pholipids. Gelatinisation temperatures were 57.3–64.9°C (mean 61.8°C) and enthalpies 6.4–11.8 Jg^?1 (mean 9.7Jg^?1) in excess water, measured by differential scanning calorimetry. There were no correlations between any of these parameters. Starch granule size distributions were determined with a Coulter Counter and 100–channel analyser. A-granule mean volumes were 1235–2585μm³ (av. 1778), modal volumes 863–1804μm³ (av. 1264), mean diameters 13.9–16.0μm (av. 13.99), and specific surface areas 0.236–0.302m²g^?1. B-granule mean volumes were 35.4–100.4μm³ (av. 55.9), modal volumes 16.5–54.5μm³ (av. 27.7), mean diameters 3.66–5.07μm (av. 4.09), and specific surface areas 0.684–0.920m²g^?1. The B-granule contents of the starches were 12.8–34.6% (av. 27.3) by weight (sedimentation method) and 13.0–37.3% (av. 24.0) by volume (Coulter method), the latter being the more accurate method.     

鄂尔多斯西缘前陆盆地巨厚黄土地区地震采集技术

鄂尔多斯西缘前陆盆地表层地质地貌极其复杂，有巨厚黄土区、黄土-沙漠区及山前砾石-黄土区，独特的黄土地貌使得地震采集面临着诸多技术难题。根据以往巨厚黄土地区地震采集经验，采用多种方法系统地开展黄土表层结构精细调查，深入研究黄土地球物理特征及激发因素与表层黄土结构之间的关系，优选激发井位和井深，确保了激发效果；采用小道距、三线小线距、高密度空间采样技术，获得了高信噪比、高分辨率地震资料。研究表明，巨厚黄土地区地震采集时应优选激发井位和岩性，合理选择激发井深；坚持多深井组合激发、单井药量不宜过大总药量要大两项基本原则；采用高密度采样技术，提高采集资料的覆盖次数和信噪比。图10表1参15