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21.
KINETICSOFLIQUIDPENETRATINGINTOGRAINBOUNDARY¥Chen,Kanghua;Huang,Baiyun(PowderMetallurgyResearchinstitute,CentralSouthUniversi... 相似文献
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煤与粘结剂的相互作用和型煤抗压强度的关系 总被引:1,自引:2,他引:1
煤的润湿性与型煤抗压强度相关。用于表征煤的润湿性方法有煤与淀粉粘结剂的接触角、粘合功、煤的润湿临界表面张力等。研究证明,随着煤化程度的升高,煤与淀粉粘结剂接触角变小,粘合功增加,粉煤的润湿性改善,型煤抗压强度得以提高。另外,煤的润湿临界表面张力越大,煤的润湿性越好,型煤抗压强度也就越高。 相似文献
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Hans-Joachim Kleebe Giuseppe Pezzotti 《Journal of the American Ceramic Society》2002,85(12):3049-3053
The grain-boundary structure of a model SiAlON polycrystal with nominal composition Si5 AlON7 was characterized by transmission electron microscopy (TEM) both in an equilibrium (as-processed) state at room temperature and after quenching from elevated temperature. In addition, low-frequency (1–13 Hz) internal friction data were recorded as a function of temperature, showing a pronounced grain-boundary sliding peak positioned at 1030°C. High-resolution transmission electron microscopy (HRTEM) of the equilibrated low-temperature microstructure revealed residual glass only at multigrain junctions, but no amorphous intergranular films were observed. The detection of clean interfaces in the as-processed sample contradicts the internal friction data, which instead suggests the presence of a low-viscosity grain boundary phase, sliding at elevated temperatures. Therefore, a thin section of the as-sintered material was heated to 1380°C and rapidly quenched. HRTEM analysis of this sample showed, apart from residual glass pockets, wetted grain boundaries, which is in line with the internal friction experiment. This wetting-dewetting phenomenon observed in z = 1 SiAlON is expected to have a strong impact not only on high-temperature engineering ceramics but also on geological, temperature-activated processes such as volcanic eruptions. 相似文献
26.
Nathalie Nadeau Gérard L. Vignoles Claude-Michel Brauner 《Chemical engineering science》2006,61(22):7509-7527
The film-boiling chemical vapor infiltration (CVI) process is a fast process developed for composite material fabrication, and especially carbon/carbon composites. In order to help define optimal conditions, a local 1D model has been developed to study the densification front which establishes itself during the processing of a carbon/carbon fibrous preform. The model features heat conduction, precursor gas diffusion, densification reactions and structural evolution of the porous medium. The effects of total mass flux, Thiele modulus, porous medium geometry on front behavior parameters such as width, velocity and residual porosity are presented as semi-analytical correlations. An existence criterion is produced, which involves a minimal heat flux. Comparison between process-scale experiments and simulation is then possible by inserting the semi-analytical results achieved in the local study of the front into a light numerical model involving the entire preform. The model has been validated with respect to previous experimental and numerical data. 相似文献
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The effect of partial internal wetting of catalyst pellets on apparent reaction kinetics at elevated temperatures and pressures is investigated experimentally and by modeling for benzene hydrogenation. A new method that combines adsorption and chemical reaction is introduced to study the kinetics influenced by capillary condensation of reagents at steady-state conditions. It is shown that the extent of liquid filling in the pellet interior has a critical effect on the global kinetics, and the current state of the catalyst depends on the history. Under certain conditions two steady states of the effectiveness factor exist. Moreover, either a decrease in temperature or increase in total pressure can increase the effectiveness factor. The model exhibits good agreement with experimental results. 相似文献
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介绍了橡胶工业橡制品生产中胶坯制备的三种方法,其中详细介绍了精密预成型机制备胶坯。以上海德仁橡塑机械有限公司物精密预成型机为例,从结构,性能及工艺参数等方面进行了分析,说明精密预成型机是批量生产橡胶模型制品的一种得力辅助设备。 相似文献
29.
针对湿热地区潮湿气候作用下建筑保温砂浆受潮的规律,采用天平称重法对玻化微珠保温砂浆进行了自然状态吸放湿实验,并采用热湿气候风洞实验法对其质量平衡含湿率进行测定,进而采用平板法对其湿平衡状态下的导热系数进行了一系列测试分析。结果表明,在南方地区潮湿气候条件下玻化微珠保温砂浆质量平衡含湿率约为3.55%;湿平衡状态下玻化微珠保温砂浆导热系数修正系数在1.04~1.11之间,平均值为1.08,考虑受潮现象的复杂性,建议在实际建筑工程节能设计时,该修正系数宜取1.10。 相似文献
30.
In this study,FTIR and XPS spectroscopy,specific surface area and pore size analyses,wetting and other experimental means have been applied to investigate respirable coal dust surface properties and wetting mechanism.The research shows that coal dust surface structures,chemical and element compositions are changed in the refining process of coal dust.Compared with large particle coal dust,respirable coal dust is a weak hydrophilic and strong hydrophobic substance.The reason:the smaller the particle size of coal dust,the more unsaturated its surface.The absorption of air is strong and it is easy to form an air film on coal dust surfaces.Coal dust contact with water is actually a compound contact of liquid in contact with a solid and gas in contact with a solid.The smaller the particle size,the larger the pore volume and the higher the degree of surface roughness,the larger the area of gas in contact with a solid and the worse the coal dust wettability.Another reason is that the changes in the composition of atoms on the dust surface and structures affect coal dust wettability.The results of this study establish a theoretical basis for the invention of effective reduced-dust technology. 相似文献