非对称配钢钢骨混凝土柱抗震性能试验研究

为研究非对称配钢钢骨混凝土柱的抗震性能,进行了12个T形配钢、12个L形配钢的钢骨混凝土柱试件在低周往复荷载作用下的试验研究,试验参数为剪跨比、轴压比、体积配箍率以及是否配置拉结筋,对受力过程、破坏形态、滞回特性、骨架曲线、延性、耗能能力等进行了分析比较。结果表明,在恒定轴向荷载和水平低周往复荷载共同作用下,非对称配钢钢骨混凝土柱表现出较好的受力性能,破坏形态主要有弯曲破坏、剪切黏结破坏、剪切斜压破坏、剪切复合型破坏4种,各试件表现出较明显的正负滞回环不对称现象。剪跨比对破坏形态有较大影响,剪切复合型破坏主要发生在配有严重不对称的L形配钢的试件中;各试件的延性性能均随轴压比的增大而降低,在L形配钢试件中更为明显;增大配箍率对T形配钢试件的延性和承载力均有明显的提高,并能改善试件屈服后的耗能能力,有效改善混凝土的脆性性质,但对于剪跨比较小的L形配钢试件受力性能的改善并不明显;配置拉结筋能够提高各试件的承载能力,改善加载后期试件的承载力衰减和刚度退化,并明显增强了L形配钢试件的变形能力。     

轻钢结构在大柱网工业厂房中的应用

结合具体工程设计实例,从力学模型建立、柱脚抗剪键设置、屋面坡度选择、屋面雪载取值等方面的优化与创新,介绍轻钢结构在大柱网工业厂房中的应用。同时通过大量的工程实例,介绍轻钢结构大柱网工业厂房的用钢量,可供同行参考。     

降低工业萘初馏塔酚油含萘量的试验

用改变工业萘生产装置初馏塔塔顶温度的方法,降低酚油中的含萘量,试验表明,塔顶温度降至196－199℃后,可使酚油中的含萘量降至30％左右,并可相应提高萘的提取率。     

Separation of Oil from Wastewater by Column Flotation

A new type of device, a dissolved-air flotation column, was developed for separation of oily wastewater.The unique design idea of the dissolved-air flotation column is the combined use of dissolved-air flotation and column flotation.The dissolved air release occurred within the column separation system.As a potential application the column was investigated for its performance in separating emulsified oil droplets in oily wastewater.A high separation efficiency was obtained in a series of tests.The aeration performance of the bubble generator used in the dissolved-air flotation column was also studied in particular.     

活塞式压缩机吸排气管道的振动与控制

阐述了活塞式压缩机吸、排气管道强烈振动的危害，分析了产生共振的原因，介绍了现场消减管道振动的有效措施。     

Three-dimensional Computational Fluid Dynamics Modeling of Two-phase Flow in a Structured Packing Column

Characterizing the complex two-phase hydrodynamics in structured packed columns requires a power-ful modeling tool. The traditional two-dimensional model exhibits limitations when one attempts to model...     

重烷苯中二烷基苯和茚满萘满的分离与鉴定

通过柱层析的方法将重烷基苯大致分成了6个族组分,重点对第Ⅱ族组分、Ⅲ族组分进行了分析和鉴定。通过红外光谱的鉴定,大致确定第Ⅱ族组分主要为二烷基苯,第Ⅲ族组分主要为单烷基苯和少量的二烷基茚满、萘满(DT)。然后用紫外法求得了第Ⅱ族组分中邻、间二烷基苯之和与对二烷基苯的质量比约为1：4．09。第Ⅲ族组分中DTI的质量分数约为7．23％,DTI在重烷基苯中所占的质量分数约1．22％。     

Encapsulation of titanium dioxide in styrene/n‐butyl acrylate copolymer by miniemulsion polymerization

Miniemulsion copolymerization of styrene/n‐butyl acrylate was investigated as a means of encapsulating hydrophilic titanium dioxide (TiO₂) in a film‐forming polymer. Dispersion studies of the TiO₂ were first carried out to determine the choice of stabilizer, its concentration, and the dispersion process conditions for obtaining stable TiO₂ particles with minimum particle size. Through screening studies of various functional stabilizers and shelf‐life stability studies at both room and polymerization temperatures, Solsperse 32,000 was selected to give relatively small and stable TiO₂ particles at 1 wt % stabilizer and with 20–25 min sonification. The subsequent encapsulation of the dispersed TiO₂ particles in styrene/n‐butyl acrylate copolymer (St/BA) via miniemulsion polymerization was carried out and compared with a control study using styrene monomer alone. The lattices resulting from the miniemulsion encapsulation polymerizations were characterized in terms of the encapsulation efficiencies (via density gradient column separations; DGC) and particle size (via dynamic light scattering). Encapsulation efficiencies revealed that complete encapsulation of all of the TiO₂ by all of the polymer was not achieved. The maximum encapsulation efficiencies were 79.1% TiO₂ inside 61.7% polystyrene and 63.6% TiO₂ inside 38.5% St/BA copolymer. As the density of the particles collected from the DGC increased from one layer to another, both the average particle size and the number of the TiO₂ particles contained in each latex particle increased. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 3479–3486, 2006     

亲水性Obelisc R液相色谱-串联质谱法测定猪肉样品中氨基糖苷类药物残留

建立了高效液相色谱-串联质谱法测定猪肉中9种氨基糖苷类药物(壮观霉素、潮霉素B、双氢链霉素、链霉素、阿米卡星、卡那霉素、安普霉素、妥布霉素、庆大霉素)残留量。待测样品中的氨基糖苷类药物经磷酸盐缓冲溶液提取,调节pH值后,经SupelMIP~ SPE-Aminoglycosides分子印迹固相萃取柱净化、浓缩、定容,然后采用Obelisc R高效液相色谱柱分离,以串联质谱法正离子模式检测。该方法在20~1 000μg/L范围内线性关系良好。在线性范围内,分别进行高、中、低3个浓度的添加实验,样品的回收率在76.9%~89.4%之间,相对标准偏差在3.56%~11.4%之间。该方法简便、快速、准确,可以满足猪肉中氨基糖苷类药物残留的测定需求。     

HYDRODYNAMICS AND MASS TRANSFER IN A NEW TYPE (FG) STACK PACKED EXTRACTION COLUMN

1 INTRODUCTIONOne of the major objectives in the study of extraction column is to minimize column di-mensions to fulfill a certain specific separation process.This has led to the intensiveemployment of structured packings in extraction columns [1].One of the recentdevelopments targeted for greater interfacial areas without excessive dispersion is the useof structure packings contactive claiming advantages,such as lower fluid flow friction