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31.
32.
Hydrothermal synthesis and in situ surface modification of boehmite nanoparticles in supercritical water 总被引:2,自引:1,他引:1
T. Mousavand S. Ohara M. Umetsu J. Zhang S. Takami T. Naka T. Adschiri 《The Journal of Supercritical Fluids》2007,40(3):397-401
In situ surface modification of boehmite (AlOOH) nanoparticles during hydrothermal synthesis in supercritical water was examined by adding CH3(CH2)4CHO and CH3(CH2)5NH2 as modifier reagents to the reactants. Changes in surface properties of the nanoparticles by surface modification was observed by FTIR, dispersion in solvents and TEM analyses, which demonstrated that reagents chemically binded onto the surface of the AlOOH nanoparticles. The results of SEM and TEM pictures show that the surface modification affects crystal growth and reduces the particle size and changes the morphology of the particles. 相似文献
33.
介绍65t/h煤粉炉的基本概况和存在的问题,详细阐述了采用水平浓缩煤粉燃烧技术对原燃烧器的改造过程,对改造前后运行参数及经济效益进行了对比。 相似文献
34.
Phase-separated domains prepared in the two-phase region were dissolved at a temperature in the single-phase region, and their dissolution dynamics was studied by using the time-resolved light scattering (TRLS) technique and a scanning electron microscope (SEM). The time tps of preparation of domains was chosen to be long enough for phase separation to proceed into the late stage. The scattered light intensity at small wavenumbers increased before it attenuated. As tps increased, the increase at smaller wavenumbers became more significant and the peak intensity decreased only slightly with dissolution time. The characteristic wavenumber qm evaluated from TRLS and SEM followed the power-law relation qmt−0.3. 相似文献
35.
为探索山丘地区中小型泵站技术改造的经验,选定南康县四个小型泵站作为泵站改造的试点站,进行现场测试,根据测试成果,分析各站存在的问题及效率偏低的原因,并拟定各站技术改造的措施,经实施后取得了较好的效果,本文就南康县泵站改造的实际效果阐明泵站改造的必要性及其改造过程中值得注意的问题。 相似文献
36.
通过对反击式粉碎机粉尘产生的原因进行分析,引入非均相物系重力沉降分离原理,设计了大同煤预粉碎工程的除尘装置,取得了良好的使用效果. 相似文献
37.
The effect of tetramethylammonium cations (TMA+) on TiO2 crystal morphology in hydrothermal conditions has been studied. The as-synthesized samples were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM) methods. The morphologies including besom-like particle, nanosheet and nanotube have been observed. The different ways TMA+ cations in the hydrothermal bases affect the crystal growth manner are suggested to be responsible for the different morphologies of the as-synthesized samples. 相似文献
38.
从目前市场需求和就业率出发,进行形势分析,提出优化专业设置、加强实践环节、提高高职学院办学层次、推进“双证书”制度等改革方法,以促进化工职业教育的发展。 相似文献
39.
阐述了一个全新的聚丙烯腈高聚物溶解理论,取代了以往人们思维中的高聚物大分子必须经过先溶胀再溶解的漫长的静态溶解过程。对于年产50kt/a腈纶装置可减少一次性投资约1500万元,减少运转费用360万元/a,在现有腈纶大装置上实施,经济效益十分可观。 相似文献
40.
X.B. Tu B. Jian S.J. Wang H.Y. Bian J. Wang S.G. Li 《Tunnelling and Underground Space Technology incorporating Trenchless Technology Research》2005,20(4):1106
Granite is commonly recognized as an ideal medium for underground construction. However, in the site investigation for Heimifeng Pumped Storage Power Station project, it was found that there are swelling behaviors induced by alteration in granite and eventually causing slaking and disintegration of rock blocks. The study shows that hydrothermal alteration in granite is primarily due to the intrusion of multi-phase igneous magma. The clay minerals, such as montmorillonite, chlorite, kaolinite, are the main causes for the swelling behavior of granite. In the exploratory adits, alteration was observed to occur mainly along faults or fractures in the rock masses and resulted in roof caving if water is present. Some of the highly altered borehole cores swell and crack within 24 h in water and eventually disintegrate completely. From the testing results on the samples, the maximum axial free swelling strain is about 1.2%, while the maximum axial confined swelling strain is around 0.1% with swelling stress less than 25 kPa. Under free swelling tests, 80% of swelling is completed within 24 hours. Under confined swelling condition, swelling process is completed within 1 h for some samples, with 80% of maximum swelling strain finished within around 22 h for most of the samples. Contraction of samples occurs after swelling completed. The strength of granite, reflected by deformation and elastic moduli, shear strength, decreases due to alteration. The deformation and elastic moduli are even lower compared to highly weathered rock. The shear strength is between that for highly weathered and slightly weathered rocks. The swelling characteristics of the altered rock present great challenges for support or lining during construction and operation stages. Support or lining shall be in place immediately after excavation. Since the rock may swell when encountering water, the shotcrete shall be designed accordingly. During the construction of access tunnel and caverns, water shall be drained in time. Drainage directly from surface shall be avoided so as to prevent floor heave. 相似文献