全文获取类型
收费全文 | 4463篇 |
免费 | 145篇 |
国内免费 | 166篇 |
专业分类
电工技术 | 11篇 |
综合类 | 212篇 |
化学工业 | 1499篇 |
金属工艺 | 25篇 |
机械仪表 | 135篇 |
建筑科学 | 84篇 |
矿业工程 | 16篇 |
能源动力 | 756篇 |
轻工业 | 24篇 |
石油天然气 | 1736篇 |
武器工业 | 22篇 |
无线电 | 27篇 |
一般工业技术 | 130篇 |
冶金工业 | 25篇 |
原子能技术 | 15篇 |
自动化技术 | 57篇 |
出版年
2024年 | 4篇 |
2023年 | 40篇 |
2022年 | 72篇 |
2021年 | 104篇 |
2020年 | 125篇 |
2019年 | 121篇 |
2018年 | 97篇 |
2017年 | 98篇 |
2016年 | 121篇 |
2015年 | 116篇 |
2014年 | 226篇 |
2013年 | 242篇 |
2012年 | 239篇 |
2011年 | 376篇 |
2010年 | 291篇 |
2009年 | 249篇 |
2008年 | 191篇 |
2007年 | 268篇 |
2006年 | 277篇 |
2005年 | 251篇 |
2004年 | 251篇 |
2003年 | 247篇 |
2002年 | 198篇 |
2001年 | 140篇 |
2000年 | 101篇 |
1999年 | 101篇 |
1998年 | 55篇 |
1997年 | 42篇 |
1996年 | 35篇 |
1995年 | 33篇 |
1994年 | 17篇 |
1993年 | 12篇 |
1992年 | 11篇 |
1991年 | 5篇 |
1990年 | 1篇 |
1989年 | 4篇 |
1988年 | 2篇 |
1987年 | 1篇 |
1986年 | 1篇 |
1985年 | 2篇 |
1984年 | 1篇 |
1983年 | 2篇 |
1982年 | 2篇 |
1980年 | 1篇 |
1944年 | 1篇 |
排序方式: 共有4774条查询结果,搜索用时 15 毫秒
61.
62.
Hale Sutcu 《Korean Journal of Chemical Engineering》2007,24(5):736-741
Pyrolysis of peat obtained from Yeniça?a, Bolu, Turkey was conducted in a fixed-bed tube furnace under various conditions, and variations in the structure of the char, tar and gas products were examined. The chars produced were studied by proximate and ultimate analyses. The maximum tar yield of 20.41% was obtained at a heating rate of 20 °C/min, a temperature of 450 °C, a sweeping gas flow rate of 100 ml/min and a 0.5–2.0 mm size range. The chemical composition of the tar was examined by elemental analysis, FTIR spectroscopy, 1H-NMR spectroscopy and column chromatography. The chemical composition of the tar with dense aliphatic structure was established to be CH1.22O0.25N0.02. The composition of the gases obtained at a heating rate of 20 °C/min for the 0.5–2.0 mm size range was examined by gas chromatography. 相似文献
63.
64.
A fabrication process has been developed to create suspended carbon microelectromechanical system (C-MEMS) structures. SU-8, a negative photoresist, was used as the starting material and was converted to the desired carbon microstructures using pyrolysis in an inert atmosphere. Suspended carbon-micro and nano electromechanical system (C-MEMS/NEMS) structures with feature sizes down to 500 nm were fabricated by ultra violet/electron beam (EB) lithography and pyrolysis. The problem of charging of the non-conductive SU-8 surface was solved by partially masking a thin metal layer to prevent the repulsion of negative charged electrons before EB writing. Complex suspended C-MEMS structures, such as bridges and networks have been formed. This fabrication method can accurately and reproducibly produce various suspended C-MEMS structures which have applications in microelectronics and biosensing. 相似文献
65.
CIP-1型裂解催化剂的研究 总被引:2,自引:0,他引:2
CIP-1裂解催化剂是一种多组元分子筛催化剂, 适用于催化裂解Ⅱ型工艺(DCC-Ⅱ)。该催化剂具有在生产高辛烷值汽油的同时多产丙烯及低碳异构烯烃的特点工业应用表明, 在反应温度505℃ 下汽油、丙烯、异丁烯和异戊烯的产率分别为40.98、12.52、4.57和5.78wt%, 在反应温度530℃下分别为38.45、14.43、4.75和5.93wt%. 相似文献
66.
Carbon-encapsulated Fe nanoparticles with size between 5 and 20 nm were synthesized via a picric acid-detonation-induced pyrolysis of ferrocene, which is characterized by a self-heating and extremely fast process. The nanoparticles exhibit well-constructed core-shell structures, with bcc-Fe cores and graphitic shells. The graphitic shells can protect effectively the cores against the attack of HNO3 solution. The formation of the core-shell nanoparticles can be selectively controlled by adjusting the composition of the picric acid-ferrocene mixture, which determines C/Fe atomic ratio of the reaction system. The core-shell nanoparticles are preferably formed at low C/Fe atomic ratios, while tubular structures are formed at high C/Fe ratio. The possible pathway for the carbon-encapsulated Fe nanoparticles formation is discussed briefly. 相似文献
67.
68.
Hyun-Seob?Song Joo?Sung?Lee Jae?Chun?HyunEmail author 《Korean Journal of Chemical Engineering》2002,19(6):949-953
A mathematical model for the pyrolysis reaction of polystyrene (PS) in a semi-batch reactor has been presented. The thermal
degradation of PS was flexibly modeled by a combination of random and specific chain-end scissions. Numerical simulation was
used to investigate the effect of operating conditions on the PS products spectrum, the results of which were validated by
the experimental data. It was found that as the reaction temperature increased (decreased), the monomer fraction in the products
became lower (higher) while the trimer higher (lower). No significant variation in the product composition was, however, observed
while constant temperature was maintained. These results indicate the reaction temperature is an effective manipulated variable
for the control of products composition of PS pyrolysis. The calculation of the optimum temperature trajectories through the
optimization study can thus be of interest for achieving productivity enhancement in plastics pyrolysis processes.
This paper is dedicated to Professor Dong Sup Doh on the occasion of his retirement from Korea University. 相似文献
69.
PAR分光光度法测定汽油中的痕量铅 总被引:6,自引:0,他引:6
研究了快速测定汽油中痕量铅的方法。测定经盐酸处理过的汽油与 PAR反应生成的络合物。该显色体系最大的优点是可在水相中直接用光度法测定样品中铅的含量。该配合物最大的吸收波长为 5 2 0 nm,ε52 0 =2 .2× 10 4 L· (m ol· cm ) - 1 ,Pb浓度在 0~ 2 5 .2μg· m L- 1 范围内线性关系良好 ,回归方程 A=0 .12 711C- 0 .0 6 2 93,相关系数为 0 .9992 ,检出限为 0 .4 1μg· m L- 1 。本方法显色迅速 ,稳定 ,操作简便 ,避免了使用氰化钾剧毒试剂 ,以及萃取等烦琐操作 ,可在 35 min内完成 1次测定 相似文献
70.