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91.
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93.
Solubility of dimethyl-2,6-naphthalene dicarboxylate in acetic acid, N,N-dimethylfonnamide, N,N-dimethyl acetamide, dimethyl sulphoxide, and N-methyl-2-ketopyrrolidine were determined using a dynamic method. The measured systems were correlated by UNIFAC group contribution method. A new main group (aromatic ester, ACCOO) was defined to express the activity coefficients of the aromatic ester. New interaction parameters of the ACCOO group were expressed as the first-order function of temperature and were determined from the experimental data. The calculated results for the new interaction parameters were satisfactory. The measured systems were also correlated with the Wilson and 2-h models, and the results were compared with those of the UNIFAC model. 相似文献
94.
Reda Karoum Antonio de Lucas-Consuegra Fernando Dorado Jose Luis Valverde Alain Billard Philippe Vernoux 《Journal of Applied Electrochemistry》2008,38(8):1083-1088
The electrochemical promotion of catalysis (EPOC) of propene combustion was investigated using Pt sputtered thin film on an
O2− conductor, 8 mol% Y2O3-stabilized-ZrO2 (YSZ). In order to separate the influence of the thermal migration of the O2− oxide ions from the electrolyte to the catalyst surface and the impact of an electrical polarization on the catalytic activity,
several light-off experiments (cool down and heat up procedures) were successively performed under different polarizations,
i.e. OCV, +2 and −2 V. These experiments have clearly shown that the presence of O2− (thermally or electrochemically induced) inhibits the catalytic activity of the platinum for the propene deep oxidation.
These results demonstrate the importance to define a normalized rate enhancement ratio, ρ
n
, from a reference value of the catalytic rate corresponding to a Pt surface state free of O2− ions. 相似文献
95.
(Department of Automation & Computer Baotou Iron &Steel Instetute Baotou PRC) Wang ZhichunLi Wentao(Department of Net work Baotou Filiale of Inner MongoliaMobile Corporation Baotou PRC)Yang Zhanping 《微计算机信息》2003,19(5):45-45
This paper introduces hardware connections between computer and intellectualized instrument based on 89c51 sin-glechip .It gives the techniques to compile internet applications of Virtual Instruments with Delphi6. 相似文献
96.
Study of the effective parameters on mechanical and electrical properties of carbon black filled PP/PA6 microfibrillar composites 总被引:1,自引:0,他引:1
In this study the electrical and mechanical properties of microfibrillar polypropylene (PP)/polyamide6 (PA6) blend filled with super conductive carbon black (CB) have been investigated. In situ microfibrillar PP/PA6 composites filled with CB are produced using a single screw extruder equipped with a spinneret. Glycidyl methacrylate (GMA) grafted polypropylene (PP-g-GMA) is used as the compatibilizer. To investigate the effects of extensional flow on the microstructure, electrical and mechanical properties, three adaptors with various convergence angles were designed, prepared and applied between the extruder and the spinneret. To optimize the effects of processing and material parameters on the electrical and mechanical properties, the Taguchi method of experimental design is used. Material and processing factors which are studied include: concentration of PA6, compatibilizer level, CB concentration, drawing speed of melt spinning line, adaptor angle, order of mixing and temperature profile along the extruder. The results show an increase in DC conductivity of up to 1011 times in comparison with pure PA6, by increasing the concentration of CB, drawing speed, adaptor angle and optimizing other parameters. By optimizing processing and material factors studied here, strength of microfibrillar structured composites is increased of up to 80% in comparison to pure PP. 相似文献
97.
Polyamide (PA6) and polycarbonate (PC) were prepared by a Brabender mixer ( PLV- 151) at 240℃ with 30 rpm for duration of 8 and 6 minutes respectively. The epoxy resin (E) addition can lead to substantial microstructural changes in the PA6/PC blends. Scanning electron microscope (SEM) was used to observe the mixtures characterized by the domains of clearly segregated homophases and voids between the two polymers. PA6/PC of polyamide 6 and polycarbonate with epoxy resin addition under the composition ratio of 20/80, 20/80/1, 40/60/1 and 40/60, were tested to verify the key role of epoxy in promoting the compatibility of PA6 with PC during blending. 相似文献
98.
99.
一类三元线性分组码的译码 总被引:1,自引:0,他引:1
Pless[1]证明了三元(12,6,6)Golay码具有一种双层结构,并据此给出了该码的快速硬判决译码算法。本文推广了Golay码的Pless结构,给出了由三元(n,k,d)线性分组码构造的三元(3,n+k,≥min(n,2d,6))线性分组码,其中包括(12,6,6)Golay码和(18,9,6)码,并以三元(18,9,6)码为例给出了这类码的最大似然软判决译码算法。 相似文献
100.
用化学还原法制得了尼龙6表面金属(Ni)化膜材料。研究了还原条件,金属盐浓度对膜材料电性能的影响,以及膜材料的电发热性能,用光电子能谱和扫描电子显微镜对其表面及形貌进行了表征。 相似文献