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31.
The technique of analytical pyrolysis has been used to characterize 40 similar mid-rank western Kentucky coals of widely differing ASTM Gieseler plasticity. Certain pyrolysis/g.c. variables were shown to correlate well with both ASTM Gieseler and isothermal plasticity. Highly plastic coals were shown to exhibit certain characteristic peaks in the 450 °C pyrogram which were absent in the pyrogram of the non-plastic coals. Two coals, representing the two extremes in plasticity, were selected for further study. After extraction with solvents such as DMF the characteristic peaks were absent in the 450 °C pyrogram of the extraction residue of the highly plastic coal. These peaks were also shown to decrease with increasing severity of air oxidation of the plastic coal. This technique appears to be a useful tool for the analysis of mid-rank plastic coals and supports the view that the substances contained in the bitumen fraction of these coals are involved in the development of the plastic state. 相似文献
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Crack closure in fibre metal laminates 总被引:1,自引:0,他引:1
H.M. PLOKKER R.C. ALDERLIESTEN R. BENEDICTUS 《Fatigue & Fracture of Engineering Materials & Structures》2007,30(7):608-620
GLARE is a fibre metal laminate (FML) built up of alternating layers of S2-glass/FM94 prepreg and aluminium 2024-T3. The excellent fatigue behaviour of GLARE can be described with a recently published analytical prediction model. This model is based on linear elastic fracture mechanics and the assumption that a similar stress state in the aluminium layers of GLARE and monolithic aluminium result in the same crack growth behaviour. It therefore describes the crack growth with an effective stress intensity factor (SIF) range at the crack tip in the aluminium layers, including the effect of internal residual stress as result of curing and the stiffness differences between the individual layers. In that model, an empirical relation is used to calculate the effective SIF range, which had been determined without sufficiently investigating the effect of crack closure. This paper presents the research performed on crack closure in GLARE. It is assumed that crack closure in FMLs is determined by the actual stress cycles in the metal layers and that it can be described with the available relations for monolithic aluminium published in the literature. Fatigue crack growth experiments have been performed on GLARE specimens in which crack growth rates and crack opening stresses have been recorded. The prediction model incorporating the crack closure relation for aluminium 2024-T3 obtained from the literature has been validated with the test results. It is concluded that crack growth in GLARE can be correlated with the effective SIF range at the crack tip in the aluminium layers, if it is determined with the crack closure relation for aluminium 2024-T3 based on actual stresses in the aluminium layers. 相似文献
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WC对Cu/WC_P复合材料性能及组织的影响 总被引:8,自引:0,他引:8
通过WC含量对WC/Cu复合材料性能的影响,确定了冷压-烧结法制备Cu/WC材料的适宜WC含量为10vol%左右。并就WC对该材料组织和再结晶行为的影响进行了有益的探讨。 相似文献
37.
利用挤压铸造制备氧化铝/锌合金复合材料,在扫描电镜(SEM)上观察复合材料的界面。结果表明,在复合材料中纤维与基体间存在致密界面层,合金元素通过适当的化学反应可改善纤维与基体间的结合;在凝固过程中,纤维/基体界面上的硅在共晶体的共生生长过程中起了领先相作用,导致复合材料的共晶转变是由铝硅共晶转变和锌铝共晶转变两者组成。 相似文献
38.
On the suitability of agricultural by-products for the manufacture of granular activated carbon 总被引:1,自引:0,他引:1
An investigation of several agricultural by-products revealed that their suitability for activated carbon production is not determined by general material-specific features (elemental composition) but by type-specific features. A coarse-cellular structure (as in wood), which is indicated by porosities of the raw materials higher than 35% is disadvantageous. A specific change in the properties of cokes (porosity, density, hardness) is possible by varying the conditions of pyrolysis. By rapid heating in the pyrolysis step, for instance, macroporous residues are produced. Temperature and burnoff have the greatest influence on the quality of the activated carbon during the activation step. Of the investigated materials, coconut shells yield granular activated carbon of the highest quality. The following order of suitability of raw materials for activated carbon production was established: coconut shells> peach stones> plum stones> hazelnut shells> walnut shells> cherry stones. 相似文献
39.
单轴-平面W型复合锶铁氧体的制备及其吸波特性研究 总被引:3,自引:0,他引:3
用草酸盐共沉淀和微量掺杂法研制六角晶系W型Ni,Zn,Co,Al多元复合锶铁氧体,通过调节Ni2W同Co2W的摩尔比例,可使该种铁氧体易磁化方向从C单轴型向垂于C轴的平面型转化,控制置换锶铁氧体中部分Fe3 的微量掺杂Al3 ,可以调整4πMs值,提高磁晶各向异性场,测试分析了5种不同含Co量的W型复合锶铁氧体粉料涂层的吸波特性,发现其自然共振吸收峰随Co含量增加向低频方向偏移,最高吸收峰可达32.8dB,是适用于电子隐形技术的高品位的微波吸收剂。 相似文献
40.