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61.
62.
The time‐dependent rheological behavior of a series of 3‐hydroxybuytrate‐based semicrystalline copolymers is employed to determine the expected rheological curves that would be generated in the absence of any polymer degradation. Both dynamic frequency sweep and shear rate sweep experiments were analyzed. A model for the degradation kinetics, coupled with standard rheological relationships, was employed to extrapolate the measured sweeps to predicted curves at time zero, prior to degradation. The model is broadly applicable over a wide range of frequencies or shear rates, and generates a single degradation rate constant k for each polymer studied. A similar, although ad hoc, procedure was applied to the dynamic storage and loss moduli. The model provides a method for determining the rheological behavior of degrading polymers over a time interval, typically found in processing applications. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102:1794–1802, 2006 相似文献
63.
Man Sig Lee Gun-Dae Lee Chang-Sik Ju Seong-Soo Hong 《Solar Energy Materials & Solar Cells》2005,88(4):389-401
Nanosized titania sol has been produced by the controlled hydrolysis of titanium tetraisopropoxide (TTIP) in sodium bis(2-ethylhexyl)sulfosuccinate (AOT) reverse micelles. The physical properties, such as surface area, crystallite size and crystallinity according to R and W0 ratio, have been investigated by TEM, XRD, BET, FT–IR, TGA and DTA. In addition, the photocatalytic decomposition of p-nitrophenol has been studied by using a batch reactor in the presence of UV light in order to compare the photocatalytic activity of prepared nanosized titania. It is shown that the anatase structure appears in the 300–600 °C calcination temperature range and the transformation of anatase into rutile starts above 700 °C. The crystallite size increases with increasing R and W0 ratio but W0 ratio shows a stronger effect on the crystallite size than R ratio. In the photocatalytic decomposition of p-nitrophenol, the photocatalytic activity is mainly determined by the crystallinity of titania. In addition, the titania calcined at 500 °C shows the highest activity on the photocatalytic decomposition of p-nitrophenol() and the pure anatase structure. 相似文献
64.
Whey is an undurable product. treated very often as a waste which pollutes the natural environment. Whey which is a valuable source of protein, lactose, vitamins and mineral salts should be utilized completely. The present paper is a proposal of whey drying on porous carriers. It is proved experimentally that the proposed drying method guarantees good product quality. 相似文献
65.
66.
分析了两种常用监控在用发动机油氧化衰变情况的试验方法,并通过监控试验数据,探讨酸值和红外两种监测方法的各自特点,提出高档发动机油酸值变化极限值应区别于中低档发动机油的观点,为今后监控在用发动机油选用合适的试验方法和标准提供了参考。 相似文献
67.
Alkylated ureas: mineralization and evaluation as N sources 总被引:2,自引:0,他引:2
An incubation experiment was conducted for 11 weeks to study the mineralization of ten alkylated ureas and urea in soil. Six of the alkylated ureas viz. methylurea(MU), 1,3-dimethylurea(1,3DMU), 1,1-dimethylurea(1,1DMU), ethylurea(EU), 1,3-diethylurea(1,3DEU) and butylurea(BU) and urea mineralized during the experiment. Urea mineralized immediately, while alkylated ureas mineralized after an incubation period ranging from less than a week to four weeks (delay period of mineralization). The delay period increased in the following sequence MU < 1,3DMU < EU < BU < 1,1DMU < 1,3DEU, but after the delay period was over the compounds mineralized almost as rapidly as urea. The delay period varied according to the number of carbon atoms in the alkyl group and their position with respect to each other on the molecule. It appeared to be specific for each compound and was apparently not influenced by the presence of urea or other alkylated ureas. This character can be used to develop mixture of various alkylated ureas to obtain N mineralization at the desired time. Rapid evolution of CO2 and N2O was observed during the mineralization of urea as well as alkylated ureas. Increase in soil pH was also observed during this period. The simultaneous ocurrence of these events suggested the formation of urea as an intermediate during the mieralization of alkylated ureas. None of the alkylated ureas showed adverse affect on emergence of wheat seedlings and except DEU and BU at high concentration no other alkylated urea showed any adverse effect on initial growth of wheat seedlings. 相似文献
68.
The remaining useful life (RUL) prediction of a rolling element bearing is important for more reasonable maintenance of machinery and equipment. Generally, the information of a failure can hardly be acquired in advance while running and the degradation process varies in terms of different faults. Thus, fault identification is indispensable for a multi-condition RUL prediction, where, however, the fault identification and RUL prediction are separated in most studies. A new hybrid scheme is proposed in this paper for the multi-condition RUL prediction of rolling element bearings. The proposed scheme contains both classification and regression, where the 2D-DCNN based classifier and predictors are built concerning typical fault conditions of a bearing. For the online prediction, the raw signals are spanned in the time-frequency domain and then transferred into images as the input of the scheme. The classifier is used to monitor the vibration of rolling bearings for online fault recognition and excite the corresponding predictor for RUL prediction once a fault is detected. The output from the predictor is amended by the proposed adaptive delay correction method as the final prediction results. A demonstration is performed based on the XJTU-SY datasets and the results are compared with those from the state-of-the-art methods, which proves the superiority of the proposed scheme in improving the accuracy and linearity of RUL prediction. The time cost of the proposed online prediction scheme is also investigated and the results indicate high time effectiveness. 相似文献
69.
70.
传统的静电纺丝法使用单一的毛细管状喷头喷丝,通常用于制备实心且表面光滑单一组分的纳米纤维,无法得到具有多种功能性结构的复合材料,应用范围较窄。以酞酸丁酯和尿素为原料,采用同轴静电纺丝法成功制备了TiO2/g-C3N4复合材料,并用X射线衍射(XRD)、傅里叶变换红外光谱(FTIR)、紫外可见漫反射光谱(UV-vis DRS)、场发射扫描电子显微镜(SEM)和Brunauer-Emmett-Teller (BET)分析对样品进行了表征,通过光催化降解亚甲基蓝溶液(MB)研究了不同g-C3N4添加量对TiO2/g-C3N4复合材料光催化性能的影响。实验结果表明,采用同轴静电纺丝法结合500℃煅烧工艺成功制备了大比表面积及高光催化性能的TiO2/g-C3N4复合材料。当g-C3N4添加量为0.15 g时,TiO2/g-C3N4复合材料对亚甲基蓝溶液(MB)的光催化降解效率可达93.8%,且经过5次重复实验后降解率仍可达80%以上。 相似文献