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91.
92.
K HondaM Yoshimura R UchikadoT Kondo Tata N Rao D.A TrykA Fujishima M WatanabeK Yasui H Masuda 《Electrochimica acta》2002,47(27):4373-4385
Electrochemical characteristics for several redox systems at diamond films with highly ordered nanometer-scale cylindrical pores (‘nano-honeycombs’) were examined with cyclic voltammetry (CV) and electrochemical impedance measurements. The cyclic voltammetric anodic-cathodic peak separations for these nano-honeycomb electrodes were in the same range as those for polished polycrystalline diamond films, indicating that the involvement of the oxygen-terminated surface of the nano-pore walls, which should give rise to large peak separations for certain redox couples was only slight. Moreover, the peak currents in the CV were not enhanced to the extent expected on the basis of the roughness factors of the nano-honeycomb films. Ac impedance plots results indicated the existence of a concentration gradient of the reactant in the nano-pores, which is in agreement with theoretical predictions for charge transfer reactions in porous electrodes. The average concentration of the reactant (Fe2+/3+) inside the nano-pores was a factor of ca. 80 lower than that in the bulk electrolyte. The results of the impedance analysis also indicated an increase in the reaction resistances with decreasing pore diameters. 相似文献
93.
94.
大化肥煤代油CO耐硫变换工艺流程的设计 总被引:2,自引:0,他引:2
分析石脑油制氨装置改扩建为水煤浆制氨装置CO耐硫变换工艺的特点,具体阐述其工艺流程优化设计中需考虑的主要技术问题。 相似文献
95.
96.
Human tracking has been a challenging task for robot in the past decades. In this paper, to realize the human following in a cluttered environment, a human tracking system based on adaptive multi-feature mean-shift (AMF-MS) under the double-layer locating mechanism (DLLM) is proposed to solve the problem of distinguishing target, occlusion, and quick turning. The DLLM, considering the course location processing and fine location processing, is designed to estimate the person’s position using the fusion of heterogeneous data. As an ID tag attached on target can be detected by RF antennas, the course locating method can track the target easily and quickly. The Bayes rule is introduced to calculate the probability where the tag exists due to the instability of RF signals. In the fine locating step, the AMF-MS is proposed because it can reduce computational load and represent target by multi-feature histogram function. Meanwhile, we combine extended Kalman filter and AMF-MS to overcome MS’s inability of occlusion. To control the robot following the target person precisely, an intelligent gear shift strategy based on fuzzy control is implemented by analyzing the robot structure. Experiments demonstrate that the proposed approach is robust to handle complex tracking conditions, and show the system has an optimum performance. 相似文献
97.
高小红 《计算机与应用化学》2014,(9):1119-1121
利用热力学基础数据和相关软件对Co-Mo-K催化剂上COS、HCN加氢和水解反应进行了热力学计算。在热力学上,COS、HCN加氢和水解反应在耐硫变换条件下均为自发过程。计算结果表明在Co-Mo-K耐硫变换条件下COS、HCN主要发生的是水解反应,该结果与工业经验数据基本一致,可以作为工业实际借鉴。 相似文献
98.
为实时提取三维实体表面,提出一种基于GPGPU并行计算的实体表面实时提取方法。在分析深度剥离算法原理和GPU图形绘制管线的基础上,给出在GPU上利用深度剥离算法实现实时提取三维实体表面的算法;通过OpenGL的高级着色语言GLSL控制GPU的图形绘制管线实现了该算法,给出其伪代码。以龙、叶轮和刀具扫描体的模型为应用实例验证了该算法效果良好,特别是对于刀具扫描体表面的提取,可满足实时性要求。 相似文献
99.
George G. Olympiou Christos M. Kalamaras Constantinos D. Zeinalipour-Yazdi Angelos M. Efstathiou 《Catalysis Today》2007,127(1-4):304-318
Steady-state isotopic transient kinetic analysis (SSITKA) experiments coupled with mass spectrometry were performed for the first time to study essential mechanistic aspects of the water–gas shift (WGS) reaction over alumina-supported Pt, Pd, and Rh catalysts. In particular, the concentrations (μmol g−1) of active intermediate species found in the carbon-path from CO to the CO2 product gas (use of 13CO), and in the hydrogen-path from H2O to the H2 product gas (use of D2O) of the reaction mechanism were determined. It was found that by increasing the reaction temperature from 350 to 500 °C the concentration of active species in both the carbon-path and hydrogen-path increased significantly. Based on the large concentration of active species present in the hydrogen-path (OH/H located on the alumina support), the latter being larger than six equivalent monolayers based on the exposed noble metal surface area (θ > 6.0), the small concentration of OH groups along the periphery of metal-support interface, and the significantly smaller concentration (μmol g−1) of active species present in the carbon-path (adsorbed CO on the noble metal and COOH species on the alumina support and/or the metal-support interface), it might be suggested that diffusion of OH/H species on the alumina support towards catalytic sites present in the hydrogen-path of reaction mechanism might be considered as a slow reaction step. The formation of labile OH/H species is the result of dissociative chemisorption of water on the alumina support, where the role of noble metal is to activate the CO chemisorption and likely to promote formate decomposition into CO2 and H2 products. It was found that there is a good correlation between the surface concentration and binding energy of CO on the noble metal (Pt, Pd or Rh) with the activity of alumina-supported noble metal towards the WGS reaction. 相似文献
100.
高温变换催化剂制备条件的神经网络优化 总被引:4,自引:0,他引:4
将影响低汽气比条件下LB型节能高温变换催化剂活性的主要因素作为人工神经网络的特征输入向量,将全部实验数据分为训练集和预测集,运用Matlab神经网络工具箱,按改进的Bayes自动归一化算法建立反向传播神经网络模型,不仅可防止网络陷入局部最小,而且提高了网络训练精度和泛化能力。适当拓宽正交实验各因素的水平范围,经过不同因素、不同水平间的组合模拟,预测出LB型节能高温变换催化剂的最佳制备条件为氧化铈质量分数0.76%、氧化铜质量分数5.8%、氧化铬质量分数8.6%、氧化镧质量分数1.0%、铁液浓度92 g/L、中和过程最终pH值9.5。在最佳条件下试制催化剂在低汽气比下的平均活性达77.6%。 相似文献