某钛合金零件疲劳断裂影响因素分析

对振动疲劳试验后的一批某钛合金零件进行了荧光、表面加工质量、前后缘部位细根圆角检查.通过进一步的显微组织检查,显微硬度测定,以及裂纹断口的宏观形貌观察和部分断口的微观形貌观察发现,在应力给定的情况下,影响该批零件低寿命的主要因素是显微组织和细根圆角程度;提高金相组织等级可明显提高零件的疲劳性能,零件前缘R〈60μm的细根将明显降低零件的疲劳性能;硬度以（HVB0.2B）〉370为宜;加工痕迹的方向分布对寿命的影响比较小,其主要影响裂纹萌生的位置.     

Analysis of Microstructure and Mechanical Properties of Different Hot Stamped B‐bearing Steels

Hot stamping is a technique to produce ultra high strength automobile components. The common material used in hot stamping process is coated and/or uncoated 22MnB5 boron alloyed steel. Ferritic‐pearlitic microstructure in as‐delivered sheets is transformed to fully lath martensitic after hot stamping. In the present research, hot stamping under water or nitrogen cooling media was investigated using different boron alloyed steel grades. Microstructural analyses, linear and surface hardness profiling as well as tensile tests of hot stamped samples were performed. Various microstructures of fully bainitic and/or fully martensitic were produced. The resulting microstructures provided yield strengths of 650–1370 MPa and tensile strengths of 850–2000 MPa. There is an optimum carbon equivalent content for which the highest formability index value, UTS × A₂₅, is achieved. Using a nitrogen cooled punch resulted in higher yield strength without significant changes in ultimate tensile strength. It is concluded that a wide range of B‐bearing steels having an extended carbon equivalent range with an acceptable formability index value can be used by increasing the cooling rate in the die assembly.     

零保温奥氏体逆相变淬火温度对40Cr钢组织性能的影响

采用正交组合回归设计试验方法,研究了零保温奥氏体逆相变淬火温度对40Cr钢强度、硬度的影响,分析了其组织特征。实验表明,40Cr钢840～920 ℃零保温奥氏体逆相变淬火,可以细化奥氏体晶粒,得到细小的板条状马氏体组织。淬火温度较低时,马氏体板条间分布少量条状铁素体,随淬火温度提高铁素体逐步减少,880 ℃淬火得到全部板条状马氏体组织。在实验温度范围内,900 ℃+880 ℃两次淬火后40Cr钢的强度、硬度最高,其力学性能显著好于常规的880 ℃一次淬火。     

L360QS/316L不锈钢复合钢管焊接工艺和性能研究

介绍了?准355.6 mm×(10+3) mm规格L360QS+316L不锈钢复合钢管的新型焊接工艺,即首先采用TIG焊在复合钢管管端进行堆焊预处理,然后再采用氩气保护TIG焊进行对焊操作。为评价环焊缝的性能,焊后对其焊接接头进行了拉伸试验、冲击试验、硬度测试、晶间腐蚀及应力腐蚀试验。试验结果表明,采用该工艺焊接的L360QS+316L不锈钢复合钢管环焊缝焊接接头性能良好,且具备耐晶间腐蚀和应力腐蚀性能;堆焊层起到了很好的隔离作用,保证了焊缝的质量。     

高韧性钢Q345LCLA焊接工艺研究

为匹配室温冲击吸收功高达237 J的低碳低合金高韧性钢Q345LCLA,选择国产焊接材料H10Mn2/SJ101和进口焊接材料Primerweld Ni1K/JF-B分别进行焊接工艺评定。对2种焊接接头进行室温拉伸和侧弯试验,并对焊缝及热影响区在室温,0 ℃,-20 ℃和-40 ℃温度条件下进行冲击试验,同时进行硬度检测及金相组织分析。结果表明,2种焊接材料均具有良好的焊接性,强度、塑性均达到AWSD1.1—2010标准要求,且具有较好的低温及常温冲击韧性,相对而言,Primerweld Ni1K/JF-B的冲击吸收功稍高;2种焊接材料金相组织比较接近,未出现晶粒粗大的魏氏组织及脆硬的马氏体组织,具有良好的金相组织。     

塑胶用高硬度高光泽热塑性丙烯酸树脂的研究

本实验解决了热塑性丙烯酸树脂高光泽、高硬度、高抗刮性能、高颜料分散性不能平衡的问题。讨论了分散介质、反应单体、玻璃化转变温度、油改性醇酸树脂、反应温度和时间、固体含量等对树脂性能的影响。以该方法制备的热塑性丙烯酸树脂各项综合性能优异。     

采用多向压缩制备超细晶纯铝的研究

采用多向压缩技术成功制备了最终晶粒尺寸为2 μm的超细晶纯铝。对不同应变量下材料的微观结构表征发现,变形过程中的晶粒细化机制主要是变形带细化和位错分割细化; 由于变形导致材料温度升高,材料的晶粒细化也与再结晶有关系。硬度测试表明,随着应变量增加,材料硬度先增加后减小,等效应变为1.4时,材料硬度达到了最大值46.3HV。材料硬度的升高主要与位错增殖及缠结有关,硬度值的降低与位错密度降低、压缩过程中材料的动态回复有关。     

A study of microstructural analysis for nondestructive evaluation of thermal annealing using magnetic properties

Two kinds of thermally aged Fe-Cu alloys with different Cu proportions 0.05% and 0.45% were prepared and their magnetic properties were investigated to apply magnetic nondestructive testing techniques for the assessment of irradiation embrittlement of materials. Initially, the alloy is 10% cold rolled and then isothermally aged at 500 °C and 400 °C with different aging time up to 1000 h in order to create Cu-precipitates in the Fe metal matrix. The hysteresis loop (HL), Barkhausen noise (BN) and Magnetic Adaptive Testing (MAT) parameter were measured for magnetic properties studies and mechanical properties were investigated by Vickers hardness. The HL, BN were decreased and the MAT parameter was increased by thermal aging. The changes of these parameters were explained by copper rich precipitations (CRPs) formation, interaction with domain walls and dislocation movement pinned by CRPs. It was confirmed by TEM and EDX analysis.