多孔粒状铵油炸药在边坡预裂爆破中的应用

通过工程实践，介绍了利用多孔粒状铵油炸药进行边坡预裂爆破的设计原理及施工工艺。该技术能确保预裂爆破质量。简化施工工序，大幅度降低爆破成本。技术经济指标优越。     

高放废液中^147Pm的测定

建立了高放废液中~(147)Pm的测定方法。用HDEHP萃取稀土,再用HDEHP萃淋树脂柱分离AM和稀土。然后用高效液相色谱法将~(147)Pm从Eu、Ce等其它稀土中分离出来,用液体闪烁法测量~(147)Pm的放射性活度。     

Extraction of penicillin G from simulated media by an emulsion liquid membrane process

The extraction of penicillin G from simulated media was performed by water/oil/water (w/o/w) emulsion liquid membranes (ELMs) and studied under various operational conditions in a batch system. The degree of extraction achieved was between 80% and 95% under specific conditions. A concentration of greater than nine times the initial concentration of penicillin G in the external phase was obtained in the internal phase. The pH of the internal aqueous solution, containing a basic salt, was theoretically calculated on the basis of the amount of penicillin G transported into the internal phase. The calculated results agreed with the experimental data well and were used to select a suitable type and concentration of a basic salt in the internal phase to give a pH within the range 5 to 8 where penicillin G was stable after the termination of extraction. The extraction of penicillin G was successfully performed by the ELM process with sodium carbonate in the internal phase.     

On the permeation rate of copper extraction through liquid membranes

The understanding of the permeation rate of metal ions through liquid membranes is important for the design of such systems. In this paper, the permeation rates of copper ions through liquid surfactant membranes, including interfacial reaction rates and the diffusion rate of the copper ion, were analyzed using a model based on a mobilized hollow spherical globule configuration. The analysis shows that the extracting reaction is dominant at the external interface of the membrane and the stripping reaction is dominant at the internal interface; this means the reactions at both interfaces are not in equilibrium during the course of extraction. It also shows that the extraction rate, the diffusion rate and the stripping rate are not of equal value, especially at the early stage of the run.     

Liquid–liquid extraction of a recombinant protein with reverse micelles

Recombinant cytochrome b₅ was extracted into the reversed micelle phase of an anionic surfactant (AOT) in octane and back-extracted to a final aqueous phase. The extraction of the protein was controlled by an electrostatic mechanism, since it was dependent on the global charge of the protein. This was directly demonstrated by experiments with native and mutant cytochromes obtained by site directed mutagenesis. The back-extraction of cytochrome b₅ to a fresh aqueous phase was decreased by factors that reduced the size of the water pool of the organic phase, such as high salt concentrations (1–2 mol dm^?3 NaCl) and low temperatures (4°C), probably because of an increase in a favourable interaction of this protein with the surfactant at closer distances.     

The Problem of Estimating the Uncertainty of the Fixed Point Temperature Due to the Presence of Impurities

The main problems in estimating the uncertainty due to the presence of impurities in the material: the absence in the documents of a unique definition of the quantity being measured – the fixed point temperature, the lack of agreed methods of realizing the fixed points and the insufficient justification of the equations used for the estimate, are analyzed. The results of a measurement of the melting point of gallium are presented, which differ in the conditions in which they were realized – with one and two liquid-solid interfaces and different solidification conditions, are presented. The reasons for the considerable difference between the values of the temperatures obtained in these experiments are discussed.     

Procedure for the evaluation of the accumulation of defects in metallic structural materials under complex elastoplastic loading

Within framework of the continual fracture mechanics, we describe the engineering approach to the assessment of scattered microdamage accumulation kinetics in metallic materials under elastoplastic loading conditions in case of plane stressed state. Automatized experimental stand and the respective investigation technique are discussed. The stand has been developed based on modification of the UMé-10T electromechanic test machine. State-of-the-art computer technologies and microprocessing hardware are incorporated in the stand automation. We present the technique of experimental assessment of damage accumulation kinetics in metallic structural materials under complex elastoplastic loading conditions with account of two different fracture (cleavage and shear) processes, which technique is based on measuring the specific electric resistance of the specimen. __________ Translated from Problemy Prochnosti, No. 1, pp. 128–137, January–February, 2006.     

Effects of weak shear on hyperswollen lyotropic smectic liquid crystals

We have developed a Zimm-type viscometer specially designed for the simultaneous measurements of the structure factor and the viscosity of hyperswollen lyotropic liquid crystals under a very weak shear. We have investigated the shear effects on the layer undulation fluctuation in the lamellar structure and the transition from the anisotropic lamellar to the isotropic sponge phase. We have found a significant difference in the rheological properties between the lamellar and the sponge phase: The former exhibits non-Newtonian flow behavior, while the latter exhibits Newtonian behavior.Paper presented at the Twelfth Symposium on Thermophysical Properties, June 19–24, 1994, Boulder, Colorado, U.S.A.     

Flow stress of high density polyethylene and nylon 66 at high rates of strain

Measurement of the flow stress of high density polyethylene (HDPE) and nylon 66 at strain rates of 10³ s^?1 using a split Hopkinson pressure bar technique is discussed. The flow stress at a strain of 10% has been determined for both polymers at 20°C. The intrinsic errors involved in this technique are briefly reviewed. The results indicate that the flow stress of HDPE and nylon 66 were 50MPa and 150MPa, respectively, at strain rates of about 10³s^?1.