大型钢制焊接双层低温储罐设计建造

介绍了大型钢制焊接双层低温储罐的结构形式、选材、建造、检验及保冷要求 ,结合所设计的低温液氨储罐 ,对设计建造这类储罐必须考虑的一些问题作了分析     

Ti基MnO_x型DSA析氧电极材料的性能

本文报导了新型 Ti/SnO_2+MnO_x+RuO_2/MnO_x(DSA)电极材料的各种性能,其中包括电极的导电性、表面粗糙度、电化学活性表面积、析氧阳极特性等,并用 X 射线衍射法进行了物相分析、用 SEM观察了表面形貌。确认该电极性能良好,加之成本较低,可作为酸性介质中的析氧电极材料。     

Structure and Magnetic Properties of LaCo_(13-X)M_X Intermetallic Compounds

ＳｔｒｕｃｔｕｒｅａｎｄＭａｇｎｅｔｉｃＰｒｏｐｅｒｔｉｅｓｏｆＬａＣｏ＿（１３－Ｘ）Ｍ＿ＸＩｎｔｅｒｍｅｔａｌｌｉｃＣｏｍｐｏｕｎｄｓＷＵＪｉａｎＭｉｎ；ＬＩＦｅｎｇ；ＴＡＩＬｉＣｈｉａｎｄＺＨＥＭＧＱｕｎＳｔｒｕｃｔｕｒｅａｎｄＭａｇｎｅｔｉｃＰ...     

准分子激光的应用

本文介绍了准分子激光器的基本类型、主要应用领域及其与材料相互作用的机理。对准分子激光在电子工业、生物医学和材料加工方面的一些重要应用做了比较详细的论述。     

攀钢高炉焖砂口试验

分析了高炉冶练钒钛磁铁矿炉前砂口损坏的原因。对新型砂口泥进研制，同时改进了套砂口工艺，满足了攀钢高炉焖砂口的需要。攀钢高炉采用闷砂口工艺后，从根本上解决了铁水带渣问题，提高了铁水的洁净度。     

结构振动控制中压电阻尼技术研究—压电被动阻尼技术（一）

压电阻尼技术有两种类型：压电被动阻尼技术和压电主动阻尼技术。本文对其中的压电被动阻尼技术进行了研究，结果表明：通过给压电元件并联适当的外部电路，可使压电系统具有与粘弹阻尼材料及动力吸振器相似的物理特性。合理配置电路参数，可以实现最优阻尼比。     

对我国酱油酿造几项新技术应用之浅见

本文概述了三十年来我国酿造酱油工业开展研究的六项新技术在现阶段的投产可行性，及进一步研究方向的看法。     

Application of SiC-Si functionally gradient material to thermoelectric energy conversion device

Because of its high–temperature chemical stability, SiC ceramic is a promising material for high-temperature device applications such as thermoelectric energy converters. However, the electrical conductivity of SiC ceramic is too low for it to be used as a thermoelectric energy converter at the cold junction. Therefore, we propose a SiC-Si functionally gradient material (FGM) in order to improve the electrical conductivity of the SiC ceramic at the cold junction. An SiC rod was fired in a temperature gradient furnace. One end of the SiC rod was maintained at 2473 K and the other end was maintained at 1973 K for 30 min. After firing, the porous SiC edge fired at 1973 K was dipped into molten Si in order to infiltrate molten Si into the porous SiC. The microstructure of the FGM is classified into three regions: the SiC-Si composite material; the porous SiC ceramic; and the densified SiC ceramic. The electrical conductivity, the Seebeck coefficient and the thermal conductivity for each region of SiC-Si FGM was measured at 300 K; a figure of merit was calculated. The figure of merit of the SiC-Si FGM at the cold junction, at room temperature, was 10⁸ times higher than that of a nongradient SiC ceramic.     

学习新版建筑工程施工质量验收规范的体会

结合新版建筑工程施工质量验收规范的学习和施工实践 ,介绍了新版标准与旧标准的差异和特点 ,并就如何贯彻实施新标准、准确掌握检验批等问题作了分析 ,提出了执行中的相关注意事项。     

Preparation and characterization of polyurethane microcapsules containing n‐octadecane with styrene‐maleic anhydride as a surfactant by interfacial polycondensation

A series of polyurethane microcapsules containing a phase change material (PCM) of n‐octadecane was successfully synthesized by an interfacial polymerization in aqueous styrene‐maleic anhydride (SMA) dispersion with diethylene triamine (DETA) as a chain extender reacting with toluene‐2,4‐diisocyanate (TDI). The average diameter of microPCMs is in the range of 5–10 μm under the stirring speed of 3000–4000 rpm. Optical and SEM morphologies of microPCMs had ensured that the shell was regularly fabricated with the influence of SMA. FTIR results confirmed that the shell material was polyurethane and the SMA chains associated on core material reacted with TDI forming a part of shell material. The shell thickness was decreasing in the range of 0.31–0.55 μm with the molar ratio of DETA/TDI from 0.84 to 1.35 and the weight of core material increasing from 40 to 80% (wt %). By controlling the weight ratio of PCM as 40, 50, 60, 70, and 80% in microPCMs, it was found using DSC that the T_m and T_c of microPCMs were in the range of 29.8–31.0^oC and 21.1–22.0°C and an obvious phase change had been achieved nearly the same temperature range of that of PCM. The results from release curves of microPCM samples prepared by 1.4, 1.7, and 2.0 g of SMA indicated the release properties were affected by the amount of the dispersant, which attributed to the emulsion effect and shell polymerization structure. The above results suggest that the shell structure of microPCMs can be controlled and the properties of microPCMs determined by shell will perform proper practical usage. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 4996–5006, 2006