Anodic dissolution of spongy titanium in ethanol solution for preparation of nano-sized TiO2 powder

Nano-sized TiO₂ powder was prepared by electrochemical dissolution of spongy titanium in an ethanol solution following direct hydrolysis of the electrolyte solution. Characterization of the electrochemical product revealed that Ti(OEt)₄ was formed by anodic dissolution of spongy titanium in ethanol solution. X-ray diffraction and transmission electron microscope were, respectively, used to investigate the structure of TiO₂. This study showed that nano-sized TiO₂ prepared by this method has a structural and thermal stability with a narrow size distribution of 5-10 nm. The optimum electrochemical operating conditions established were a temperature of 333-343 K, current density of 400 A m⁻² and faradaic efficiency of 86%. Experiments showed that this process might be recommended as a promising technique for synthesis of nano-sized powder.     

Chemical Reaction Engineering and Research and development of gas solid systems

A general procedure is proposed for innovative research and development of gas-solid reactor systems, with a brief explanation of the significance of each step in the procedureBased upon the contacting mode between gas and solid phases, as well as the ways of supplying thermal energy to the reacting regions, various types of gas-solid reactor systems are classified by using tables of so called “matrix” form, for thermal cracking and gasification of heavy oils, gasification of coal, gasification of solid waste, calcination of limestone, clinkering of cement and reduction of iron ore.The importance of fundamental concepts is emphasized for successful research and development by presenting several examples; namely, calcination of limestone, thermal cracking of heavy oils and gasification of solid waste materials.In connection with the direction in which fundamental research should be oriented, four primary ways of thinking are proposed, which can be applied to obtain innovative ideas for further research and development in this field.One example of the author's practical experience was selected to show the role of the fundamental research in the course of large scale development. Finally the author outlines the role of chemical reaction engineering to innovate the novel gas-solid reactor systems which may be inevitable for simultaneous solution of the three big E's; namely, Energy, Environment and Economy.     

Progressive events in supervisory control and compositional verification

This paper investigates some limitations of the nonblocking property when used for supervisor synthesis in discrete event systems. It is shown that there are cases where synthesis with the nonblocking property gives undesired results. To address such cases, the paper introduces progressive events as a means to specify more precisely how a synthesised supervisor should complete its tasks. The nonblocking property is modified to take progressive events into account, and appropriate methods for verification and synthesis are proposed. Experiments show that progressive events can be used in the analysis of industrial-scale systems, and can expose issues that remain undetected by standard nonblocking verification.     

浅析杨柳青传统年画中娃娃的服饰文化

年画是文化的载体,是一种颇受人民喜欢且富有教育意义的—种艺术表现形式．它记暴下了社会的真实写照,文化中的点点滴滴。有着丰富的内容以及饱满生动的人物形象。虽然在现代社会中,年画逐渐淡出了主导地位。但是依然可以从古老的年画中,认识和体会当时那段历史时期的服饰文化。文章通过简析天津杨柳青传统年画中的娃娃形象,欣赏和体会当时那段时期幼童的服饰文化。     

远程I/O系统与DCS通讯的实现

远程I/O系统是一种新型的控制系统 ,近几年来发展迅速 ,应用量越来越大 ,技术上有一定的先进性。文中简要介绍了远程I/O的发展历史和技术特点 ,通过对德国p +f公司RPI和IS -RPI的具体分析 ,旨在使读者对远程I/O接口的技术特点有一个清晰的认识和了解 ,最后对p +f远程I/O接口与典型的DCS系统的通讯方式作了较详细的介绍。     

聚氨酯弹性体的电致伸缩效应

电致伸缩是指在外电场作用下电介质所产生的与场强二次方成正比的应变。近年来对聚氨酯电致伸缩性能的研究发现，聚氨酯弹性体综合了压电聚合物与传统的锆钛酸铅(PZT)压电陶瓷片的优点，具有很好的应用前景，本文简单介绍了聚氨酯的电致伸缩效应。     

小型轴流压气机清洗两相流场的数值模拟

针对某小型航空发动机单级轴流压气机的清洗需求,以数值模拟结合实验的方法对压气机清洗流场的各种参数进行了分析研究.在初步确定清洗方案的基础上,建立了基于S-A湍流模型的离散相数值模拟理论模型,以经验公式估算喷嘴形成的初始液滴分布,并对喷嘴的实验参数进行了校准,最后以CFD软件进行了流场的数值模拟,计算结果表明：清洗液滴不会对压气机的流场产生明显影响,平面扇形喷嘴在该小型压气机上能获得较好的清洗效果.     

MUSIC算法的FPGA实现

针对多重信号分类（MUSIC）算法计算复杂度高,难以实时实现的特点,给出了适用于均匀线阵的实数化预处理算法和实用的空间谱定义,并选择了适合FPGA硬件实现的特征值分解算法,给出了MUSIC算法FPGA实现的整体架构。仿真实验结果表明,该FPGA实现能够完成MUSIC算法的准确、快速计算。     

CPR1000核电站三废处理控制系统仿真测试技术应用

为实现工厂测试期间,能够最大限度地模拟核电厂三废系统的工艺设备,对三废控制系统（DCS）的组态逻辑正确性进行验证,通过结构化文本语者编写仿真测试程序,对现场的工艺设备的运行状态进行仿真模拟。同时选取对核电站硼回收系统（TEP）的1号除汽器的仿真测试,验证仿真测试程序的可行性,提出了一种低成本,高效率的测试方法。     

那曲典型草地植被光谱特征分析

遥感是大尺度生态研究的重要工具之一,而地面植物群落特征与其光谱特征之间的关系是解译遥感影像的关键。地面实测数据由于其高空间分辨率和高光谱分辨率,能够准确反映地物光谱信息,可以用来指导卫星遥感解译工作,同时为遥感监测草地退化、草地模型建立等提供数据支持。选取西藏那曲地区的优势植被类型作为研究对象,利用ASD FieldSpec 3便携式光谱仪测定优势种的冠层光谱并进行比较,并取其中一种优势种测量其在不同覆盖度和不同生长期的光谱反射特点。研究结果表明:①不同植被群落冠层光谱具有特殊的光谱曲线,可见光波段光谱反射率依次是紫花针茅、小嵩草和藏北嵩草,近红外波段光谱反射率则依次是小嵩草、藏北嵩草和紫花针茅;红边位置可以识别藏北嵩草,但是不能区分小嵩草和紫花针茅;②不同覆盖度的小嵩草红边、“绿峰”位置不随覆盖度的变化而发生变化;连续统去除后得到吸收深度随覆盖度的增加而变大,吸收峰面积随覆盖度的增加而增加;③小嵩草衰退期内,在可见光波段和红边波段,冠层光谱反射率随着叶绿素含量的减少而下降,出现“红边蓝移,绿峰下降”的现象。