Optimizing the Vacuum Heat-Treatment of Hot-Work Tool Steels by Linear Elastic Fracture Mechanics

Linear elastic fracture mechanics was used to optimize the vacuum heat-treatment procedures for conventional hot-work AISI H11 tool steel. The fracture toughness was determined with non-standard, circumferentially notched and fatigue-precracked tensile-test specimens. The fracture-testing method is sensitive to changes caused by variations in the microstructure resulting from the austenitizing and tempering temperatures as well as the homogeneity of the material itself. The combined tempering diagram- Rockwell-C hardness, Fracture toughness K_Ic, Tempering temperature was used for the choice of the vacuum heat-treatment parameters necessary to obtain the best properties for a given application with respect to the investigated steel.     

钛及钛合金中氧和氢的联合测定

叙述了用红外吸收法对钛及钛合金中氧和氢联合测定的方法，取得了测定的最佳条件。连续测定6次的相对标准偏差在10％以下，作加标回收试验的回收率为95．6％～103．9％。分析时间在3min以内，可应用于日常分析，结果满意。     

全面实施工程量清单计价之我见

随着国家《建设工程工程量清单计价规范》及各省计价依据的颁布,工程量清单计价工作已在全国开始实行,但实施的深度和广度不够。作者从管理角度,就如何全面实施工程量清单,对造价管理部门和招投标管理机构相关工作的完善阐述了几点建议和意见。     

松嫩平原洪涝旱碱综合治理及水土资源可持续利用问题

文章依据松嫩平原洪、涝、旱、碱综合治理和在水土资源中存在的问题，提出必须加大科研力度，提高技术含量，从保护生态环境可持续开发利用自然资源的战略角度出发，综合治理洪、涝、旱、碱灾害，并提出了一些具体作法。     

蒸发式冷凝在制冷工艺上的应用

分析对比制冷工艺中几种冷凝方式，指出发展蒸发式冷凝技术对制冷系统节能的重要意义；通过分析蒸发式冷凝的换热机理，在试验和实践的基础上讨论了影响蒸发式冷凝器性能的几个重要因素。     

Procedure for Measuring Low Concentrations of H2 and H2S Above a Water Surface

A simple measuring procedure for low concentrations of H₂ and H₂S (at the level of ppm fractions) above the surface of water by using sensitive gas analyzers is suggested. The procedure is easily accomplished in conditions outside the laboratory (under field conditions).     

Discrete Modeling and Suggested Measurement of Heat Transfer in Gas-Solids Flows

This article presents a two-dimensional transient model for gas-solids flow and heat transfer through pipes using the coupled Computational Fluid Dynamics and Discrete Element Method approach. Numerical simulations have been conducted to examine the modification of fluid thermal structure due to the presence of particles in a pneumatic transport pipeline. Modeled results have demonstrated the key role of transversal motion of rebounding particles in the pipe cross section in altering fluid temperature. Further implementation of this modeling technique in air-drying processes is discussed and possible experimental methods for the measurement of in situ particle and fluid motion and temperature profile are cited.     

Microwave heating synthesis of HgS and PbS nanocrystals in ethanol solvent

A novel route was developed to prepare PbS and HgS nanocrystals in ethanol solvent in the presence of sodium hydroxide by microwave heating method. PbS and HgS nanocrystals were obtained with an average size of approximately 10 and 6 nm, respectively. In the reaction, mercury acetate and lead acetate were used as mercury and lead source; sulfur powder was employed as chalcogenide source. The products were characterized by X-ray powder analysis (XRD), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS) and UV–Vis absorption spectroscopy. The probable mechanism was presented.     

陕北富县探区天然气藏钻井液屏蔽暂堵技术

陕北富县探区上古生界储层属低孔、低渗的致密储层,下古生界主要储集空间为溶蚀孔洞和裂缝,孔洞多为1～3 mm的小孔,裂缝宽度为0.2～7.0 mm,油气主要聚集在裂缝中.优选出了由复合暂堵剂CXD、憎水性屏蔽剂DYC和表面活性剂ABA组成的屏蔽暂堵配方,其中CXD具有架桥作用并对裂缝性储层有独特暂堵效果,DYC有浊点效应、能在井壁上快速形成阻止滤液侵入的油膜,ABA能减少水锁损害.加入暂堵剂后的钻井完井液,抑制性增强,页岩回收率在90%以上;高温高压滤失量降低,滤饼薄而韧、光滑;岩心静态渗透率恢复值大于90%;滤饼摩阻系数降低.富古6井通过使用该完井液,堵塞比和表皮系数都在轻微污染范围内,井径扩大率比其它井有不同程度的降低,表明优选出的屏蔽暂堵钻井完井液,能很好地保护陕北探区天然气藏.     

油罐冒罐事故的原因分析及预防

通过事故实例分析，阐述油罐冒罐事故的原因，并针对原因提出要加强操作人员的责任心教育，完善各项规章制度，不断提高操作人员素质，严格遵守岗位操作规程，及时消除设备缺陷、完善罐区硬件设施和罐区实行现代科学管理等项措施。