曲面小构件变形状态的全场检测问题研究

针对传统方法难以测量曲面小构件非均匀变形的问题,比如受力时发生变形失稳的镍钛形状记忆合金微管,提出了显微成像法和三维形扫描法.它们以非接触和全场的方式追踪构件在不同变形状态下表面标记点的位置,从而获取位移数据,并通过固体力学中经典的几何方程计算得到应变结果.实验证明了所提出方法的易操作性和可靠性,还得到了对于相变材料的力学问题的研究具有重要意义的结果.     

一维声子晶体杆状结构纵向振动带隙特性

基于传递矩阵法,以一维声子晶体杆状结构纵向振动带隙特性为研究对象,应用MATLAB编程,数值模拟了A为金、铜、铝和碳,B为环氧树脂时纵向振动带隙特性,得到铜与与环氧树脂构成一维声子晶体时,形成最大振动带隙宽度3．39KHz ,其中金能够形成较多的带隙区间。数值模拟了A为铜,B为硅橡胶、有机玻璃1、有机玻璃2和塑料时,得到A为铜,B为塑料时形成最大带隙在0．51KHz -7．06KHz ,带隙宽度为6．55KHz ,这两种组合形成了最大带隙宽度。A为铜,B为有机玻璃1时形成较多的带隙结构。研究结论为一维声子晶体器件制作提供参考。     

基于时间约束的优化编码传输算法

考虑到对数据包延迟等服务质量要求比较高的流媒体应用,文章研究了在有记忆接收节点模型也即接收节点可以缓存多个数据包的前提下,数据包有延迟约束的无线网络中基于网络编码的广播调度问题,目标在于最小化超过延迟约束数据包的数目。本文提出一种利用着色图的方法来进行编码调度的算法,可以显著减少超过延迟约束数据包的数目,为以后针对QoS需求的网络编码问题提供了参考。模拟实验表明相比于接收节点丢弃暂时无用数据包的无记忆模型,在有记忆模型下我们的算法可以在很多情况下有效地降低超出延迟约束率,这对时间关键的应用非常重要。     

Characterisation of rare earth minerals with field emission scanning electron microscopy

Abstract

Rare earth elements are becoming increasingly in demand, due to their prevalence in both renewable energy devices and high end electronics. The characterisation of the composition and morphology of the various phases that have valuable rare earth elements in the ores are needed in conjunction with the study of their physicochemical properties to optimise industrial process to extract the minerals containing the rare earth elements. Rare earth bearing minerals contain many elements with overlapping X-ray peaks (L- and M-lines) with an energy dispersive spectrometry detector, requiring a high degree of X-ray energy resolution. A program was developed to obtain the intensity of each peak by deconvolution of the X-ray spectrum. Low accelerating voltage of less than 5 kV and small beam diameter of less than 10 nm of a cold field emission scanning electron microscope allow x-ray microanalysis on the nanometre scale. A 100 nm wide phase was observed at 4 kV on a backscattered electron micrograph. Furthermore, a small beam diameter of less than 10 nm was used for identification of small phases of a few micrometres.

Les éléments de terre rare sont de plus en plus en demande, grâce à leur prévalence tant dans les dispositifs d’énergie renouvelable que dans l’électronique de haute gamme. On a besoin de caractériser la composition et la morphologie des différentes phases qui contiennent des terres rares de valeur dans les minerais, en combinaison avec l’étude de leurs propriétés physico-chimiques, afin d’optimiser le procédé industriel d’extraction des minéraux contenant les terres rares. Les minéraux porteurs de terre rare contiennent plusieurs éléments ayant des pics de rayons x qui se chevauchent (lignes L et M) avec un détecteur de spectroscopie à dispersion d’énergie, nécessitant une haute résolution énergétique. On a développé un programme visant à obtenir l’intensité de chaque pic par déconvolution du spectre de rayons x. Un faible voltage d’accélération de moins que 5 kV et un faisceau à faible diamètre de moins que 10 nm d’un microscope électronique à balayage par cathode froide permettent la microanalyse des rayons x à l’échelle du nanomètre. On a observé une phase de 100 nm de largeur à 4 kV sur une micrographe d’électrons rétrodiffusés. De plus, on a utilisé un faisceau de faible diamètre de moins que 10 nm pour l’identification de petites phases de quelques μm.     

开展设备状态检修推动生产管理升级

围绕供电公司状态检修工作的开展,对状态检修工作进行了系统的思考,提出了深化落实的具体思路和方法。     

New Linkage with Linear Actuator for Tracking PV Systems with Large Angular Stroke

This paper focuses on the development of an optimized photovoltaic tracking system involving low-cost, relative simple mechanisms, with linear actuators able to insure strokes comparable with those resulted when using gear rotary actuators. Starting with a rhombus linkage, with a linear actuator on the diagonal used for the elevation motion till 90°, a new performance solution is generated. This new linkage allows large angular strokes by using an asymmetric rhombus and an eccentrically positioned linear ac...     

Variation in structural and dielectric properties of co-precipitated nanoparticles strontium ferrites due to value of pH

Nanoparticles of strontium ferrites with nominal composition SrFe₁₂O₁₉ were prepared by co-precipitation method, by decreasing pH from 13 to 8 with a regular step of 1. The secondary phase of α-Fe₂O₃ was increased with the decrease in pH. The crystallite size estimated from X-rays diffraction data was in the range 52-70 nm, which is much smaller than that already reported. Most of the particles formed had hexagonal structure, as observed by the scanning electron microscopy. Particle size and dielectric loss were increased where as dc electrical resistivity and dielectric constant were decreased with decrease in pH. The results show that the material synthesized with higher pH is phase pure and is potentially more suitable for high frequency applications.     

Twinning, dynamic recovery and recrystallization in the hot rolling process of twin-roll cast AZ31B alloy

Hot-rolling experiments with a reduction from 10% to 60% in single pass were conducted on AZ31B twin-roll cast sheets. Optical microscope (OM), electron backscattered diffraction (EBSD) tests and transmission electron microscope (TEM) were used to investigate twinning and DRV/DRX behaviors at different stage in the hot-rolling process. Two types of twinning occurred in the initial stage of hot-rolling process. DRV and discontinuous recrystallization dominated at moderate strain while continuous DRX took place homogeneously throughout original grains at the largest strains.     

Isocyanate-rich cellulose nanocrystals and their selective insertion in elastomeric polyurethane

Cellulose nanocrystals (CNC) were successfully obtained and modified with 1,6-hexamethylene diisocyanate (HDI) by means of in situ polymerization varying the CNC/HDI molar ratio to evaluate the number of anchored chains to the CNC. The modification was examined by elemental analysis, nuclear magnetic resonance (¹³C NMR) and attenuated total reflection Fourier transform infrared spectroscopy (IR-ATR). Nanocomposites containing 1.5 wt% CNC, modified and unmodified, were prepared by solvent casting. Thermal and mechanical properties of the resulting films were evaluated from the viewpoint of polyurethane microphase separated structure, soft and hard domains. CNC were effectively dispersed in the polyurethane matrix and depending on surface chemistry, the nanoreinforcement interacts selectively with matrix nanodomains. This interpretation is supported by differences in thermal and mechanical properties of the nanocomposites and also confirmed by AFM images. Isocyanate rich cellulose nanocrystals interacted with matrix hard phase, promoting physical association with hard segments, enhancing stiffness and dimensional stability versus temperature of the nanocomposite.