Ti6Al4V钛合金表面蓝色微弧氧化膜的制备及性能

利用微弧氧化技术在Ti6Al4V钛合金表面制备出蓝色微弧氧化膜。对微弧氧化膜的微观形貌和元素组成进行了分析,并对微弧氧化膜的显微硬度进行了测试。结果表明:微弧氧化膜表面光整,呈均匀深蓝色,其主要由Ti、Mn、O和C四种元素组成,还含有少量的V、Al和Si元素;微弧氧化膜的表面粗糙度约为0.159μm,与钛合金的表面粗糙度相近;微弧氧化膜的显微硬度为5 437.4 MPa,显著高于钛合金的显微硬度。     

M2高速钢强脉冲离子束表面改性及其耐磨耐蚀性

针对陶瓷梯度涂层性能优良,在大气氛围下等离子喷涂制备涂层会受到空气氧化这一情况,在可控气氛（Ar气）中采用等离子喷涂的方法制取了NiCrBSi/Al₂O₃的梯度涂层,并且与大气条件下制取的NiCrBSi/Al₂O₃的梯度涂层进行对比.借助扫描电子显微镜（SEM）、x 射线衍射仪（XRD）对涂层的组织分布、相结构进行分析.结果表明：在Ar气和大气中梯度涂层的组织内部都没有明显的界面,实现了组织的连续变化;在Ar气中制取的梯度涂层的组织更加致密,被氧化的程度更低,质量更好.     

一种节能高效固体软氮化技术的研发

针对固体软氮化存在的能耗高、效率低等不足之处,研究设计了一种新的节能、高效固体软氮化技术。新技术通过在软氮化粉末渗扩介质与被渗样品间施加合适参数的直流电场来实现。研究结果表明,直流电场可降低处理外热温度,显著增加渗速,改善渗层硬度梯度分布,达到了节能、高效之目的。     

Effect of heat treatment on the mechanical properties of FeCoZrWB bulk metallic glass

A Fe61Co10Zr5W4B20 bulk metallic glass (BMG) with a diameter of 2 mm was prepared by using copper mould suction casting. The X-ray diffraction (XRD), differential scanning calorimetry (DSC), micro-hardness and compression tests were adopted to investigate the structure, thermal stability, especially, the effect of heat treatment on the micro-hardness and compression strength of this BMG. The BMG exhibits micro-hardness of about 1 207 Hv and compression fracture strength of about 1 707.6 MPa. After being annealed below the onset of crystallization temperature, the micro-hardness almost keeps constant. But after being annealed above the peak of crystallization temperature, the micro-hardness increases firstly and then declines gradually with the elongation of annealing time. However, annealed for the same period of time, the micro-hardness will increase with the rise of annealing temperature, while the compression fracture strength will apparently decrease.     

电脉冲对335HRB螺纹钢凝固组织和力学性能的影响

对335HRB螺纹钢进行电脉冲处理,结果显示:经过2600V电脉冲处理后335HRB螺纹钢宏观凝固组织均发生明显变化,树枝晶减少,等轴晶增加;微观凝固组织中魏氏铁素体组织减少,珠光体增加,且珠光体片层间距变薄。电脉冲对335HRB螺纹钢显微硬度也具有明显的影响,使珠光体的显微硬度(HV)由183HV0.1提高到219HV0.1,铁素体显微硬度由未经过处理的127.2HV0.1提高到138.1HV0.1。     

表面活性剂对Cu-SiO_2复合镀层性能的影响

分别添加十二烷基硫酸钠、十六烷基三甲基溴化铵和聚乙二醇,制备Cu-SiO2复合镀层。考察了表面活性剂的带电性质与添加量对Cu-SiO2复合镀层的显微硬度及耐磨性的影响。结果表明:添加十二烷基硫酸钠获得的Cu-SiO2复合镀层的显微硬度相对较高且耐磨性较好。     

基于正交设计的Cu-Ni-Si合金时效工艺研究

利用L9(33)表对Cu-3.2Ni-0.75Si-0.3Zn合金的时效工艺进行了正交试验,结果发现,各因素对合金电导率和显微硬度影响程度的主次顺序为:时效温度>合金状态>时效时间。综合分析后认为,该合金热轧板材经60%冷变形后,可直接进行500℃×2h时效而省去固溶处理。本工艺在保证合金性能不降低的情况下,可以显著节约成本和提高生产率。试验所得合金的性能为:导电率43.95%IACS,显微硬度219.9HV,已达到国外的先进水平。     

45^#钢在高周疲劳循环下的循环软化问题的研究

通过研究４５＾＃钢疲劳循环后材料的力学性能来反映高周疲劳产生的材料软化现象，取得了一些进展。实验结果与假设基本一致。     

激光表面熔凝处理对30Cr2Ni4MoV转子钢高温水腐蚀性能的影响

进行了三种强度级别的30Cr2Ni4MoV钢的激光表面熔凝处理,用电化学极化曲线和高温应力腐蚀试验考察了其耐腐蚀性能。研究表明:激光熔凝处理后在30Cr2Ni4MoV表面形成了约10~20μm的致密马氏体硬化层和压应力状态,基材状态对激光熔凝硬化层的性能无明显影响,但激光功率增大会导致表面熔凝层硬度水平降低;激光表面熔凝处理使腐蚀电位左移,腐蚀电流密度减小,抗腐蚀性能明显增强。     

Microstructural Evolution of a Hypoeutectoid Pearlite Steel under Rolling-sliding Contact Loading

To study the microstructural evolution of pearlite steel subjected to pure rolling and rolling-sliding contact loading,a hypoeutectoid pearlite steel with composition and microstructure similar to BS11 was designed and twindisc tests of this pearlite steel were performed to simulate the wheel/rail system.After a series of twin-disc tests,optical microscope(OM)observation,scanning electron microscope(SEM)observation,X-ray diffraction(XRD),and micro-hardness tests were conducted to characterize the microstructure.Under the pure rolling contact condition,a large amount of reticular cracks emerged within 60μm below the contact surface of the samples after 120 000 revolutions.The largest deformation was approximately 200μm below the contact surface.Under the rolling-sliding contact condition,the nodularization of pearlite within 100μm below the contact surface was obvious.The microstructure and stress-strain distribution of the area within 2mm below the contact surface were investigated.The distribution of micro-hardness under the contact surface varied with contact conditions.Finite element method(FEM)was used to simulate the stress-strain distribution.The results of SEM,FEM,and micro-hardness tests indicated that under the pure rolling contact condition,the maximum plastic strain was approximately 200-400μm below the contact surface.Conversely,under the rolling-sliding contact condition,the maximum plastic strain emerged on the contact surface.Under the pure rolling contact condition,the distribution of micro-hardness was almost identical to that of the equivalent plastic strain.Under the rolling-sliding contact condition,the distribution of micro-hardness was affected by the equivalent plastic strain and tangential stress.