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61.
62.
M. D. Joseph Sebastian B. Rudraswamy M. C. Radhakrishna Ramani 《Bulletin of Materials Science》2003,26(5):509-515
Cobalt ferrite (CoxFe3?xO4) is prepared in powder form by thermal decomposition of iron and cobalt salts and is analysed by X-ray diffraction and Mössbauer spectroscopic techniques. The variation of Mössbauer parameters, lattice parameters and crystallite size of the products formed with variation in the composition of Fe and Co ratios are studied. The studies confirm the formation of nano-size cobalt ferrite particles with defect structure and it is found to be maximum for the Fe : Co = 60 : 40 ratio of the initial precursor oxides. 相似文献
63.
Stanislav I. StoliarovPhillip R. Westmoreland Marc R. Nyden Glenn P. Forney 《Polymer》2003,44(3):883-894
The theory and implementation of reactive molecular dynamics (RMD) are presented. The capabilities of RMD and its potential use as a tool for investigating the mechanisms of thermal transformations in materials are demonstrated by presenting results from simulations of the thermal degradation of poly(methyl methacrylate) (PMMA). While it is known that depolymerization must be the major decomposition channel for PMMA, there are unanswered questions about the nature of the initiation reaction and the relative reactivities of the tertiary and primary radicals formed in the degradation process. The results of our RMD simulations, performed directly in the condensed phase, are consistent with available experimental information. They also provide new insights into the mechanism of the thermally induced conversion of this polymer into its constituent monomers. 相似文献
64.
Z.M. Zhong J. Chen P. Zhong J.B. Wu 《The International Journal of Advanced Manufacturing Technology》2006,28(9):855-862
As the result of vibration emission in air, a machine sound signal carries important information about the working condition
of machinery. But in practice, the sound signal is typically received with a very low signal-to-noise ratio. To obtain features
of the original sound signal, uncorrelated sound signals must be removed and the wavelet coefficients related to fault condition
must be retrieved. In this paper, the blind source separation technique is used to recover the wavelet coefficients of a monitored
source from complex observed signals. Since in the proposed blind source separation (BSS) algorithms it is generally assumed
that the number of sources is known, the Gerschgorin disk estimator method is introduced to determine the number of sound
sources before applying the BSS method. This method can estimate the number of sound sources under non-Gaussian and non-white
noise conditions. Then, the partial singular value analysis method is used to select these significant observations for BSS
analysis. This method ensures that signals are separated with the smallest distortion. Afterwards, the time-frequency separation
algorithm, converted to a suitable BSS algorithm for the separation of a non-stationary signal, is introduced. The transfer
channel between observations and sources and the wavelet coefficients of the source signals can be blindly identified via
this algorithm. The reconstructed wavelet coefficients can be used for diagnosis. Finally, the separation results obtained
from the observed signals recorded in a semi-anechoic chamber demonstrate the effectiveness of the presented methods . 相似文献
65.
Li-Tang Yan 《Polymer》2006,47(18):6472-6480
The surface-directed spinodal decomposition (SDSD) of polymer binary mixture with different values of surface potential is numerically simulated in three-dimension (3D) by cell dynamic systems (CDS). Furthermore, the growth laws of the wetting layer are theoretically analyzed by the current equation and the dynamical scaling. The results show that the thickness of the wetting layer increases with the increasing surface potential. The crossover, which is later for larger values of surface potential, appears in the evolution curve of the wetting layer. Before the crossover, the growth law is the surface potential dependant growth law. Subsequently, the growth law is the typical Lifshitz-Slyozov (LS) growth law. The results indicate that the surface potential can result in the mutual transformation between completely wetting and partially wetting for the substrate interface. It can be found that the higher surface potential leads to the faster and stronger transmission of the effect of the substrate on the spinodal decomposition in the bulk. 相似文献
66.
We consider the problem of finding a transitive orientation of a comparability graph, such that the edge set of its covering graph contains a given subset of edges. We propose a solution which employs the classical technique of modular tree decomposition. The method leads to a polynomial time algorithm to construct such an orientation or report that it does not exist. 相似文献
67.
Jung-Han Kimn Marcus Sarkis 《Computer Methods in Applied Mechanics and Engineering》2007,196(8):1507-1514
Overlapping balancing domain decomposition methods and their combination with restricted additive Schwarz methods are proposed for the Helmholtz equation. These new methods also extend previous work on non-overlapping balancing domain decomposition methods toward simplifying their coarse problems and local solvers. They also extend restricted Schwarz methods, originally designed to overlapping domain decomposition and Dirichlet local solvers, to the case of non-overlapping domain decomposition and/or Neumann and Sommerfeld local solvers. Finally, we introduce coarse spaces based on partitions of unity and planes waves, and show how oblique projection coarse problems can be designed from restricted additive Schwarz methods. Numerical tests are presented. 相似文献
68.
S. Zisekas G. Karagiannakis C. Kokkofitis M. Stoukides 《Journal of Applied Electrochemistry》2008,38(8):1143-1149
The reaction of NH3 decomposition was studied on Ag in a proton conducting double chamber cell-reactor. The proton conductor was a strontia-ceria-ytterbia
(SCY) perovskite of the form SrCe0.95Yb0.05O3−α. The reaction was studied at 350–700 °C and atmospheric total pressure. The proton transference number (PTN) was calculated
by simultaneous measurement of the imposed current and the proton flux and it was found to vary between 0.5 and 0.7. The effects
of imposed current, temperature and inlet gas composition on the reaction rate and the PTN, were examined. Although the faradaic
efficiency (Λ) remained near unity in all experiments, reaction rate enhancements (ρ) as high as 57 were achieved. An up to
90% decrease in the activation energy of the reaction was observed when protons were electrochemically “pumped” away from
the catalyst. 相似文献
69.
The temperature programmed (palladium) hydride decomposition appeared very effective method for diagnosing the extent of alloying in Pd-Pt/SiO2 catalysts. Introduction of Pt to Pd catalysts moves the TPHD peak gradually towards lower temperatures and the shift in hydride decomposition peak is accompanied by a decrease in the amount of released hydrogen. The catalysts prepared the direct redox method showed much better alloy homogeneity than the samples prepared by coimpregnation. The results of probing with other techniques, i.e. catalytic probing with hydrodechlorination of CCl2F2 and XRD, were in line with TPHD data. The catalytic probing showed the presence of synergistic effect, a clear indication of Pd-Pt mixing. XRD data of post-reaction samples showed carbon incorporation into Pd-rich phase, whereas separate Pt-rich phase did not experience any bulk carbiding. 相似文献
70.
本文研究了用金属有机物热发解法制备PLT8薄膜的工艺过程和基片对薄膜结构的影响,并且给出了铁电性能的测量结果。 相似文献