迁安精矿粉高碱度烧结矿试验研究

对迁安地区磁选精矿粉添加磷石粉和Ｂ２Ｏ３，生产二元碱率为２．０左右的高碱度烧结矿，在实验室和现场进行了试验。结果表明：加入少量磷灰石粉或硼即可完全抑制烧结矿冷却过程中的自然粉化现象；ＭｇＯ含量对烧结矿质量影响明显；烧结矿的冶金性能良好。     

锰锌铁氧体纳米粉体的液相制备及磁性能

以δ-FeOOH为前驱体,用氨水调节溶液的pH值,分别采用(1)90℃水浴加热动态转化、(2)沸腾回流动态转化,(3)90℃静态转化及(4)200℃水热法四种方法合成了锰锌铁氧体纳米粉体.采用X射线衍射仪(XRD),透射电子显微镜(TEM)、振动样品磁强计(VSM)和X射线荧光光谱仪(XRF)等方法对粉体进行了表征,对四种液相法制备的锰锌铁氧体纳米粉体的结构和性能等进行了对比和分析.结果表明,四种方法中沸腾回流相转化法得到的产物具有磁性能较好、形状较规则、粒径可控等优点.     

纳米陶瓷的制备

纳米陶瓷材料可显著降低材料的烧结致密化程度,节约能源;并可改善陶瓷材料的性能,提高其使用可靠性。主要介绍了纳米陶瓷的制备方法,包括纳米陶瓷粉体的制备、成型和烧结。     

Nondegradative microextrusion of resorbable polyesters for pharmaceutical and biomedical applications: The cases of poly‐lactic‐acid and poly‐caprolactone

In recent years biodegradable polymers, particularly polyesters such as the poly(lactic acid) (PLA) and polycaprolactone (PCL), have gained high interests for their applicability in the biomedical and pharmaceutical fields where they're used for manufacturing various different resorbable devices, from tissue engineering scaffolds to controlled drug release systems. Despite many positive characteristics, processability of these materials still remains a critical issue as they easily tend to degrade during manufacturing. In this article we aimed to assess microextrusion as a nondegradative process for manufacturing PLA and PCL. The results we experimentally obtained, that are hereby presented, set a new point in the on‐going debate on degradation during processing of resorbable polymers as they allow to affirm that microextrusion leaves unmodified molecular weight distributions without producing any evident reductions in mean molecular weight. Microextrusion thus represents a risk‐free high molecular weight polymer processing solution for obtaining nondegraded products within pharmaceutical and biomedical production lines, such as for scaffolds for tissue engineering applications or drug delivery. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008     

Engineering extruded collagen fibers for biomedical applications

Extruded collagen fibers constitute a promising biomimetic scaffold for tissue engineering applications. In this study, we compared the structural, thermal, and mechanical properties of fibers produced from either NaCl or poly(ethylene glycol) with a number-average molecular weight of 8000 (PEG 8K), the only two coagents that have been used in the fabrication process. As novel, we report the fabrication of fibers with properties similar to native or synthetic fibers using other coagents. NaCl derived fibers were characterized by higher thermal stability (p < 0.026), stress (p < 0.001), and modulus (p < 0.0025) values than PEG 8K, whereas the latter yielded more extendable fibers (p < 0.012). Poly(ethylene glycol)s with number-average molecular weights of 200 and 1000 produced fibers with similar mechanical properties (p > 0.05) that were thinner (p < 0.033), stiffer (p < 0.022), and less extendable (p < 0.0002) than those of PEG 8K. Poly(vinyl alcohol) (PVA) with a number-average average molecular weight of 9–10,000 and PEG 8K yielded fibers with similar diameters and stress-at-break values (p > 0.05); however, the poly(ethylene glycol) derived fibers were more extendable (p < 0.0003), whereas the PVA fibers were stiffer (p < 0.029). Gum-arabic- and soluble-starch-derived fibers were of similar tensile strength, extendibility, and stiffness (p > 0.05). In this in vitro study, the thickest (p < 0.011) and the weakest (p < 0.0066) fibers were produced in the presence of sodium sulfate. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008     

石油套管的壁厚公差对承载能力的影响

石油套管的强度计算是按API标准进行的，它未能反映高强度套管和尺寸公差对抗压溃能力的影响。利用弹塑性力学理论建立理想的石油套管的抗压溃能力计算公式，并考虑套管的壁厚公差对计算公式进行修正。用该方法对受均匀载荷及非均匀载荷作用的套管进行分析，并同有限元计算结果相比，两者十分吻合，说明该方法的有效性。     

WG硅微粉及用于塑料制品的试验

简要介绍了硅粉的理化性能，分析了WG硅微粉的形成过程，并进行了用于塑料制品的使用性能的试验研究，为硅粉用于塑料制品工艺提供了有利的借鉴。     

Relation between microstructure, properties and spark plasma sintering (SPS) parameters of pure ultrafine WC powder

A combined experimental/numerical methodology is developed to fully consolidate pure ultrafine WC powder under a current-control mode. Three applied currents, 1900, 2100 and 2700 A, and a constant pressure of 20 MPa were employed as process conditions. The developed spark plasma sintering (SPS) finite-element model includes a moving-mesh technique to account for the contact resistance change due to sintering shrinkage and punch sliding. The effects of the heating rate on the microstructure and hardness were investigated in detail along the sample radius from both experimental and modeling points of view. The maximum hardness (2700 HV10) was achieved for a current of 1900 A at the core sample, while the maximum densification was achieved for 2100 and 2700 A. A direct relationship between the compact microstructure and both the sintering temperature and the heating rate was established.     

AgWC12C3的粉末粒度对产品密度的影响

粉末粒度对粉末制品的性能具有重要的影响,而这些影响主要通过改善材料的密度来达到。该文根据模拟粉末堆积模型,确定相对合理的粒度组成,并通过试验予以验证。