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本文用超声浸液法测量了单向纤维增强热塑性树脂及其半互穿聚合物网络(Semi-IPN)复合材料的杨氏模量、剪切模量、泊松比和内耗,并对不同树脂、纤维和Semi-IPN中共混组成比对弹性性能的影响进行了研究。 相似文献
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This paper addresses the problem of semi‐global stabilization by output feedback for a class of nonlinear systems whose output gains are unknown. For each subsystem, we first design a state compensator and use the compensator states to construct a control law to stabilize the nominal linear system without the perturbing nonlinearities. Then, combining the output feedback domination approach with block‐backstepping scheme, a series of homogeneous output feedback controllers are constructed recursively for each subsystem and the closed‐loop system is rendered semi‐globally asymptotically stable. 相似文献
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In this paper, a feedback model predictive control method is presented to tackle control problems with constrained multivariables for uncertain discrete‐time nonlinear Markovian jump systems. An uncertain Markovian jump fuzzy system (MJFS) is obtained by employing the Takagi‐Sugeno (T‐S) fuzzy model to represent a discrete‐time nonlinear system with norm bounded uncertainties and Markovain jump parameters. To achieve more generality, the transition probabilities of the Markov chain are assumed to be partly unknown and partly accessible. The predictive formulation adopts an on‐line optimization paradigm that utilizes the closed‐loop state feedback controller and is solved using the standard semi‐definite programming (SDP). To reduce the on‐line computational burden, a mode independent control move is calculated at every sampling time based on a stochastic fuzzy Lyapunov function (FLF) and a parallel distributed compensation (PDC) scheme. The robust mean square stability, performance minimization and constraint satisfaction properties are guaranteed under the control move for all admissible uncertainties. A numerical example is given to show the efficiency of the developed approach. Copyright © 2011 John Wiley and Sons Asia Pte Ltd and Chinese Automatic Control Society 相似文献
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Summary: A semi‐batch process using nitroxide mediated polymerization, was explored for the design of low molecular weight solvent‐borne coatings, typical of those used in the automotive industry. While living radical polymerization (LRP) offers many advantages in the control of polymer chain microstructure that may confer important physical and chemical property benefits to coatings, adapting LRP to a semi‐batch process poses significant challenges in the design and operation of the process. Using styrene monomer, various two‐component initiating systems (free radical initiator, 4‐hydroxy‐TEMPO) were studied to understand the effects of different initiators on the course of polymerization. In addition, an alkoxyamine was synthesized and used as the initiating source. The initiators Luperox 7M75 and Luperox 231 give higher polymerization rates and reasonable control over polymerization, while benzoyl peroxide (BPO), Vazo 67, and the alkoxyamine are less effective. The number of polymer chains in the final product is always less than the theoretical value, reflecting poor initiation efficiency, probably resulting from undesirable termination reactions that become important due to the nature of the semi‐batch process. Adding camphorsulfonic acid (CSA) or charging initiator concurrently with monomer during semi‐batch feed, can increase the polymerization rate while maintaining the living character of the polymerization. The copolymerization of styrene and butyl acrylate is also shown to exhibit living character.
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Semi1 and semi2 interpenetrating polymer networks (IPNs) of PVC and in situ formed PMMA have been synthesized using diallyl phthalate and ethylene glycol dimethacrylate as the crosslinkers of PVC and PMMA, respectively. These two types of IPNs have been compared w.r.t their physical, mechanical, and thermal properties and an endeavor has been made to find a correlation of these properties with the morphology generated in these systems. The semi1 IPNs displayed a decrease in their mechanical parameters and the physical properties as well, while in contrast, the semi2 IPNs exhibited a marginal increase in the corresponding values after an initial drop upto about 15% of crosslinked PMMA incorporation when compared to the crosslinked PVC in the case of semi1 IPN and linear PVC in the case of semi2 IPN. The various samples of semi1 and semi2 IPNs showed a two‐stage degradation typical of PVC, while confirming the increased stability with the samples having higher percentages of PMMA. The influence of crosslinking of the major matrix in semi1 IPN was almost counterbalanced by the influence of crosslinking in the dispersed PMMA phase in the case of semi2 IPN. The softening characteristics as detected by the extent of penetration of the probe, as has been detected by thermomechanical analysis, are in conformity with their mechanicals. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 97: 1725–1735, 2005 相似文献
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To reduce the highly hydrophilic property of chondroitin sulfate (ChS), a semi‐interpenetrating polymer network (semi‐IPN) of chondroitin sulfate/polyacrylic acid (PAA) was prepared as a drug carrier by crosslinking acrylic acid with diethyleneglycol diacrylate. The swelling properties of the semi‐IPNs with different concentrations of crosslinking agent were correlated. The moisture sorption profiles were evaluated using differential thermal analysis. Ketoprofen was used as a drug probe to evaluate the performance of the drug released from the semi‐IPN matrices. The prepared semi‐IPNs demonstrated significant swelling reduction properties with both gastric and intestinal fluids compared with those of both the pure ChS and the ChSAA blend without the crosslinking agent. The amount of accumulated drug released from the semi‐IPNs was less than 30 wt % at pH 1.2 and up to 80 wt % at pH 7.4. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 114–122, 2002 相似文献