Instrumental characterization of clay by XRF,XRD and FTIR

Instrumental characterizations of the clay were performed by different techniques such as XRF, XRD and FTIR. XRF shows the chemical compositions of the clay where Al-oxide and silica oxide are present in major quantity whereas XRD confirms the presence of these minerals in clay. FTIR studies show the presence of quartz, alumina, haematite and different mineral matters.     

Electron spectroscopies and their use for materials characterization

We present here a general overview of electron spectroscopies from a practical point of view. The most frequently used ones are described and the type of structural information they can provide on materials is explained in relation to the physical processes on which they are based. Furthermore, we explore critically and in detail various tools that have been developed to allow a systematic solving of structures by these spectroscopies.     

Young’s modulus of crystalline C60 nanotubes studied by in situ transmission electron microscopy

Bending tests of crystalline nanotubes composed of fullerene C₆₀ molecules are performed inside a high-resolution transmission electron microscope. We fixed one side of a C₆₀ nanotube with a body-centered tetragonal structure with typical inner and outer diameters, i.e., 180 nm and 510 nm, respectively, and then applied concentrated forces on the other side using piezomanipulation of a silicon nanotip. The bending process was observed in situ by transmission electron microscopy with simultaneous measurements of the forces by an optical deflection method. It was found that the Young’s modulus of the nanotube was estimated to be 62–107 GPa, which was 1.1–3.3 times larger than that of C₆₀ nanowhiskers. The result concerning the increase in the Young’s modulus of the C₆₀ nanotube provided an experimental evidence for the structural model composed of an inner core and a surface shell for C₆₀ nanowhiskers.     

多相流动超声波测井模拟实验研究

油田油井动态监测的实质是准确地测量各生产层位的流量和含水率，为此研制了超声波三相流量测试仪。利用该仪器测量油、气、水多相流动的各相流量，通过模拟井动态实验验证了该测井方法的可行性，适用于我国90％以上的生产井．克服了现有国产仪器不能测气和用集流伞下井测量等缺点。     

Preparation and Characterization of Zeolite Beta with Low SiO_2/Al_2O_3 Ratio

Zeolite beta with a low SiO2/Al2O3 ratio was synthesized by a novel two-step process.The synthesized sample was characterized with XRD,SEM,FTIR,and N2 adsorption-desorption and solid-state MAS NMR.The results showed that aluminium species were inserted into the framework of zeolite beta.The BET surface area,volume,and particle size of the zeolite beta sample decreased with decreasing SiO2/Al2O3 ratio.Our process was proved an efficient route to synthesize zeolite beta with a low SiO2/Al2O3 ratio.     

CTS-26型超声探伤仪典型故障的分析与排除

在简要介绍CTS-26型超声探伤仪工作原理及组成的基础上。对其几种典型故障作了具体的分析和处理。     

Ultrasonic study of molecular association of poly(vinyl chloride) solution in tetrahydrofuran

Ultrasonic absorption, velocity, adiabatic compressibility, relaxation time and relaxation amplitude measurements are reported on poly(vinyl chloride) (PVC) solution in tetrahydrofuran (THF) using pulsed ultrasonic apparatus operating at 2 MHz and 313 K. Results show a linear increase of velocity. density, viscosity, absorption coefficient, relaxation time and relaxation amplitude values with the increase of PVC concentration in THF. In contrast the compressibility decreases with increasing PVC concentration. This suggests interaction between PVC and THF molecules.     

Increasing testing productivity and software quality: A comparison of software testing methodologies within NASA

Pressure to compress the development life cycle and reduce the duration and resources committed to testing lead to experimentation in testing at the NASA Goddard Space Flight Centerís Software Engineering Laboratory. This study investigates the trend to reduce developer testing and increasingly rely upon inspection techniques and independent functional testing to shorten the development life cycle, improve testing productivity, and improve software quality.An approach is developed to conduct this comparison. In particular, the problem faced by software researchers, having a comprehensive characterization of software projects so similar types may be identified for comparative studies, is addressed using expert opinion.     

第四十届国际尖端材料学会年会与展览简介

介绍国外先进材料技术现状与发展趋势，即强调发展新材料技术，低成本生产技术，质量控制技术，重视先进材料应用，两用技术和军转民。     

基于LabVIEW的超声信号小波阈值去噪方法

图形化编程软件LabVIEW具有强大的信号采集功能,但对于需要进行大量数据运算处理的复杂应用就显得力不从心。数学工具软件MATLAB强大的计算功能及较高的编程效率可以弥补LabVIEW开发的不足。文中结合两者软件的优点,采用混合编程的方法进行实际工程的去噪处理,同时针对超声缺陷回波信号信噪比低、易于被噪声淹没的特点,选取小波阈值去噪的方法,通过调用LabVIEW里的MATLAB Script节点对信号进行仿真实验,仿真结果表明采用stein的无偏风险阈值去噪的方法消噪效果最为明显,得到较高的信噪比。