3-丙酰氨基-N,N-二丙酸甲酯基苯胺的合成研究

用无水三氯化铝作催化剂在较低温度下将3-氨基丙酰苯胺和丙烯酸甲酯转化为3-丙酰氨基-N,N-二丙酸甲酯基苯胺,其产品收率达到89%,纯度高于92%。     

深厚软土地基上新建煤场与海堤的最小安全距离分析

软土在我国广泛分布,其工程性质极差。本文结合实际工程,运用传统极限平衡法和FLAC3D数值计算方法,综合分析了深厚软土地基上新建煤场大面积堆载对邻近海堤地基稳定性的影响,提出了煤场与海堤之间最小的安全距离。     

Remote plasma etching of titanium nitride using NF3/argon and chlorine mixtures for chamber clean applications

To avoid plasma induced erosion of chamber hardware, the application of remote plasma sources to activate the etch gases was introduced. We present results on the etch behaviour of titanium nitride (TiN) using mixtures of NF₃, Cl₂ and argon. The gas mixture was excited in a remote plasma source and then routed through a reaction chamber to study the etch behaviour of TiN samples which simulate the situation at the chamber walls. The dependency of the TiN etch rate on temperature, gas flow, composition and pressure was examined. While the temperature (studied in the range 25-300 °C) turned out to be the most sensitive parameter, the general etch rate was mainly dependent on the availability of atomic fluorine. Etch products and NF₃/Cl₂ dissociation have been monitored by quadrupole mass spectrometry and infrared spectroscopy. While NF₃ showed a high decomposition up to 96%, chlorine decomposition was not observed. However the addition of chlorine increased the etch rates up to 260% in the low pressure/low temperature regime. Surface effects of chlorine addition are indicated by X-Ray Photoelectron Spectrometry and REM surface analysis.     

Production and properties of crude enterotoxin of Pseudomonas aeruginosa

Pseudomonas aeruginosa CTM-3 was found to be the most potentially enteroxigenic strain out of the 12 isolates recovered from milk, as a high fluid length ratio, i.e. F/L (1.1) in rabbit gut and a strong permeability response in rabbit skin (38.5 mm² necrotic zone) was obtained with this culture. No clear-cut relationship between the two tests was observed. Six of the ethidium bromide (300 μg/ml) cured variants of this culture completely lost their ability to produce enterotoxin indicating the possible involvement of a plasmid in enterotoxin synthesis. The crude enterotoxin from P. aeruginosa CTM-3 was completely inactivated in 15 s at 72°C. However, it was fairly stable at pH values in the range 4.5–7.5. Both pepsin and trypsin inactivated the enterotoxin activity at a concentration of 40 μg/ml. Organic acids, formalin and hydrogen peroxide had no significant effect on the enterotoxin activity. The need for further investigations with purified preparations is emphasized.     

An Algorithm to Detect the Presence of 3D Target Motion from ISAR Data

We present an algorithm to detect the presence of 3D target motion from ISAR data. Based on the 3D point scatterer model, we first examine the effect of 3D motion on ISAR imaging. It is shown that existing motion compensation algorithms cannot properly focus targets exhibiting 3D motion during the imaging interval. An algorithm is then derived to blindly detect the degree of 3D target motion from raw radar data. It is based on measuring the linearity of phases between two or more point scatterers on the target. The phase estimation is implemented using the adaptive joint time-frequency technique. Examples are provided to demonstrate the effectiveness of the 3D motion detection algorithm with both simulation and real ISAR data. The detection results are corroborated with the truth motion data from on-board motion sensors and correlated with the resulting ISAR images.     

以3G为核心的通信新技术综述

随着第三代移动通信标准的发展,涌现出各种新兴的通信技术,它们所带来的变化是巨大的,影响是深远的。这些技术进步是革命性的,它大大提高并拓展了人与人、人与机器甚至机器与机器之间的通信能力,并进一步挖掘了通信潜力。该文主要系统分析了3G中采用的通信新技术,并对这些新技术的应用前景进行了展望。     

无线MIMO系统的容量分析及其在3G中的应用

在无线MIMO(MultipleInputMultipleOutput)系统信号模型的基础上,分析了无线MIMO系统的容量,讨论了无线MIMO系统提高频谱利用率的基本原理,并且给出收发天线数量和信噪比对系统容量影响的试验结果。最后,对无线MIMO系统的应用,尤其在第三代移动通信中的应用做出了比较详细的说明。     

热循环对SiCp/Al复合材料性能影响的研究

SiCp/Al复合材料具有可调的热膨胀系数(CTE)、高热导率、低密度和良好的尺寸稳定性等优异性能,广泛应用于航空航天、军用电子等封装领域,由于SiCp/Al复合材料制成的组件工作环境较为苛刻,温度变化对其影响值得探讨。文章研究了热循环对SiCp/Al复合材料的CTE、热导率和弯曲强度的影响,并对其热膨胀行为作了分析。实验结果表明,热循环能有效降低SiCp/Al中的热残余应力,其热性能比铸态明显改善,弯曲强度有所降低;在低温阶段,经退火处理和退火处理+热循环处理后SiCp/Al的CTE基本重合,在高温阶段,经退火处理+热循环处理后的SiCp/Al具有更低的CTE。     

基于全景虚拟现实技术的科普系统

本文设计了基于全景虚拟现实技术的科普系统架构及功能框架.主要针对现实中的科普植物对象进3D建模,并进行三维全景展示,实现一个基于Web3D的科普系统.