填丝TIG焊接Mo—Cu合金与18-8不锈钢接头的微观组织

采用填丝钨极氩弧焊（TIG）对Mo—Cu合金与18—8不锈钢进行焊接．采用金相显微镜、扫描电镜、显微硬度计及x射线衍射仪等对Mo—Cu／18—8接头的微观组织、显微硬度、元素分布及熔合区附近的物相组成进行分析．结果表明,Mo—Cu合金侧的熔合区为马氏体和奥氏体的混合组织,焊缝和18—8钢侧的熔合区为奥氏体和铁素体双相组...     

八通道嵌入式探伤系统软件设计

介绍了一种八通道超声波探伤系统软件设计方案。嵌入式软件基于嵌入式Linux和Qt/Embedded开发,采用了层次化和模块化的设计思想。重点研究该软件系统实现的若干关键技术：利用Linux异步通知和Qt的用户事件机制,实现了驱动程序到应用程序八通道实时数据传输;利用FPGA运算与应用软件处理相结合,实现八通道实时声光报警;利用Qt的文件类库和Linux的系统调用,实现探伤文件系统等。系统运行正常,各项指标符合设计要求,性能测试表明该方案合理可行。     

Microwave dielectric properties and its compatibility with silver electrode of Li2MgTi3O8 ceramics

The effects of BaCu(B₂O₅) (BCB) additions on the sintering temperature and microwave dielectric properties of Li₂MgTi₃O₈ ceramic have been investigated. The pure Li₂MgTi₃O₈ ceramic shows a relative high sintering temperature (∼1000 °C) and good microwave dielectric properties as Q × f of 40,000 GHz, ?_r of 27.2, τ_f of 2.6 ppm/°C. It was found that the addition of a small amount of BCB can effectively lower the sintering temperature of Li₂MgTi₃O₈ ceramics from 1025 to 900 °C and induce no obvious degradation of the microwave dielectric properties. Typically, the 0.5 wt% BCB added Li₂MgTi₃O₈ ceramic sintered at 900 °C for 2 h exhibited good microwave dielectric properties of Q × f = 36,200 GHz (f = 7.31 GHz), ?_r = 26 and τ_f = −2 ppm/°C. Compatibility with Ag electrode indicates this material can be applied to low temperature-cofired ceramics (LTCC) devices.     

Au/CuMn催化剂对于C3H8还原NO催化性能的研究

以沉积-沉淀法制备了系列Au/CuMn催化剂,并对催化剂进行了XRD和XPS等表征,研究了Au负载量和催化剂焙烧温度对Au/CuMn催化剂性能的影响。实验结果显示,60℃烘干、Au理论负载量为3%的催化剂性能最佳,在50℃的反应条件下,NO的转化率达到72.4%,但催化剂失活较快。XPS分析显示,催化剂表面的Au3+与吸附氧物种Oads.是反应的活性中心,反应过程中催化剂表面氧化态Au3+与Oads.物种部分被还原,可能是催化剂失活的重要原因。另外,反应后在催化剂表面生成的亚硝酸盐、硝酸盐和碳酸盐等物种,覆盖了活性中心,也是导致催化剂失活的原因之一。     

突发8PSK信号载波同步算法研究

在时分多址(TDMA)通信网络中,由于COSTAS环会出现"悬隔效应"导致其不太适应突发方式载波恢复的解调要求。因此,提出了一种开环结构的全数字无前导字的突发8PSK解调方案。与常规算法相比,该算法可以在较低信噪比、较大载波频偏下工作,适合用于突发通信。在已有的理论基础上对算法进行了讨论,并给出了计算机的仿真结果。     

一种扩大8 mm波段综合孔径辐射计成像视场的方法

针对8mm波段综合孔径辐射计射频前端电尺寸较大,采用常规Y形阵列布局系统成像视场范围小的缺点,首先提出了一种星形天线阵列布局,它使可视度函数采样点之间的间隔变为天线单元间隔的一半,从而使系统的成像视场扩大到原来的两倍;然后,针对星形阵列可视度函数采样点缺失的问题,研究了背景对消与凸集投影相结合的图像反演算法,并进行了成像仿真。仿真结果验证了该反演算法的有效性。     

K0．8 Fe1．7 SeS超导体内的畴区形貌及三维分布研究

本文利用高角环形暗场像（HAADF）和衍衬像研究了K0．8 Fe1．7 SeS超导样品的超导畴区形貌及三维分布。在[001]带轴下观察到两类形貌的超导畴区,一类畴区尺寸为1μm左右,另一类为由几十纳米大小的小畴区组成的阵列。选区电子衍射和电子能量损失谱结果表明母体区对应Fe空位有序,而超导畴区可能对应K空位有序。STEM-EDS元素Mapping表明超导畴区边缘处K元素含量较多,K0．8 Fe1．7 SeS超导样品中可能至少存在三个相,分别为：K空位有序超导相、畴区外部Fe空位有序基体相以及两种空位有序区的过渡相。在[100]带轴下观察到了超导畴区具有连通性,构建了K0．8 Fe1．7 SeS超导样品中超导畴区的三维分布图。     

船载卫星通信地球站伺服系统硬件设计

随着通信技术的发展,卫星通信以其克服地形和自然条件限制的良好能力而越来越受到人们的青睐。但是在舰船移动时卫星天线跟踪系统的平台基准线会在方位、俯仰和横滚三个方向上发生偏移。为了解决舰船移动时稳定收发卫星信号的问题,设计了一种基于C8051F020的伺服系统。介绍了天线跟踪方式和硬件系统设计,最后实现稳定跟踪控制功能。实验结果表明,船载伺服系统对于克服载体运动带来的干扰,实现在动载体上稳定收发卫星信号具有重要的意义。     

Solvent Extraction of Heavy Lanthanides(III) with 5,7‐Dibromo‐8‐hydroxyquinoline from Aqueous Perchlorate Solution

Abstract

The extraction of Tb(III), Dy(III), Ho(III), Er(III), Tm(III), and Yb(III) with 5,7‐dibromo‐8‐hydroxyquinoline (Hdbq or HA) in chloroform from aqueous perchlorate solutions was investigated. The formation of the LnA₃ species (where Ln = Tb, Dy, Ho, Er, Tm, and Yb) in the organic phase was supported by the data. The parameters of the extraction processes were determined, and the separation factors between two adjacent lanthanides(III) were calculated.     

Contribution of Nitrated Polycyclic Aromatic Hydrocarbons in Diesel Particles to Human Lung Cancer Induction

By following the prognosis of 112 patients with carcinomas, we found that the deposition of 1-nitropyrene (1-NP), 1,3-dinitropyrene (1,3-DNP), and 3-nitrofluoranthene (3-NF) in lung tissues influenced their 5-year-survival after determination of chemicals. Lung specimens were divided into two groups of higher and lower chemical concentrations at levels of 18 pg/g for 1-NP, 15 for 1,3-DNP, and 35 for 3-NF, and the findings were statistically analyzed by adjusting for age, gender, stage, smoking status and cell type. The 5-year-survival of patients was significantly lower in the higher concentration group than the lower group. In addition, the higher concentration group correlated significantly with poor cell differentiation. The results suggest that tumors can be induced by continuous deposition of small amounts of environmental carcinogens in human lungs.

Formation of 8-hydroxyguanosine (8-OHdG) is normally used as a biomarker of oxidative damage in in vitro and in vivo systems. 8-OHdG was detected in all 22 cases of lung tissues with carcinomas, and levels increased with the increasing age of the patients, suggesting a correlation between age and the presence of diesel-originating carbon particles in lung tissues. In the inhatlacheal intratracheal administration diesel particles without most organic chemicals into mice, & OHdG formation was elevated more than by a single admummion of benzo[a]p,mne, 1-NP and 1,8-DNP. These results suggest that olbaneceous particles, but not mutagens or carcinogens, promote the formation of & OHdG, and that as a mechanism, alveolar mamphages may be assoCiated with oxidative damage, involving the generation of a hydroxyl radical during phagocytosis in the lungs.