C=0抽样方案在石英谐振器产品检验中的应用

基于质量管理体系的核心价值是以顾客为关注焦点,让顾客满意.只有为顾客提供满意的产品或服务,才能取得顾客长久的信任,保持对产品的忠诚.而实施“零缺陷”的管理和产品检验,就能将产品的质量风险降到最低,获得顾客满意,从而实现公司的经营目标.经对产品质量的分析,通过C=0的抽样方案、MIL-STD-1916抽样方案与GB/T2828.1-2003的抽样方案的实际使用和比较;突出C=0抽样方案在产品检验方面的优点;得出C=0抽样方案是目前在石英谐振器产品检验中值得推广采用的质量控制方案.     

SrFe0.6Co0.4O3催化降解孔雀石绿的研究

具有复杂分子结构的三苯甲烷类染料孔雀石绿是一种典型的较难降解染料,是工业废水处理的难点之一。本文根据Goldschmidt半径容差规则法,设计了用于孔雀石绿降解的ABO₃型SrFe_(1-x)Co_xO₃催化剂,并选择出活性较高的SrFe_0.6Co_0.4O₃催化剂。通过XRD、SEM、BET吸附及XPS分析表明:该催化剂是纯净钙钛矿结构,颗粒形貌为无规则堆叠的“蜂窝”片状;吸附等温线没有明显的回滞环,说明没有“墨水瓶”类孔结构;XPS谱中,B位离子同时存在Fe²⁺/Fe³⁺和Co²⁺/Co³⁺ 4种价态离子,且反应前后,4种离子的分布比例有较大变化。根据实验结果,推测该催化反应机理为:催化剂B位Co³⁺与溶解氧形成活性氧[O₂]⁺和Co²⁺;活性氧[O₂]⁺完成氧化反应后其正电荷转移到B位Fe²⁺上形成Fe³⁺,Fe³⁺的正电荷可再转移到Co²⁺形成Co³⁺,完成催化过程的电荷转移与循环。     

基于DOE的加氢裂化柴油95%点参数优化

依托某公司加氢裂化装置,通过Minitab软件建立拟合回归模型,以柴油95%点(95%回收温度)作为响应值,考察了17个可控的或间接可控的影响因素对柴油产品质量的影响,从中筛选出6个主要效能因子并建立了柴油95%点与主要效能因子间的响应面方程。通过响应优化器确定了柴油95%点为360.5℃时的操作条件:柴油热回流量为49.5 t/h,柴油灵敏板温度为329℃,喷气燃料抽出温度为228℃,喷气燃料塔底温度为223℃,喷气燃料返塔温度为200℃,喷气燃料中段量为115 t/h,确定了操作参数的优先级及操作水平,实现了操作的科学性。     

钴氮共掺杂碳基电催化剂的制备及性能调控

贵金属基电催化剂是促进燃料电池及金属-空气电池技术发展的关键材料,然而,其单一的氧还原/氧析出催化功能及高昂的制备成本制约了其推广应用。为此,开发低成本、高效的非贵金属双功能电催化剂至关重要。以核壳金属有机框架（MOFs）为前驱体,通过高温煅烧法制备具有核壳结构、高催化活性、高导电性的钴/氮共掺杂碳基电催化剂（Co/Co₃O₄@NGC）。结果表明：煅烧温度是影响电催化剂微纳结构、物化组成和催化活性的关键因素,最佳烧结温度为900℃;制备的电催化剂（Co/Co₃O₄@NGC-900）具有清晰的核壳结构和3D十二面体形貌,微表面遍布Co/Co₃O₄纳米颗粒和Co-N_x位点。同时,Co/Co₃O₄@NGC-900有机地结合了多元活性成分（如活性Co/Co₃O₄纳米颗粒、Co-N_x及N掺杂）和高度石墨化碳基底的共同作用,具备高效的氧还...     

基于外点检测的加权k-means算法

为解决k-means聚类算法中异常样本点破坏数据分布,致使簇中心发生较大偏差的问题,通过计算样本点与潜在簇中心的距离赋予样本点不同的权重,降低外点对数据分布的影响,并通过对权重向量施加₀-norm范数在聚类模型中自适应移除外点. 采用交替最小化优化算法求解模型,在人工合成数据集和真实数据集上的实验表明,所提模型能有效降低外点对聚类的影响,可得到更有效的聚类效果.     

MCNP模拟钴-60辐照装置空间剂量场

为模拟辐照室中辐照工位外的周围空间剂量场分布,采用蒙特卡罗粒子输运程序MCNP建立钴-60辐照装置模型。以单板源架中心点为坐标原点的笛卡尔坐标系,考虑钴-60源的γ射线非自吸收和自吸收两种情况,研究坐标轴方向上每隔10 cm间距的空气平面的剂量率和坐标轴上剂量率的变化规律。结果表明,辐照室中辐照产品占满辐照工位的情况下,周围空间剂量场空气面剂量率整体较小;单板源架中心坐标轴上的剂量率变化规律更符合二项式拟合函数。在钴-60源γ射线自吸收情况下,单板源架端面坐标轴附近的空气面剂量率明显偏小,且随着空气面远离单板源架,空气面上的高剂量率区域向两侧移动;在钴-60源γ射线非自吸收情况下,单板源架端面处的空气面高剂量区域始终位于坐标轴附近。MCNP理论模拟计算分析对于利用钴-60辐照装置辐照工位外的周围空间剂量场具有重要的实际指导意义。     

Detailed thermodynamic characterization of hermetic reciprocating compressors

The aim of this paper is the detailed analysis of different well-known thermodynamic efficiencies usually used to characterize hermetic compressors. Attention is focussed on the volumetric efficiency, the isentropic efficiency, and the combined mechanical–electrical efficiency. A procedure is presented to detach these efficiencies into their main components (physical sub-processes) to get deeper insight on the overall behavior.The volumetric efficiency is split into partial efficiencies related to pressure drop and heat transfer effects, supercharging effects, superdischarging effects, leakages, etc. The isentropic efficiency is detached using two different points of view: the work associated to the individual sub-processes (compression, discharge, expansion, suction), and the work associated to the underpressures, overpressures, and between the inlet and outlet mean compressor pressures. Finally, the combined mechanical–electrical efficiency is related to the heat transfer losses/gains, and to the exergy transfers and exergy destroyed.Even though some of the concepts introduced in the paper can be applied to different kinds of compressors, the discussion is specially focussed on hermetic reciprocating compressors. An advanced simulation model developed by the authors has been used to generate data to illustrate the possibilities of the detailed thermodynamic characterization proposed. The criteria developed are useful tools for comparison purposes, to characterize compressors, and to assist designers during the optimization process.     

Spacer defined FinFET: Active area patterning of sub-20 nm fins with high density

We present a method to obtain Si-fins with a critical dimension (CD) below 20 nm, separated by a minimum distance of 25 nm and connected by a common source/drain (S/D) pad. The method comprises of recursive spacer defined patterning to quadruple the line density of a 350 nm pitch resist pattern defined by 193 nm lithography. Spacer defined patterning is combined with resist based patterning to simultaneously define fins and S/D pads in a Silicon on Insulator (SOI) film. CD and Line Width Roughness (LWR) analysis was done on top down SEM images taken in a center die and in an edge die of a 200 mm wafer. The average CD is 17 nm in the center of the wafer and 18 nm at the edge. The LWR is 3 nm for both center and edge. Additional process steps to remove etch damage and round the top corner of the fin (i.e. oxidation followed by H₂ anneal) further reduce the CD to 13 nm.     

Cell Cycle Control in Eukaryotes: A BioSpi model

This paper presents a stochastic model of the cell cycle control in eukaryotes. The framework used is based on stochastic process algebras for mobile systems. The automatic tool used in the simulation is the BioSpi. We compare our approach with classical ODE specifications.     

PI实时数据库系统在石油化工生产管理中的应用

在石油化工生产中,过程信息管理系统的核心是实时数据库,它是连接生产装置控制层和企业管理层管理信息的桥梁和纽带。实时系统的采用可以为最终用户提供快捷、准确的工厂信息,增进产品的质量、减少设备瓶颈、提高产量、降低生产成本。