A procedure to prepare cross-sectional samples for TEM

Cross-sectional transmission electron microscopy (XTEM) is an imaging technique particularly suited to the study of layered structures. For integrated electronic devices it has become a common practice to use XTEM to assess the shape and crystallinity of component layers as well as defect structures introduced by processing. A procedure for preparing samples to be viewed by XTEM is described.     

Metathesis as a versatile tool in oleochemistry

Olefin metathesis, awarded with the Nobel Prize in Chemistry 2005 for Chauvin, Grubbs and Schrock, has emerged as a powerful tool for organic as well as polymer chemistry. In oleochemistry, this reaction is well known and has been applied for many decades. Examples include the functionalization of the double bonds of different oleochemicals or the (direct) polymerization of plant oils via metathesis. More recent developments, particularly the development of better and more robust catalysts, allow for highly efficient cross‐metathesis reactions opening new possibilities for the direct introduction of chemical functionalities. Within this contribution, the development of metathesis in oleochemistry will be discussed, covering self‐metathesis as well as more recent developments in the field of cross‐metathesis that lead to desired platform chemicals.     

冷轧厂酸洗机组3号横剪大流量中高压液压系统设计方案探讨

在宝钢２０３０ｍｍ冷轧厂酸洗机组中，为了满足厚规格ＩＦ钢的生产，拟将原有的气动式剪切机改成液压式剪切机。为此，设计了一套中高压大流量的液压系统以满足３号横剪大剪切力（最高达７００ｋＮ）和快速剪切（３秒／次）的需要。由于采用了蓄能器增速回路和二通插装阀控制技术，使该液压系统较传统的剪切机液压系统具有响应速度快、体积小、重量轻、发热少和降低电机能耗等优点。     

堤身的数据采集及断面设计的几点建议

针对堤防设计的基础资料采集和设计优化，提出了一些合理性建议。     

Data requirements for neutron activation: Part I: Cross sections

Existing neutron cross section libraries such as EAF-2003 contain a large number of reactions. Of these only a small proportion are significant in the production of the nuclides that dominate activation quantities such as activity or γ-dose rate at various decay times. These reactions were identified in a recent extensive set of calculations on all the elements and reported in the ‘Activation Handbook’. These 1340 reactions are considered here and the set of reactions with no differential or integral data are listed and prioritised. A set of 339 reactions with very limited possibility of measurement are given; these require further study by theoretical calculations. A set of 100 reactions with either discrepant or no data, that might be measurable are listed and are recommended to be the subject of future experimental work.     

IRS-P6 LISS-3和Landsat-5 TM两种多光谱传感器影像数据的对比分析

随着载有各种新型传感器的卫星相继发射升空,不同传感器之间的相互比较成了一个研究热点。首先从传感器的轨道特征、光谱范围等方面对IRS-P6 LISS-3和Landsat-5 TM进行了机理方面的对比分析,选取3对同日过空的遥感影像,研究了IRS-P6 LISS-3和Landsat-5 TM遥感数据在可见光-近红外、短红外各对应光谱波段之间的关系,建立TM和LISS-3各波段之间的相互转换公式,与Chander等提出的转换公式进行对比分析。结果表明:实际TM和模拟TM多光谱数据之间具有较强的相关关系,决定系数R²均大于0.97;模拟TM与实际TM的水体指数(MNDWI)和归一化植被指数(NDVI)空间散点分布和实际LISS-3与实际TM的空间散点分布相比,具有更强的相关关系,其决定系数R²有一定提高,散点分布趋于对称。因此,所求的关系转换方程具有较高的精度和有效性,效果优于Chander等提出的转换公式。     

Traditional organizations and crisis management in transition—Organizational perspectives on new dynamics of independent civil engagement

Digitalization and the trend towards more short‐term and project‐oriented social engagement have had a direct impact on traditional crisis management. This societal change has supported the evolution of new types of volunteers who use low‐threshold potentials to organize and maintain support independently. Traditional institutions like the German Red Cross are challenged to deal with these rapid changes regarding their own organizational culture in relation to the new phenomenon of so‐called unaffiliated volunteers. This paper investigates how unaffiliated volunteers influence and change the organizational culture of German disaster management by analysing and reflecting organizational adaptation processes in the aftermath of the German floods in 2013, the storm events in the west of Germany in 2014 and the refugee relief mission in 2015–2016. Therefore, semi‐structured interviews with experts of the German Red Cross were held to analyse their reactions towards unaffiliated Volunteers during the Floods in 2013 and the refugee relief missions, and further focus group interviews were conducted to validate the extracted results. Findings suggest that among professionals and leading entities in the German Red Cross, a process of rethinking has emerged, recognizing the importance and necessity to open up organizational structures for the collaboration and coordination of unaffiliated volunteers.     

Entropy/cross entropy-based group decision making under intuitionistic fuzzy environment

We study the group decision making problem under intuitionistic fuzzy environment. Based on entropy and cross entropy, we give two methods to determine the optimal weights of attributes, and develop two pairs of entropy and cross entropy measures for intuitionistic fuzzy values. Then, we discuss the properties of these measures and the relations between them and the existing ones. Furthermore, we introduce three new aggregation operators, which treat the membership and non-membership information fairly, to aggregate intuitionistic fuzzy information. Finally, several practical examples are presented to illustrate the developed methods.     

塑料充模流动粘性模型研究

对多种塑料在不同温度下的剪切速率一稳态剪切粘度数据进行Cross粘性模型参数拟合，得到了表征材料粘度的模型参数(B，Tb，τ^*，n)。其拟合效果良好，能较准确地描述塑料熔体在一定剪切速率和温度范围内的粘流特性，为工程计算和塑料熔体模流分析提供了数据支持。结果表明，该方法有较广泛的适用性。     

优化SVR的加权马尔可夫链用电量预测

研究电力系统中用电量的准确预测问题.由于影响用电量的因素众多,并且用电量数据与相关因素之间呈现高度的非线性关系,传统的预测方法很难捕捉用电量的变化趋势,预测精度较低.为了提高预测的精度,提出了一种马尔可夫链优化的SVR模型.上述模型根据支持向量回归机原理,以网络搜索交叉验证的思想优化模型参数,通过加权马尔可夫链原理优化预测结果,将原来的数值预测转化为概率区间上的预测.同时,在利用加权马尔可夫链的预测信息之后,也提高了预测的精度.最后,将改进模型应用于江苏省全社会用电量的预测分析,实验结果表明优化的支持向量模型优于其它对比模型,有较高的泛化能力和预测精度.