Repeatability and Reproducibility techniques for the analysis of measurement systems

This research was conducted with the aim of analyzing two of the main metrological characteristics of any measurement system: Repeatability and Reproducibility. Both of these features play an important role in the analysis of the measurements and they can give us a lot of information about who and what influences any measuring system. The analysis of Repeatability and Reproducibility is generally carried out through the use of the study Gage R&R. This study permits to understand which are the decisive factors in a measurement system, and, definitively, if the process is stable, that is under statistical control or out of statistical control.     

A robust design to reduce variability in glass container inspection

This article presents research efforts made to assist a Fortune 500 glassmaker in reducing the variability of its automated visual inspection systems in assessing product quality. Through interviewing line workers, engineers and managers, and direct observations of the inspection process possible causes leading to large variability observed in the inspection process were identified. Responding to these findings, solutions related to equipment setup, job changes, and operational procedures were suggested in order to minimize the inspection process variations as well as to improve the replicability of the inspection stations. Additionally, a unique statistical experiment was conducted to analyze how three factors (namely, operator, defect size, and threshold value used) would affect the mean of the defective ratio. A robust design aiming at controlling these variations was then given to optimize the system's performance.     

Efficient separation of (R)‐(‐)‐mandelic acid biosynthesized from (R,S)‐mandelonitrile by nitrilase using ion‐exchange process

BACKGROUND: (R)‐(‐)‐Mandelic acid (R‐MA) is an important intermediate and chiral regent with broad uses. An efficient method for the separation of R‐MA from the bioreaction mixture with high yield is of great importance, thus, the main objective of this work is to investigate the recovery of R‐MA using an ion‐exchange process. RESULTS: The equilibrium isotherms for the separation of R‐MA by resin HZ202 were obtained in the pH range 5.0–9.0 and temperature range 25–35 °C. The equilibrium data are well fitted by the Langmuir isotherm. Batch kinetic experiments showed that the mobility of R‐MA^? in solution was rapid and the R‐MA^?/OH^? ion‐exchange process reached equilibrium after about 60 min. Adsorption kinetics were analyzed by a linear driving force mass‐transfer model, yielding good prediction of the kinetic behavior. In fixed bed column experiments, the breakthrough curves of R‐MA from the solution on resin HZ202 were determined at different flow rates and R‐MA was eluted with different concentrations of HCl. A favorable breakthrough curve and optimal eluant concentration were obtained. The results were used for the separation of R‐MA biosynthesized from (R,S)‐mandelonitrile with nitrilase, and separation was successfully achieved with above 90% recovery yield. CONCLUSION: Resin HZ202 presents favorable behavior for the recovery of R‐MA, in terms of capacity, kinetics, affinity, and susceptibility to regeneration. The results of this study provide an efficient method for R‐MA recovery from bioreaction mixture and could potentially be used in industry. Copyright © 2010 Society of Chemical Industry     

Metacognitive control over the distribution of practice: When is spacing preferred?

The authors clarify the source of a conflict between previous findings related to metacognitive control over the distribution of practice. In a study by L. Son (2004), learners were initially presented pairs of Graduate Record Examination (GRE) vocabulary words and their common synonyms for 1 s, after which they chose to study the pair again immediately (massed practice), later (spaced practice), or not at all (done). Learners chose spaced practice less as pair difficulty increased. A. S. Benjamin and R. D. Bird (2006), using different materials and procedures and a longer presentation duration (5 s), concluded just the opposite. The authors adopted Son’s materials and procedures and replicated her findings with a 1-s stimulus duration. However, the declining choice of spacing as item difficulty increased largely reflected learners’ failure to fully perceive items with brief presentations. With longer presentations, ensuring full perception, the choice of spaced practice increased with greater pair difficulty, in agreement with Benjamin and Bird. Theoretical implications are discussed in the context of discrepancy-reduction and proximal-learning perspectives. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

基于MSP430单片机半平衡桥RLC测量仪设计

介绍了一种基于 MSP430 单片机的 RLC 测量仪的设计与实现.测量仪采用MSP430单片机为中心控制器,用未知元 件(R,L,C)与基准电阻串联作为一个半桥,MDAC TLC7524 作为另一个半桥,MSP430 单片机控制 DDS 芯片 AD9851 产生频率 可调的驱动信号驱动这两个并联的半桥,通过单片机调节...     

NUTRIOSE(R)06,不仅仅是一种膳食纤维NUTRIOSE(R)06的肠道生态系统益处和技术功效回顾——为了更健康更美味的配方

Nutriose(R)06是Roquette公司独家生产的一种可溶性膳食纤维,已经纳入中国"公共营养改善Oligo+计划"批准为一种益生元产品;Nutriose(R)06不但体现更健康的营养部分,而且有卓越的健康益处尤其是肠道健康;这篇文章将回顾Nutriose(R)06的益生元功效以及耐受性,技术功效.     

Performance of heat pumps charged with R170/R290 mixture

In this study, thermodynamic performance of R170/R290 mixture is measured on a heat pump bench tester in an attempt to substitute R22. The bench tester is equipped with a commercial hermetic rotary compressor providing a nominal capacity of 3.5 kW. All tests are conducted under the summer cooling and winter heating conditions of 7/45 °C and −7/41 °C in the evaporator and condenser, respectively. During the tests, the composition in R170/R290 mixture is varied from 0% to 10% with an interval of 2%. Test results show that the coefficient of performance (COP) and capacity of R290 are up to 15.4% higher and 7.5% lower, respectively than those of R22 for two conditions. For R170/R290 mixture, the COP decreases and the capacity increases with an increase in the composition of R170. The mixture of R170/R290 mixture at 4%/96% composition shows the similar capacity and COP as those of R22. For the mixture, the compressor discharge temperature is 17–28 °C lower than that of R22. For R170/R290 mixture, there is no problem with mineral oil since the mixture is composed of hydrocarbons. The amount of charge is reduced up to 58% as compared to R22. Overall, R170/R290 mixture is a good long term ‘drop-in’ candidate from the view point of energy efficiency and greenhouse warming to replace R22 in residential air-conditioners and heat pumps.     

Experimental investigation of a direct driven radial compressor for domestic heat pumps

The presence of oil in domestic heat pumps is an obstacle toward higher efficiency, particularly for enhanced surface evaporators and for advanced concepts based on two-stage cycles. Very compact direct driven radial compressors supported on oil-free bearings represent a promising alternative. This paper presents the derivation of the specifications, the choice for an appropriate refrigerant fluid and the design of a proof of concept prototype with the various tradeoffs between the impeller characteristics to follow the seasonal heat demand, the bearing and rotordynamics for a stable operation. Heat pump simulation results, the design of the impeller as well as the layout of the experimental facility and first experimental results are presented. An impeller with a tip diameter of 20 mm has been tested at rotational speeds of up to 210 krpm reaching pressure ratios in excess of 3.3 and efficiencies above 78%. The refrigerant chosen for this first experimental approach is HFC 134a.