化学镀Ni—P镀层的X射线衍射研究

根据X射线衍射分析结果,对化学镀高P(含P>11wt％或19at％)Ni-P镀层加热时效时,镀层成分和加热温度对结构转变的影响作了研究,结果表明,高P共晶、过共晶(含P>11wt％或19at％)合金的结构转变有如下特征:(1)相同加热时效条件下,Ni-P合金的结构转变与成分有密切关系:(2)对同一成分的过共晶合金,Ni-P合金的结构转变与时效温度密切相关;(3)过共晶合金在290～360℃温度范围内时效处理,出现Ni_xP_y介稳相,X射线衍射分析认为Ni_xP_y为Ni_(12)P_5。     

智能化红外焊缝检测仪的实时信号自相关分析

详细介绍了在改进红外焊缝检测仪的过程中实时信号的一种抗干扰方法－－自相关方法。重点离自相关方法的数学模型，软件框图及设计思想，并给出了实验结果。     

石英砂的相变与换向器套筒铸件的变形

用呋喃树脂石英砂工艺生产牵引电机换向器套筒出现变形、裂纹等铸造缺陷,是由石英砂相变膨胀引起,后用高铬刚玉砂代替石英砂得到解决.     

高岭土在碳热还原氮化过程中的相变

系统研究了苏州高岭土碳热还原氮化合成SiAlON过程在不同温度下的相变。对试样的XRD、SEM以及EDXA分析结果表明 ,1 30 0℃之前 ,试样中没有氮化物生成 ,物相为莫来石、石英和方石英 ;1 30 0℃时 ,高岭土开始发生氮化反应 ,生成过渡型SiAlON和β SiAlON。此时 ,石英和方石英相基本消失 ;1 4 0 0℃时 ,过渡型SiAlON、β SiAlON和X SiAlON三相共存 ,β SiAlON有所增多并有少量刚玉相生成 ;从 1 4 50℃到 1 550℃ ,Z值为 3的β SiAlON成为惟一的氮化产物 ,与少量SiC和刚玉相并存。莫来石在 1 50 0℃时完全消失     

Catalytic properties of aluminated sepiolite in ethanol conversion

The aluminated sepiolite, obtained by alkaline treatment with KAlO₂, as well as the silver-exchanged aluminated sepiolite were tested in ethanol conversion. The reactions were performed at 280°C and with 50 Torr of ethanol in He. After the alumination through KA1O₂, ethanol dehydrogenation and ethanol dehydration resulted from the Lewis acidity. The dispersion of silver led to a bifunctional catalytic system and the overall catalytic activity and the selectivity towards the acetaldehyde production increased. As a result of the Prins reaction, a significant yield in butadiene was observed.     

实时数据仓库中一种改进的数据流更新算法

为实现数据仓库中数据的高效集成,针对数据偏斜分布现象,提出一种改进的数据流更新算法EH-JOIN。该算法对传统散列连接方法进行改进,利用索引将部分频繁使用的主数据存储在内存中,解决了高速数据流下的磁盘频繁访问问题。实验结果表明,与MESHJOIN算法和R-MESHJOIN算法相比,EH-JOIN算法的服务速率在磁盘存储关系集保持适当大小时分别提高了96%和81%,在内存大小不同时提高了57%和48%。     

基于线性动态系统稀疏编码的异常事件检测

线性动态系统模型结合稀疏编码实现异常事件检测。线性动态系统可有效地捕捉动态纹理在时间和空间的转移信息,描述视频的时空小块。然而,线性动态系统属于非欧氏空间,无法直接用传统的稀疏编码进行异常检测。基于约束凸优化公式,将相似性变换与稀疏编码结合,可实现线性动态系统稀疏编码的优化求解。实验表明,所提出的方法具有更好的性能。     

Crystallization and phase transformation kinetics of poly(1-butene)/MWCNT nanocomposites

Poly(1-butene)/MWCNT nanocomposites were prepared by simple melt processing technique. Crystallization, crystal-to-crystal phase transformation and spherulitic morphology were studied using differential scanning calorimetry (DSC), wide angle X-ray diffraction (WAXD) and optical microscopy (OM). The non-isothermal crystallization exhibited higher values of Z_t derived from Avrami theory and lower values of F(T) obtained from Avrami-Ozawa analysis, while the isothermal crystallization revealed a significant increase in crystallization temperatures and lower crystallization half times compared to pristine PB. The observed changes in the crystallization kinetics were ascribed to the enhanced nucleation of PB in the presence of MWCNT. The nucleating activity calculated from the non-isothermal crystallization data revealed that the MWCNTs provide an active surface for the nucleation of PB. The optical micrographs exhibited significantly smaller crystallites with disordered morphology for the nanocomposites compared to the well defined spherulitic morphology for pristine PB. The rate of phase transformation from kinetically favored tetragonal to thermodynamically stable hexagonal form was noticeably enhanced as evidenced by the reduction in the half time for phase transformation from 58 h to 25 h for PB reinforced with 7% MWCNT.     

小波变换在求解重力测定反问题中的应用

针对重力测定反问题,提出将其离散为线性不适定问题,利用小波变换方法进行数值求解.该方法将小波变换和正则化方法相结合,选取小波函数作为一组基底,将原不适定问题转化为粗子空间上的适定问题,并给出选取粗子空间基的方法.通过数值模拟已有方法和小波变换方法求解结果的比较,表明了小波变换方法的可行性和有效性.     

浅议高职院校科研成果转化问题

当前,高职院校科研工作发展迅速,但是往往"重研究,轻应用",科研成果转化数量少,这是一种资源的浪费。高职院校科研成果转化具有重要的现实意义,应该得到大力发展。文章分析了当前高职院校科研成果转化存在的问题,提出了促进高职院校科研成果转化的对策建议。