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991.
992.
Poly(acrylamide‐co‐maleic acid) [P(AAm/MA)] hydrogels, with various compositions, were prepared from ternary mixtures of acrylamide (AAm)/maleic acid (MA)/water by using 60Co γ‐rays. The effect of composition of these hydrogels, on the competitive removal of Pb2+, Cd2+, and Zn2+ ions from aqueous solution, was investigated. The hydrogel compositions and their adsorption behaviors were determined by use of differential pulse polarography, a very sensitive electroanalytical technique. It was observed that the external stimuli of pH, temperature, and ionic strength have an important role on the adsorption. The increments of MA content in P(AAm/MA) hydrogels caused a significant increase in the adsorption these ions. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 94: 2401–2406, 2004 相似文献
993.
Vulcanizates of blends of ethylene–propylene–diene rubber and polyamide copolymers were prepared by reactive compatibilization. A reactive route was employed for compatibilizing these blends with the addition of chlorinated polyethylene (CPE). The influence of the compatibilizers, crosslinking agents, blend compositions, and addition modes of the compatibilizers on the mechanical properties of the blends was investigated. The morphologies of the blends were determined with scanning electron microscopy. The addition of CPE was found to reduce the particle size of the dispersed phase remarkably. The stability of the blends with compatibilizers was measured by high‐temperature thermal aging. The mechanical properties were examined by stress–strain measurements and dynamic mechanical thermal measurements; the addition of polyamide copolymers caused significant improvements in the tensile properties of these blends.© 2003 Wiley Periodicals, Inc. J Appl Polym Sci 89: 1727–1736, 2003 相似文献
994.
由于子区域分割粒度的限制,基于阶次序列的定位算法(Sequence-based localization,SBL)存在边缘区域节点定位误差较大和不能保证平均定位误差性能的问题。针对这些问题,提出了一种基于SBL和APIT的混合定位算法,利用APIT信标三角形切割SBL算法子区域,减小子区域面积,实现了分割粒度的细化。通过预先进行系统训练,优化了混合算法的加权系数,进一步提升了算法的定位精度。仿真结果表明,相比于原算法,所提出的混合算法有效地提升了边界区域节点的定位精度,其平均定位误差降低了17.9%,使基于阶次序列的定位算法的定位精度得到了有效改善。 相似文献
995.
目的 选择固相金属亲和层析柱的金属离子,以优化分离纯化重组戊型肝炎病毒包涵体的条件。方法 在同一试验条件下用4种金属离子柱分离纯化目的蛋白。结果 包涵体经不同离子柱层析时目的蛋白的收获率、纯度、洗脱条件各异。结论 镍离子柱纯化效果最佳。 相似文献
996.
Tsugio Sato Kenji Dosaka Toshiaki Yoshioka Akitsugu Okuwaki Kazuo Torii Yoshiro Onodera 《Journal of the American Ceramic Society》1992,75(3):552-556
Amorphous CeO2 –ZrO2 gels were prepared by coprecipitation in ammonia solutions. The onset of crystallization of the gels, from calcining in air, was 420°C, while 200° to 250°C in the presence of water and organic solvents such as methanol and ethanol. The sintering behaviors of CeO2 –ZrO2 powders were sensitive to the crystallizing conditions, since hard agglomerates formed when the precipitated gels were crystallized by normal calcination in air, whereas soft agglomerates formed when they were crystallized in water or organic solvents. CeO2 –ZrO2 powders crystallized in methanol and water at 250°C were sintered to full theoretical density at 1150° and 1400°C, respectively, whereas that crystallized by calcination in air at 450°C was sintered to only 95.2% of theoretical density, even at 1500°C. 相似文献
997.
以聚乙二醇-4000钾盐为引发剂.合成了食不同长度聚醚链段的聚D.L-乳酸-聚乙二醇-聚D.L-乳酸(PLA-PEG-PLA)三嵌段共聚物。考察了溶剂用量、引发剂用量、反应温度和时间、PEG分子量、不同溶剂对聚合反应的影响。以1H-NMR、IR、DSC、GPC对共聚物进行了表征。 相似文献
998.
Blends of polypropylene (PP) and thermoplastic elastomers (TPE), namely SBS (styrene‐butadiene‐styrene) and SEBS (styrene‐ethylene/1‐butene‐styrene) block copolymers, were prepared to evaluate the effectiveness of the TPE type as an impact modifier for PP and influence of the concentration of elastomer on the polymer properties. Polypropylene homopolymer (PP‐H) and ethylene–propylene random copolymer (PP‐R) were evaluated as the PP matrix. Results showed that TPEs had a nucleating effect that caused the PP crystallization temperature to increase, with SBS being more effective than SEBS. Microstructure characterization tests showed that in most cases PP/SEBS blends showed the smallest rubber droplets regardless of the matrix used. It was seen that SEBS is a more effective toughening agent for PP than SBS. At 0°C the Izod impact strength of the PP‐H/SEBS 30% b/w blend was twofold higher than the SBS strength, with the PP‐R/SEBS 30% b/w blend showing no break. A similar behavior on tensile properties and flexural modulus were observed in both PP/TPE blends. Yield stress and tensile strength decreased and elongation at break increased by expanding the dispersed elastomeric phase in the PP matrix. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 95: 254–263, 2005 相似文献
999.
1000.
A polymer electrolyte based on microporous poly(vinylidene fluoride-co-hexafluoropropane) (PVdF-HFP) film was studied for use in lithium ion batteries. The microporous PVdF-HFP (Kynar 2801) matrix was prepared from a cast of homogeneous mixture of PVdF-HFP and solvents such as ethylene carbonate (EC), dimethyl carbonate (DMC), and ethyl methyl carbonate (EMC). After evaporation of DMC and EMC, a sold film of the PVdF-HFP and the EC mixture was obtained. EC-rich phase started its formation in the PVdF-HFP/EC film at EC content of about 60 wt.% based on the total weight of PVdF-HFP and EC. The formation of the new phase resulted in the abrupt increase of the porosity of the PVdF-HFP matrix from 32 to 62%. The ionic conductivity of the film soaked in 1 M LiPF6-EC/DMC=1/1 was significantly increased from order of 10−4 S/cm to order of 10−3 S/cm at the EC content of 60 wt.%. Thermal and spectroscopic investigations showed that most of the EC interact with PVdF-HFP with the EC content being below 60 wt.%. MCMB/polymer electrolyte/LiCoO2 cells employing the microporous PVdF-HFP polymer film showed stable charging/discharging characteristics at 1C rate and good rate capability. 相似文献