Encapsulation and Ostwald Ripening of Au and Au–Cl Complex Nanostructures in Silica Shells

We report a general template strategy for rational fabrication of a new class of nanostructured materials consisting of multicore shell particles. Our approach is demonstrated by encapsulating Au or Pt nanoparticles in silica shells. Other superstructures of these hollow shells, like dimers, trimers, and tetramers can also be formed by nanoparticle‐mediated self‐assembly. We have also used the as‐prepared multicore Au–silica hollow particles to perform the first studies of Ostwald ripening in confined microspace, in which chloride was found to be an efficient mediating ligand. After treatment with aqua regia, Au–Cl complex is formed inside the shell, and is found to be very active under in situ transmission electron microscopy observations while confined in a microcell. This aspect of the work is expected to motivate further in situ studies of confined crystal growth.     

高分散度Pt/C电催化剂的制备

Cabot公司Vulcan XC-72型炭黑，经过H2O2氧化处理后作为Pt的载体，H2PtCl6作为金属前驱体制备了高度分散的Pt/C催化剂。讨论了不同条件下H2PtCl6在炭黑上的吸附性能。载体经过H2O2氧化处理24h,H2PtCl6在pH=9下吸收48h，H2 350℃还原2h，可以制备出铂晶粒平均大小为1.8nm的Pt/C电催化剂。     

Anatase Sol Prepared from Peroxotitanium Complex Aqueous Solution Containing Niobium or Vanadium

Niobium- or vanadium-doped anatase sols were prepared by hydrothermal treatment of 0.1 mol/dm³ peroxotitanium complex aqueous solutions dissolving 0–10 mol% niobium or vanadium at 100°C for 8 h. Niobium-doping caused the increase of lattice constants of anatase and the shape change of anatase crystal from spindle-like to cubic-like structure, but no change of the optical absorbance. Vanadium-doping caused the decrease of lattice constant of c -axis, the miniaturization of anatase crystal and the increase of optical absorbance at the wavelength from 350–700 nm.     

DS90C363/DS90CF364 LVDS发送/接收器在数字RGB液晶屏上的应用

通过在FPD铁路上使用LVDS技术可使具有数字RGB接口的液晶显示屏的工作距离大大增加。文章通过一个具体应用环境介绍了21位LVDS发送器/接收器DS90C363/DS90CF364传输套片的主要特性、引脚功能、工作原理，同时指出了在具体设计使用时的注意事项。     

实时操作系统DSP/BIOS在DSP开发中的应用

本文介绍了RTOS(实时操作系统)DSP／BIOS在DSP的开发设计中的应用。在简述了DSP的一般模型后，论述了RTOS在DSP／BIOS外设管理，实时性能分析以及程序流程控制中的应用。     

Thaumasite––direct, woodfordite and other possible formation routes

Two main formation routes for thaumasite exist below 15 °C. One is the direct route from C–S–H reacting with appropriate carbonate, sulfate, Ca²⁺ ions and excess water. The other route is the woodfordite route from ettringite reacting with C–S–H, carbonate, Ca²⁺ ions and excess water, in which thaumasite arises through the intermediate formation of the solid solution woodfordite. The woodfordite route for thaumasite formation appears to be relatively quicker (although still slow) than the direct route, presumably because with the former the ettringite already has the octahedral [M(OH)₆] units that can facilitate the critical change from [Al(OH)₆]³⁻ to [Si(OH)₆]²⁻ groupings. Both routes are mutually dependent on each other. The presence of magnesium salts can modify the path to thaumasite formation. High pressure might be able to stabilise [Si(OH)₆]²⁻ groupings and allow thaumasite to become formed above 15 °C. This possibility is discussed.     

Windows2000设备驱动程序即插即用的实现

概述了Windows2000即插即用系统组成及其实现过程,结合实例介绍了Windows2000设备驱动程序如何支持用户即插即用的功能。     

CDMA 1x EV-DO覆盖模型的分析与仿真

结合经过校正后的适合于本地无线环境的OKUMURA-HATA传播模型，建立起一种新的本地化基于1x EV—DO系统数据业务吞吐量分析的覆盖预测仿真模型，可应用于1xEV—DO系统的网络规划及系统性能分析。     

一种适合∑-△A／D转换器的FIR数字滤波器

讨论了一种用于∑-△A／D转换器的固定系数半带（half-band）FIR数字滤波器，分析了其线性相位特性和低通滤波特性，给出了频率仿真结果，以及在Cadence设计系统中的电路和版图实现。     

印制电路板翘曲弓形的模具整平法

当PCB板发生翘曲,用常规方法整平仍达不到出货要求时,推荐采用弓形模具进行整平。