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71.
Analysis of characteristic odors from human male axillae   总被引:7,自引:0,他引:7  
A number of studies concerning the analysis of axillary odors have assumed that the characteristic odor produced in the axillae is due to volatile steroids and isovaleric acid. Organoleptic evaluation of Chromatographic eluants from axillary extracts was employed to isolate the region in the chromatogram where the characteristic odor eluted. The odor of the dissolved eluant was eliminated when it was treated with base, suggesting that acids make up the characteristic axillary odor. Subsequent extraction of the pH-adjusted axillary extract in conjunction with organoleptic evaluation of the Chromatographic eluant, preparative gas chromatography, and analysis by GC-MS as well as GC-FTIR showed the presence of a number of C6 to C11 straight-chain, branched, and unsaturated acids as important contributors to the axillary odor. The major odor component is (E)-3-methyl-2-hexenoic acid. Three homologous series of minor components are also important odor contributors; these consist of the terminally unsaturated acids, the 2-methyl-C6 to -C10 acids and the 4-ethyl-C5 to -C11 acids. These types of acids have not been reported previously as components of the human axillary secretions and have not been proposed previously as part of the principal odor components in this area.  相似文献   
72.
The humidity response characteristics of La doped BaTiO3 with different sintered densities and room temperature electrical conductivities were investigated using complex impedance measurement. The samples with low density and high resistivity showed the large and nearly linear sensitivity to the change of humidity. The impedance spectra of samples, when exposed to high humidity, can exhibit microstructure-related features, even though they do not give rise to a noticeable characteristic change when exposed to low humidity. The observed impedance patterns were dependent upon the density, and hence the oxidation kinetics of BaTiO3.  相似文献   
73.
定量电子晶体学硼对Ni3Al的电荷密度分布的影响   总被引:1,自引:0,他引:1  
朱静 《材料研究学报》1997,11(6):639-648
阐述了定量电子晶体学测定晶体电荷密度分布的基本原理和方法,不足之处和改善途径。以硼对Ni3Al的电荷密度分布的影响为实例,介绍了定量电子晶体学在研究晶体电子结构方面的应用前景。  相似文献   
74.
The chemical reaction between lanthanum oxide and molybdenum carbide was studied by thermodynamic calcu-lation, thermal analysis and in-situ X-ray Photoelectron Spectroscopy. The theoretical results show that at the environment allowing for the evaporation of lanthanum, such as in high vacuum, La2O3 in the La2O3-Mo materials can be reduced to metallic lanthanum by molybdenum carbide (Mo2C). To confirm the conclusion, many analysis methods such as XRD, SPS, and TG-DTA were taken. The experimental results show that the chemical state of lanthanum changes during heat-ing. It was proved, for the first time, that reacted metallic lanthanum appears at the surface of this kind of material at high temperature.  相似文献   
75.
We present a data-driven dynamic coupling between discrete and continuous methods for tracking objects of high dofs, which overcomes the limitations of previous techniques. In our approach, two trackers work in parallel, and the coupling between them is based on the tracking error. We use a model-based continuous method to achieve accurate results and, in cases of failure, we re-initialize the model using our discrete tracker. This method maintains the accuracy of a more tightly coupled system, while increasing its efficiency. At any given frame, our discrete tracker uses the current and several previous frames to search into a database for the best matching solution. For improved robustness, object configuration sequences, rather than single configurations, are stored in the database. We apply our framework to the problem of 3D hand tracking from image sequences and the discrimination between fingerspelling and continuous signs in American Sign Language.  相似文献   
76.
77.
20CrMnTiH钢水口堵塞机理研究与解决措施   总被引:1,自引:0,他引:1  
研究了转炉生产20CrMnTiH钢时连铸水口堵塞的机理,主要通过精炼造CaO—Al2O3-SiO2-CaF2系渣,保持熔渣良好的流动性和高碱度、低熔点、低氧化铁,提高吸附夹杂能力并针对引起水口堵塞的物质,对钙处理、软吹及进站S含量进行严格的要求,成功解决了水口堵塞问题。  相似文献   
78.
Post harvest application of Isopropyl-N (3-chlorophenyl) carbamate considerably reduced the degradation of starch when potato tubers were stored in an evaporative cooling chamber. The starch degraded at a faster rate when tubers were kept under refrigerated and room storage conditions.  相似文献   
79.
本文用不同的测试技术和方法测定了锗酸铋(BGO)单晶的比热(300~800K)热膨胀系数(100~1100K)和导温系数(140~700K),进而导出了 BGO 单晶不同温度下的导热系数、定容比热、德拜温度和格虑内森数。本文还对 BGO 单晶热物理性质的变化规律作了理论解释。  相似文献   
80.
Skeletal form of KnbO3 crystals growing in Li2B4O7 solvent was in-situ observed at 900℃ and it was found that shallow depression started to develop on the surface of KnbO3 crystals when the crystal size exceeded several micron,typically 7 micron.Based on the quantitative criterion derived by Chernov,the estimated critical size of KNbO3 crystals was 1 micron,which was consistent with the experimental measurement.The kinetic coefficients,Kcorner and Kcr,in the criterion were experimentally obtained in the diffusive-convective and diffusive-advective flow states respectively.  相似文献   
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