宽频介电谱仪热激励去极化电流功能研究

利用宽频介电谱仪拓展热激励去极化电流模块测量介质材料的TSDC操作简单实用,它不仅容易把材料中的各种不同活化能或弛豫时间的荷电粒子区分开,并且能从TSDC谱中直接得出被测材料的介电性能以及相关微观参数,这为研究材料内部机理提供了一条捷径。     

γ谱仪测量^109Cd的影响因素研究

不确定度分析是实现放射性活度测量质量保证的重要方面．本文对谱仪测量工作中影响加。Cd比活度的因素进行了研究与分析,为γ能谱分析工作及放射性活度测量中不确定度评定提供有益借鉴．     

薄层层析-紫外分光光度法测定银杏茶中银杏酸含量

采用薄层层析一紫外分光光度法建立了一种银杏茶中银杏酸快速检测的方法．采用正己烷索氏提取银杏茶中的银杏酸;以硅胶G为固定相,石油醚;乙酸乙酯：冰醋酸（18：1：1）为展开剂对银杏酸进行分离纯化;紫外分光光度法测定,波长为307nm．结果表明：该方法测定银杏酸含量的线性关系良好,线性范围为0．009-0．093mg／mL（R^2=0．9997）,精密度RSD为2．15％,平均回收率为100．90％,测定结果同HPLC法结果对照无明显差异,适用于银杏茶中银杏酸含量的测定．     

电子元器件用紫外荧光敷型涂层材料的研制

以硅烷偶联剂、甲基丙烯酸甲酯、甲基丙烯酸、引发剂过氧化二苯甲酰(BPO)、环保型混合溶剂、荧光粉等为原料,采用溶剂聚合方法,合成了环保型紫外荧光三防保护涂料;考察了反应温度、引发反应诱导期、引发剂用量等因素对涂料性能的影响;介绍了环保型紫外荧光三防保护涂料的性能特点.     

UV、臭氧和电离辐射工艺用于污水消毒的对比研究及经济分析

介绍了UV、臭氧和电离辐射消毒技术的原理以及主要优、缺点,比较了3种消毒方式的消毒效果、消毒副产物以及影响因素,并对各种工艺在1×104 m3/d、5×104 m3/d、1×105 m3/d处理规模下的工程投资总额、总运行成本和单位运行成本进行了经济分析。结果表明:当污水厂处理规模为1×104 m3/d时,UV、臭氧和电离辐射消毒工艺的单位运行成本分别为:0.075元/m3,0.21元/m3,0.25元/m3;当污水厂处理规模为5×104 m3/d时,UV、臭氧和电离辐射消毒工艺的单位运行成本分别为:0.049元/m3,0.19元/m3,0.17元/m3;当污水厂处理规模为1×105 m3/d时,UV、臭氧和电离辐射消毒工艺的单位运行成本分别为:0.041元/m3,0.17元/m3,0.16元/m3。     

基于AVR单片机的高精度紫外线检测仪的设计

介绍一种基于ATmega16L的高精度紫外线检测仪的设计,并给出了仪表设计的硬件结构框图和软件运行流程图。通过中船重工某所应用表明,该仪表具有测量精度高、性能稳定等技术优势。它能够适用于医院、卫生防疫部门、化工等消毒紫外线灯辐照强度的监测,具有广泛的应用前景。     

Chemical and Chromatic Bases for Preferential Visiting By the Cabbage Butterfly, Pieris rapae, to Rape Flowers

Scent and coloration of corolla were examined as floral attributes responsible for preferential visiting by the cabbage butterfly, Pieris rapae, to rape flower, Brassica rapa. Floral volatile components that release the flower-visiting behavior of the butterfly were identified by chemical analyses, electroantennography (EAG), and two behavioral bioassays: proboscis extension reflex (PER) in response to odor and attraction to artificial flowers. GC and GC-MS analyses of the headspace volatiles from the flowers revealed the presence of six aromatic compounds, benzaldehyde, phenylacetaldehyde, benzyl alcohol, 2-phenylethanol, phenylacetonitrile, and indole in decreasing order of quantity. Of these, phenylacetaldehyde elicited the highest response in the PER assay. While benzyl alcohol, 2-phenylethanol, benzaldehyde, and phenylacetonitrile evoked moderate responses, the PER-eliciting activity of indole was very weak. In two-choice behavioral bioassays, artificial flowers scented with any one of these PER-active compounds attracted significantly more butterflies than control (unscented) flowers, whereas those treated with indole were almost inactive. The EAG activities of the six chemicals were not high and were about the same at a low dose (1 g), but phenylacetaldehyde elicited a much stronger response from both sexes at higher doses (10 and 100 g). An overall profile of EAG responses at a dose of 100 g was analogous to that of PER performance, suggesting that floral volatiles may be involved in close-range location or recognition of flowers rather than long-range attraction. By spectroscopic and UV-photographic examinations of rape flower, the central part of the corolla was found to absorb UV rays in marked contrast to the other parts, which reflected near-UV rays (_max = 350 nm). This indicates that the flower is endowed with a conspicuous nectar guide that is probably an important visual stimulus for attracting foraging adults of P. rapae. Consequently, the present findings strongly suggest that this elaborate pollination strategy of rape flower, characterized by its good combination of olfactory and visual attractiveness, accounts for preferential visiting by the cabbage butterfly to the flower.     

一缩二乙醇二缩水甘油醚双丙烯酸酯的合成

以一缩二乙二醇二缩水甘油醚(DGDE)和丙烯酸为原料,N,N-二甲基苄胺为催化剂,对羟基苯甲醚为阻聚剂,制得了一缩二乙二醇二缩水甘油醚双丙烯酸酯(ADGDE)。讨论了催化剂用量、反应温度等因素对反应的影响,并用FT-IR和Photo-DSC对ADGDE的化学结构及光固化行为进行了表征。结果表明,反应温度为100℃、催化剂用量为1 0%时催化效果和反应速率较理想,用对羟基苯甲醚作阻聚剂得到的ADGDE颜色较浅;ADGDE的光聚合速率随光引发剂的用量增加而提高。     

成分分析仪在硫磺回收装置上的选用

针对硫磺回收工艺气的成分分析要求．结合某炼油厂硫回收装置中成分分析仪的选用与配置，个绍了两种成分分析仪的工作原理及特点．以及在硫磺回收装置中的选用与分析控制方案。     

The choice of gamma spectrometer for determining the content of 241Am

An express-estimation algorithm for determining the minimum detectable activity of ²⁴¹Am is developed. Semiconductor spectrometers manufactured by the ORTEC Company (USA) and scintillation spectrometers manufactured by the Atomtekh Company (Belarus) are compared. It is proposed to use the results to estimate the suitability of the existing inventory of measuring instruments for the radiation monitoring of territory contaminated by ²⁴¹Am. __________ Translated from Izmeritel’naya Tekhnika, No. 9, pp. 62–66, September, 2006.