Fabrication of ultraviolet photoconductive sensor using a novel aluminium-doped zinc oxide nanorod-nanoflake network thin film prepared via ultrasonic-assisted sol-gel and immersion methods

Unique and novel thin films with aluminium (Al)-doped zinc oxide (ZnO) nanostructures consisting of nanorod-nanoflake networks were prepared for metal-semiconductor-metal (MSM)-type ultraviolet (UV) photoconductive sensor applications. These nanostructures were grown on a glass substrate coated with a seed layer using a combination of ultrasonic-assisted sol-gel and immersion methods. The synthesised ZnO nanorods had diameters varying from 10 to 40 nm. Very thin nanoflake structures were grown vertically and horizontally on top of the nanorod array. The thin film had good ZnO crystallinity with a root mean square roughness of approximately 13.59 nm. The photocurrent properties for the Al-doped ZnO nanorod-nanoflake thin films were more than 1.5 times greater than those of the seed layer when the sensor was illuminated with 365 nm UV light at a density of 5 mA/cm². The responsivity of the device was found to be dependent on the bias voltage. We found that similar photocurrent curves were produced over eight cycles, which indicated that the UV sensing capability of the fabricated sensor was highly reproducible. Our results provide a new approach for utilising the novel structure of Al-doped ZnO thin films with a nanorod-nanoflake network for UV sensor applications. To the best of our knowledge, UV photoconductive sensors using Al-doped ZnO thin films with a nanorod-nanoflake network have not yet been reported.     

成像光谱技术的古画隐藏信息提取

目的 古画隐藏信息是包含在画作中的一种微弱信息,对于文物鉴定与修复具有非常重要的意义,如何快速无损准确提取古画中微弱的隐藏信息是目前研究和应用的一大技术难题,本文利用高光谱成像技术快速无损提取古画隐藏信息。方法 对古画进行高光谱扫描成像,得到短波红外波段（1 000~2 500 nm）的高光谱立方体数据,联合多种光谱匹配技术分析古画中人物头冠颜料种类;利用主成分分析技术,提取古画头冠周围涂抹痕迹。结果 通过多种光谱匹配算法对颜料进行分析,确定了颜料种类,并对匹配算法进行了对比,结果表明在颜料混合的情况下,光谱匹配算法仍能够有效的识别出混合颜料的端元种类,光谱信息散度与光谱角的匹配算法SID_SA匹配精度可以达到0.096,相比其他匹配算法,效果最好;利用主成分分析技术分层剥离主要背景信息后,头冠周围位于画作底层的涂抹信息得到了加强,可以有效地区分背景颜料信息与涂抹信息,提取隐藏信息。结论 高光谱分析技术对古画隐藏信息的提取有很好地识别效果,能够准确提取绘画颜料种类,发现绘画过程中的涂抹等痕迹,特别适用于混合颜料的种类识别与画作底层信息提取,发掘画作隐藏信息,为文物保护修复与鉴定提供支持。     

宽频介电谱仪热激励去极化电流功能研究

利用宽频介电谱仪拓展热激励去极化电流模块测量介质材料的TSDC操作简单实用,它不仅容易把材料中的各种不同活化能或弛豫时间的荷电粒子区分开,并且能从TSDC谱中直接得出被测材料的介电性能以及相关微观参数,这为研究材料内部机理提供了一条捷径。     

基于AVR单片机的高精度紫外线检测仪的设计

介绍一种基于ATmega16L的高精度紫外线检测仪的设计,并给出了仪表设计的硬件结构框图和软件运行流程图。通过中船重工某所应用表明,该仪表具有测量精度高、性能稳定等技术优势。它能够适用于医院、卫生防疫部门、化工等消毒紫外线灯辐照强度的监测,具有广泛的应用前景。     

成分分析仪在硫磺回收装置上的选用

针对硫磺回收工艺气的成分分析要求．结合某炼油厂硫回收装置中成分分析仪的选用与配置，个绍了两种成分分析仪的工作原理及特点．以及在硫磺回收装置中的选用与分析控制方案。     

The choice of gamma spectrometer for determining the content of 241Am

An express-estimation algorithm for determining the minimum detectable activity of ²⁴¹Am is developed. Semiconductor spectrometers manufactured by the ORTEC Company (USA) and scintillation spectrometers manufactured by the Atomtekh Company (Belarus) are compared. It is proposed to use the results to estimate the suitability of the existing inventory of measuring instruments for the radiation monitoring of territory contaminated by ²⁴¹Am. __________ Translated from Izmeritel’naya Tekhnika, No. 9, pp. 62–66, September, 2006.     

Surface modification of biodegradable plastics by ion beams

Biodegradable plastics can be used as conventional plastics, while on disposal they decompose to water and carbon dioxide by microorganisms existing in natural environment. Products using biodegradable plastics have recently been developed in many companies pursuing ecology. In this study, surface modification of biodegradable plastics was carried out by inert ion beams for improvement of photo deterioration under an ultraviolet ray. The hardness of biodegradable plastics tended generally to decrease with irradiation of an ultraviolet ray. In this method, the hardness of ion-bombarded biodegradable plastics was kept at an initial value under an ultraviolet ray, because the modified layer by ion bombardment intercepted an ultraviolet ray. The hardness of He⁺ ion-bombarded biodegradable plastics showed larger value than that of Ar⁺ ion bombardment. He⁺ ion bombardment at ion energy of 10 keV produced the suitable property with both of high transmittance of a visible ray and high interception of an ultraviolet ray in a surface layer of biodegradable plastics.     

中国环流器HL和欧洲联合环JET的检漏技术进展

对HL环流器系列装置,开发了蒽-丙酮荧光液渗透检漏用于真空内衬的零部件检漏,灵敏度可以达到10-9Pa.m 3.s-1,示漏位置分辨小于0.5mm;对大容器真空检漏,采用四极质谱计和氦质谱检漏仪相配合的检漏法;对压力容器检漏,开发了真空罩吸枪-氦质谱检漏系统,还研制了适于抽除大量水汽的检漏真空机组。对氘氚放电的JET,使用普通的氦质谱检漏仪(扇形磁体型)受到真空室壁释放所吸留的氢同位素的、尤其是氘的严重干扰,因为示漏气体氦(4H e,4.0026u)与氘(D2,4.0282u)的质量数十分相近。在氦质谱检漏仪入口处串接选择性抽气泵——用液氮冷阱来抽除可凝气体、用分子筛泵或10K低温泵来抑制氢同位素本底,并前置一个涡轮分子泵来压缩加强采样气流等。这种加强组合能使原先的氦质谱检漏系统灵敏度提高3个量级以上。     

环氧基负性光刻胶加工微结构的试验研究

在正交试验的基础上,将BP神经网应用于负性光刻胶(SU-8)加工高分辨率和高深宽比微结构的工艺研究,建立了光刻图形质量与前烘时间、前烘温度、曝光量、后烘时间之间的预测模型,该模型采用三层前向网络,学习算法为梯度下降法。通过实验,得出:前烘温度与前烘时间对光刻质量影响最大,对120～340μm厚的光刻胶,前烘温度取90℃,前烘时间50~100min时,图形的相对线宽差最小;最佳后烘时间(85～95℃)为30min;超声搅拌能缩短显影时间,改善图形质量。试验结果与网络预测结果吻合。结果表明,将BP神经网络应用于UV-LIGA技术中,可以优化光刻工艺。