放射性核素迁移的实验室研究——Ⅱ.用混合裂变产物溶液研究核素在地质材料上的吸附

应用裂变产物混合物做为示踪剂研究了~(137)Cs,~(141,144)Ce,~(103,106)Ru,~(103,106)Ru,~(95)Zr,~(95)Nb,~(89,90)Sr在花岗岩、凝灰岩、页岩上的吸附行为。应用批式技术测定了吸附比。核素的γ放射性是用连有SCORPIO-3000多道计算机系统的Ce(Li)探测器测量的。β放射性~(89,90)Sr是放化分离后在G-M计数器上测量的。结果表明:凝灰岩、页岩能强烈吸附Ce,Nb,Zr;吸附Cs居中;吸附Sr,Ru较差;花岗岩的吸附性能都差。     

Synthesis of diamond crystals and films using an oxygen-acetylene flame under atmosheric pressure

Diamond growth with rates up to 100 to 140 μm/hr was achieved using an oxygen-acetylene combustion spraying technique in an atmospheric environment. Investigations on the processing indicated that the gas flow ratio, substrate position, substrate temperature, temperature distribution, and substrate pretreatment were the most important factors affecting the growth of diamond crystals. Evaluation by means of X-ray diffraction, Raman spectroscopy, scanning electron microscopy, and electron probe microanalysis showed that the synthesized diamond was nearly perfect in morphology, structure, and purity.     

Solubility of amaranth seed proteins in sodium sulphate and sodium chloride: the main factor in quantitative extraction for analysis

Nitrogen was extracted more efficiently from amaranth seed with 0.04 M Na₂SO₄ (5% w/v) than with either 0.09 M or 0.17 M NaCl (5% or 10% w/v), despite both solutions having the same ionic strength (μ= 1). Solubility of saline soluble proteins (albumin ± globulin) was very poor in either water or 1M NaCl, but increased in 0.4M NaCl at alkaline pH between 7 and 10. Globulins were very soluble in 0.4M NaCl at a pH 9. Albumin was the main storage protein. Saline soluble proteins formed very weak gels.     

RE／S值对控轧低碳Mn－Nb－RE钢硫化物成分和形貌的影响

用扫描电镜测定了含０．０４１％～０．０７６％ＲＥ的低碳Ｍｎ－Ｎｂ－ＲＥ钢中硫化物的成分、大小和形貌。ＲＥ／Ｓ值为２．８～３．０时，钢中的硫化物充分变质。     

氨合成塔出口氨含量偏低原因分析及对策

阐述UHDE合成塔运行现状 ,分析氨净值达不到设计值的原因 ,提出相应的解决措施     

AUTOCONER-338型自动络筒机的接头工艺与切疵有效性分析

介绍了AUTOCONER-338型自动络筒机空气捻接器的接头要求与影响接头质量的因素,并且就不同品种的纱线选用不同接头工艺进行了简单分析;介绍了如何评价络筒切疵有效性与影响切疵率的因素.通过以上2方面的分析介绍,及时调整设计与工艺,提高了生产效率,改善了布面质量.     

平面药包抛掷爆破的漏斗特征解析

根据惠州港通用码头陆域平面药包抛掷爆破的实爆堆积测量分析成果 ,结合药包设计的主要参数 ,对平面药包产生的爆破漏斗的范围与形态、不同药包部位的残方比与抛掷率、药包的长抗比与圆柱体药包的应力波形演变关系予以解析 ,供硐室爆破的理论研究、模拟试验和总结条形药包特性时参考     

Preparation and properties of silicone‐containing poly(methyl methacrylate) gels

Poly(methyl methacrylate) (PMMA) gels with varying amounts of silicone and solvent and constant amounts of crosslinker were prepared by solution free radical crosslinking copolymerization of methyl methacrylate (MMA), ethylene glycol dimethacrylate (EGDM), tetraethoxysilane (TEOS) and vinyltriethoxysilane (VTES) comonomer systems. They were then studied in benzene at a total monomer concentration of 3.5 mol L^?1 and 70 °C. The conversion of monomer, volume swelling ratio, weight fraction and gel point were measured as a function of the reaction time, silicone concentration and benzene content up to the onset of macrogelation. Structural characteristics of the gels were examined by using equilibrium swelling in benzene, gel fraction and Fourier‐transform infrared (FTIR) analysis. The morphology of the copolymers was also investigated by SEM. Based on the obtained results, it was concluded that the FTIR data did not have the capacity to show the presence of the VTES or TEOS moiety in these kinds of copolymers. On the other hand, the variation of weight fraction of gel, W_g, and its equilibrium volume swelling ratio in benzene, q_v, exhibited the same behaviour as that of MMA/EGDM copolymers. Also, the dilution of the monomer mixture resulted in an increase in the gel point and swelling degree and a decrease in the percent of conversion and gel fraction. Finally, TEOS is not an ideal silicone compound for reaction in the MMA/EGDM copolymerization system, whereas VTES is a suitable silicone comonomer for this system and it has been proved useful. Copyright © 2005 Society of Chemical Industry     

砌筑砂浆达不到设计要求的事故原因分析

从砂浆的配合比、和易性、原材料等对砌筑砂浆达不到设计要求的事故原因进行了分析。     

岩屑泊松比实验测定仪

针对目前地层泊松比测定方法的局限 ,提出了利用上返岩屑压实测定地层泊松比的设想 ,并研制出岩屑泊松比实验测定仪。某油田已有的压实岩屑泊松比与实际声波测井资料计算泊松比对比发现 ,运用岩屑泊松比实验测定仪所得的实验结果与原始地层的泊松比有很好的一致性(两者的误差在± 5 %之间 )。利用该测定仪 ,可实现对钻井过程中上返岩屑的连续快速测定 ,大大降低工程取心所增加的钻井成本 ,还可为钻井施工在第一时间提供相关的地层信息