Development of three-electrode type micro-electrochemical reactor on anodized aluminum with photon rupture and electrochemistry

Photon rupture with a focused single pulse of pulsed YAG-laser irradiation was used to fabricate an aluminum electrochemical micro-reactor. Porous type anodic oxide film formed on aluminum specimens was irradiated in solutions with a pulsed Nd-YAG laser beam through a convex lens to fabricate micro-channels, micro-electrode, and through holes (for reference electrode, solution inlet, and outlet). During irradiation, specimens were moved by a computer controlled XYZ stage. After irradiation, the surface of the micro-channel and through hole were again treated to form anodic oxide film and the surface of the micro-electrode was treated electrochemically to provide an Au layer. The calculated volume of the micro-reactor including micro-channel and through holes is about 1.5 μl. The cyclic voltammogram of the micro-electrochemical cell was measured in K₃Fe(CN)₆/K₄Fe(CN)₆ with both static and flowing solution at different scanning rates. The anodic and cathodic peak currents were measured and the values depended on scanning rate and ion concentration when the solution was static. With the flowing solution, limiting currents were observed and the anodic limiting current was increased with the cubic root of the solution flow rate.     

MgO／Ni系梯度功能材料的设计与制备

对ＭｇＯ／Ｎｉ系梯度功能材料（ＦＧＭ），分别用实验和微观力学模型测定和计算了用于热应力缓和设计的各物性参数。讨论了两种结果之间存在差异的原因。用有限元方法模拟了制备过程中ＦＧＭ的热应力，得到ＭｇＯ／Ｎｉ系ＦＧＭ的综合设计准则。按设计结果进一步调整粉末工艺性质，成功地烧制出ＭｇＯ／Ｎｉ系ＦＧＭ。     

Preparation and Characterization of 17O-Enriched Alumina for Nuclear Fusion Damage Experiments

Alumina enriched in ¹⁷O was successfully fabricated from aluminum isopropoxide and water containing the ¹⁷O isotope. This material was necessary for an experiment to study the radiation damage expected in alumina exposed to a nuclear fusion reactor environment. The enrichment levels of specimens subjected to different preparation schedules were measured using a nuclear reaction analysis technique. Replacement of the ¹⁷O isotope in the ceramic by atmospheric oxygen occurred readily. Therefore, successful fabrication of suitably enriched alumina specimens required that all processing steps be performed under vacuum or inertgas environments. The optimum fabrication procedure produced enriched alumina specimens of >99.5% of theoretical density, ∽10-μm grain size, and a flexural strength of 280 MPa.     

子午线轮胎生产设备的国产化及其存在的问题

对生产子午胎的九大类主要设备：炼胶设备、帘布覆胶设备、覆胶帘布裁断设备、复合挤出机及其生产线、钢丝圈设备、内衬层（气密层）生产线、成型设备、硫化机、成品检测设备进行了分析，总结介绍了我国橡机企业在这九大类设备的设计制造方面取得的成绩和水平，并与国际现状进行了对比。最后总结了我国子午胎设备目前的优势和不足。     

GHH烟气膨胀机叶片的国产化及使用情况分析

简要介绍了石家庄炼油厂GHH公司生产的烟气膨胀机叶片国产化情况、使用中出现的问题以及改进方法，肯定了进口机组叶片国产化的工作思路。     

国产化大模场掺镱光子晶体光纤的设计与制备

理论分析了空气孔尺寸与晶格常数对光子晶体光纤(PCF)单模特性的影响,设计了大模场双包层PCF的波导结构。采用自主知识产权的专利技术,制备出高数值孔径大模场掺Yb双包层PCF,其内包层数值孔径为0.65,纤芯数值孔径为0.06,有效模场面积为1 465.7μm2。     

钛合金流体软管组件的设计与工艺

高功率电子产品的散热需求越来越高,流体软管组件作为热量传输载体的必要部件,其轻量化、可靠性等性能越来越重要。文中提出了一种钛合金流体软管组件的设计方案,并系统研究了该软管组件的制备工艺,最后的可行性,为液冷散热的流体连接提供了一种有效的解决方案。     

Photonic crystal fiber Mach-Zehnder interferometer with microholes ablated by a femtosecond laser for refractive index sensing

A new structure of the photonic crystal fiber (PCF) based Mach-Zednder interferometer (MZI) is fabricated and presented. The structure has microholes ablated by a femtosecond laser. The fringe visibility can be enhanced more than 10.dB compared with the interferometer without a microhole. The interferometer is characterized by sodium chloride solutions for refractive index (RI) sensing. The RI sensitivities are greatly increased by the hole fabrication since it directly changes the cladding modes of the PCF. For the interferometer sensor with two holes, the RI sensitivity is 157.74 nm/RIU, which is 5.times than that of the sensor without a microhole. Microholes ablation with a femtosecond laser on PCF can increase the sensor''s sensitivity dramatically. Femtosecond laser has a wide application prospect in the field of performance improvement of the sensors.     

Ti3AlC2／Cu复合材料的制备及其性能研究

采用粉末冶金的方法在1000℃和30MPa的热压条件下，烧结制备了以Ti3AlC2为增强相的Ti3AlC2／Cu复合材料，研究了增强相含量（10％～40％）对复合材料的显微结构、抗弯强度、硬度和电阻率的影响。结果表明：Ti3AlC2能够有效增强铜，当Ti3AlC2含量为30％时，增强效果最佳，复合材料的抗弯强度达1033MPa，最大形变为2．5％，增强相含量继续增加时，复合材料的强度反而降低；随着增强相含量的增加，复合材料渐趋脆性断裂，同时复合材料的电阻率基本呈线性升高。     

新型铝合金拉闸的生产技术与应用

扼要介绍了铝合金拉闸的制做技术,分析了该产品的特点和功能以及其应用前景。