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11.
聚合物-金属界面相形貌的研究 总被引:1,自引:0,他引:1
环氧树脂在 Al 合金表面生成纤维状的界面相结构,其形成、发展和特征与树脂的体系、交联反应条件以及 Al 合金的表面状态有关。环氧树脂的基础相为颗粒状的超结构组织。聚合物界面相的力学破坏表现为纤维体的拉伸、变形和断裂,而基础相在纯剪切受力时出现在45°方向的裂纹,并发展导致连接层的破坏。 相似文献
12.
A photochromic nanocomposite based on Keggin structure phosphomolybdic acid (PMoA) well dispersed in polyethyleneglycol (PEG) was fabricated. TEM image showed that PMoA nanoparticles with narrow size distribution were finely dispersed in polymer matrix. FT-IR results showed that the Keggin geometry of polyoxometalates was still preserved inside the composites and strong coulombic interaction was built between PMoA and polymer matrix. Under UV irradiation, the film was reduced photochemically to yield a blue species, which was in accordance with a charge-transfer mechanism. 相似文献
13.
用己二酸二酰肼(ADH)对透明质酸(HA)进行化学修饰,制备交联透明质酸(HA-ADH)薄膜。粘度法测试表明HA-ADH是一种可降解的生物材料,并且与HA相比,HA.ADH的降解速率减慢。在此基础上,研究了以疏水性的替硝唑(TDZ)和亲水性的头孢唑啉钠(CEZ)为模拟药物的HA-ADH药物载体薄膜的释药性能。紫外-可见(UV-Vis)吸收光谱检测表明,HA-ADH是一种疏水性药物TDZ的优良缓释制荆,这是由于TDZ的疏水性和HA-ADH薄膜的缓慢溶胀和降解性能的结合而得到的,药物的释放主要受扩散机制控制。 相似文献
14.
The dynamics of a thin liquid film falling down a uniformly heated wall is studied. The model introduced by Kalliadasis et al. [J. Fluid Mech. 475 (2003) 377] for the same problem is revisited and its deficiencies, namely the prediction of a critical
Reynolds number with 20% error, cured. For the energy equation a high-order Galerkin projection in terms of polynomial test
functions is developed. It is shown that not only does this more refined formulation correct the critical Reynolds number,
but it also gives, with an appropriate expansion close to criticality, the long-wave theory. Bifurcation diagrams for permanent
solitary waves are constructed and compared with the solution branches obtained from different models. It is shown that, in
all cases, the long-wave theory exhibits limit points and branch multiplicity, while the other models predict the continuing
existence of solitary waves. Time-dependent computations show that the free surface and interfacial temperature approach a
train of coherent structures that resemble the infinite-domain stationary solitary pulses. 相似文献
15.
The switchable optical properties of Pd-protected RCo2-type Ho0.6Mm0.4Co2 alloy thin films have been investigated in a KOH electrolyte. The reversible optical switching has been carried out simultaneously by measuring transmitted light through the thin film during electrochemical charging–discharging of hydrogen. The dependence of switching speed and cyclic durability of the film on the charging and discharging current density as well as concentration of KOH electrolyte has been studied. In addition, cyclic voltammetric measurements have been performed to examine the hydride formation and decomposition reactions. 相似文献
16.
李彩虹 《南京工业职业技术学院学报》2008,8(2):1-3
根据PET薄膜的特点和高分子熔融态流动理论,分析了挤出回收用螺杆的各段结构,及螺杆参数选择,设计出大长径比、深槽、双排气、高效专用螺杆。 相似文献
17.
The breakdown processes of oil films under quasi-static loading have been investigated by using a newly developed steel-oil-mercury system. The relationship between the thickness and breakdown ratio of a hexadecane film is represented by a single master curve independently of the indentation speed, indentation load, and temperature. The master curve shows that the breakdown process of hexadecane includes two stages; one is the decrement of the thickness without breakdown and the other is the decrement of the thickness with a drastic progress of breakdown. By solving a small amount of fatty acid in hexadecane, the thickness increases and the breakdown ratio decreases noticeably; a multilayer residual film supporting normal load is formed between two metal surfaces. Experiments at different temperatures reveal a negative relationship between the temperature and thickness of residual film, which indicates that the residual film is organized by physical interaction rather than chemical interaction. At least under a lower concentration, the residual film appears to consist of not only fatty acid molecules but also hexadecane molecules. 相似文献
18.
火焰图像特征在火灾数字图像识别中的运用 总被引:1,自引:0,他引:1
火焰尖角数目和圆形度是早期火灾火焰的主要特征,本文主要论述了如何在数学形态学基础上,利用火灾火焰的两个特点判断和识别早期火情。实验中,对火焰的二值图像进行开运算,即先腐蚀,再膨胀,目的是为了对火焰图像进行形态学滤波,去噪。从实验结果可以看出,该算法可以很好的识别火焰和干扰源。 相似文献
19.
M Isabel Sánchez de Rojas Julián Rivera Moisés Frías Félix Marín 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(3):209-217
Copper slag is a by‐product generated during smelting to extract copper metal from the ore. The copper slag obtained may exhibit pozzolanic activity and may therefore be used in the manufacture of addition‐containing cements. In this paper the effect of the incorporation of the copper slag in cement is measured. Blends of copper slag with Portland cement generally possess properties equivalent to Portland cement containing fly ash, but very different to the silica fume incorporation. Copper slag and fly ash reduce the heat of hydration more effectively than silica fume in mortars. The replacement of 30% cement by copper slag reduces the flexural and compressive strength in a similar way to fly ash; however, after 28 days, the reduction is less than the percentage of substitution. Hydrated calcium aluminate phases were analysed using scanning electron microscopy (SEM) and X‐ray diffraction (XRD) techniques. The pozzolanic activity of copper slag is similar to that of fly ash and higher than silica fume. In the presence of low water/cement ratios, certain pozzolanic materials produce a very compact cement paste that limits the space available for hydration products, a determining factor in the formation of hydrated calcium aluminates. SEM was found to be a useful analytical technique when aluminates are formed and can be clearly detected by XRD. Copyright © 2008 Society of Chemical Industry 相似文献
20.