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61.
62.
E. Ya. Davydov I. S. Gaponova T. V. Pokholok G. B. Pariiskii G. E. Zaikov 《应用聚合物科学杂志》2008,108(1):128-133
The features of initiation of free radical reactions in polymers by dimers of nitrogen dioxide are considered. The conversion of planar dimers into nitrosyl nitrate in the presence of amide groups of macromolecules has been revealed. Nitrosyl nitrate initiates radical reactions in oxidative primary process of electron transfer with formation of intermediate radical cations and nitric oxide. As a result of subsequent reactions, nitrogen‐containing radicals are produced. The dimer conversion has been exhibited by estimation of the oxyaminoxyl radical yield in characteristic reaction of p‐benzoquinone with nitrogen dioxide on addition of aromatic polyamide and polyvinylpyrrolidone to reacting system. The isomerization of planar dimers is efficient in their complexes with amide groups, as confirmed by ab initio calculations. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
63.
Eu3 ions were incorporated in sol and gel by a sol-gel processing using 3-glycidoxypropyltrimethoxysilane(CH2OCHCH2O(CH2)3Si(OCH3)3, GPTMS) and ethyl silicate (TEOS) as precursors. The basic chemical-physical properties such as DTA curve, FF-IR spectra and specific surface area were recorded. The characteristics of their optical spectra were measured and investigated. The results indicate that the emission intensity of Eu3 ion in ormocer is much higher and the global line width is wider than those in SiO2 gel. The relationship between the composition and structure of gels and the fluorescence intensity and width were discussed. The obtained ormocer shows good mechanical strength, which can be cut and polished in machine without broken. 相似文献
64.
The paper presents a derivation of the dynamic impedance of a PV module. At each bias voltage, the general form of the impedance describes a semicircular locus in the complex impedance plane. Intercepts of each impedance locus yield series, shunt and dynamic resistance of a module. Determinations of the dynamic impedance of a x-Si PV module in the dark with five reverse bias voltages and over a frequency range of 1 Hz to 60 kHz are made. The experimental results validate the derived general form of dynamic impedance. 相似文献
65.
无氢类金刚石碳膜的研究进展 总被引:1,自引:0,他引:1
介绍了无氢类金刚石碳膜的制备方法 ,它们的机械、光学、电学性能 ,将无氢与含氢的类金刚石碳膜进行了简单比较 ,总结及探讨了它们的应用 相似文献
66.
Electric charges at the surface of a passive stainless steel are generally considered as concentrated either in the passive film itself, or at the metal/passive film interface, or in the electrical double layer at the film solution interface. Rest potential time dependence after immersion of a passive surface in aqueous electrolytes suggests however that slow processes occur in the onset of the surface charge. Specific experiments, such as streaming potential measurements and electrochemical impedance spectroscopy in a thin electrolyte cell, were carried out for understanding better this phenomenon. An AISI 304 type austenitic stainless steel with polished or bright annealed surface finishes was immersed in NaCl aqueous solutions with various pH and chloride concentrations. The streaming potential time evolution shows two steps: a first rapid one (∼2 min) is attributed to the onset of the surface charge. The second step is much slower (approximately several hours) and possibly due to an interphase layer between the passive film and the solution. Following this idea, the whole kinetics is controlled by cation migration across the interphase when the pH is larger than the isoelectric pH (pHiep), while chloride ions are incorporated in the interphase when pH < pHiep. Impedance measurements allow determining both the kinetics of charge transport and the thin cell conductivity. When glass is used as reference material for the cell walls instead of stainless steel, the Nyquist plots show a high-frequency response. For stainless steel cell walls, a low-frequency response is observed, attributed to a slow charge reorganisation inside the interphase layer. The charge distribution at metal/electrolyte interface is discussed in terms of a gel-like layer which possibly takes place at the passive film/electrolyte interface. 相似文献
67.
高分辨率测井约束地震反演技术在本布图地区的应用 总被引:1,自引:0,他引:1
简要介绍了高分辨率测井约束地震反演技术应遵循的原则及实现步骤,并应用该技术对焉耆盆地本布图背斜构造带进行预测和分析。通过对比分析,反演剖面的分辨率和信噪比有所提高,能较好的反映储层性质的横向变化,预测结果与实际基本符合,说明高分辨率测井约束反演技术在该地区具有一定的实用性。 相似文献
68.
直接斜率波前复原算法的控制效果分析 总被引:7,自引:0,他引:7
建立自适应光学系统功率谱抑制函数的概念,分析了采用直接斜率波前复原算法的自适应当光学系统的控制效果,理论分析与61单元自适应光学系统上的实验结果表明,直接斜率波前复原算法将导致控制效果下降。 相似文献
69.
Plasmapropertiesoflaser-ablatedSttargetinairWangXiang-Tai(王象泰);ManBao-Yuan(满宝元);WangGong-Tang(王公堂);FanXi-Jun(樊锡君);WangJun(王军)... 相似文献
70.
通过密度、可见光光谱、红外吸收光谱、Co-60辐照损伤试验及荧光光谱的测试,研究了PbO-Bi2O3-B2O3-SiO2玻璃系的光学性能与结构.密度最高可达8.464g/cm3其紫外吸收达截止波长随Pb2+及Bi3+含量升高而红移.玻璃熔化温度低达850℃.在PbO-Bi2O3-B2O3系玻璃中加人SiO2可使玻璃结构更致密.室温下该系统玻璃在360nm有一个宽的激发峰,能产生418um及438um两个弱的发射峰.该系统玻璃的结构是由[SiO4]4-、[BO3]3-、[BO4]5-、[PbO4]6-及[BiO6]9-构成.其中部分Pb2+及Bi3+以网络外体进入玻璃. 相似文献