掺杂Yb的TiO2光催化剂的制备和性能

采用溶胶-凝胶法制备了Yb掺杂TiO2纳米光催化剂,并通过XRD和BET等手段进行了表征.以对苯二甲酸作为探针分子,结合化学荧光技术研究了光催化剂表面羟基自由基的生成;并以苯酚为光催化降解反应模型化合物,考察了光催化剂的活性.测定了苯酚在TiO2和Yb掺杂TiO2光催化剂上的吸附常数.结果表明：Yb掺杂使TiO2的粒径减小,比表面积增大,同时导致羟基自由基的生成速率增大.Yb掺杂有利于反应底物在催化剂表面的吸附,Yb的最佳掺入量为Yb/Ti摩尔比=0.8%.     

Study of impurity induced modifications in amorphous N-type (GeSe3·5)100−x Bi x using high pressure technique

The technique of high pressure is utilized to study the carrier transport behaviour in doped and undoped bulk amorphous (GeSe_3·5)_100−x Bi _x (x=0, 2, 4, 10) down to liquid nitrogen temperature to observe impurity induced modifications in amorphous semiconductors. It is observed that pressure induced effects in lightly doped (2 at % Bi) and heavily doped (x=4, 10) semiconductors are markedly different. Results are discussed in view of the incorporation behaviour of the bismuth impurity.     

服装低密度聚乙烯热熔胶化学粉碎的研究

服装粘合衬布的生产需要低密度聚乙烯热熔胶的微细粉末,介绍了对该热熔胶的化学粉碎技术所进行的实验研究,表明采用适当的助剂种类和用量以及适宜的工艺过程,通过化学粉碎可以得到合格的粉末产品。     

Time Characterization of High Density Gas Jet from a Pulsed Supersonic Nozzle via Laser Produced Plasma

A high-density gas jet supersonic nozzle is reported in this paper. The jitter and actuation time of the nozzle is determined by the pin discharge and laser spark radiation respectively. The jitter time of the nozzle is within 10μs with the backing pressure as high as 25 bar. With a nanosecond laser pulse focused on the gas jet about 1 mm below the nozzle, the actuation time is calculated to be about 15 ms by detecting the laser produced spark radiation, which reveals the existence of the gas jet and the relative gas density evolving with time. Consequently the gas density is estimated to be well above 10^19 cm^-3, compared with theoretical simulations from the nozzle parameters.     

Electrical characterization of homoepitaxial diamond p–n junction

Electrical properties of homoepitaxial diamond p–n⁺ junction of boron (B)-doped p-type layer and phosphorus-doped n-type layer on Ib (111) diamond single crystal have been characterized. Current–voltage characteristics show a clear rectifying property with rectification ratio of over 10⁵ at ± 10 V. From capacitance–voltage characteristics, it is found that a spatial distribution of space-charge density N_i of the p–n⁺ junction is not uniform and N_i at a middle region of the space-charge layer formed at zero bias voltage is higher than that of other region of the space-charge layer. This peculiar characteristic can be explained by superposition of two effects; one is the deep dopant effect due to B atoms in the p-type layer, which makes to reduce N_i at around the edge of the space-charge layer formed at zero bias voltage. The other is the compensation of B acceptors by impurity atoms diffusing during the p–n⁺ interface and incorporating during the growth of p-type layer, which makes to reduce N_i at the vicinity of the p–n⁺ interface.     

激光武器对抗效能指标体系研究

武器系统的效能是规划、研制、配置和部署武器系统的基本依据,是评价武器系统优劣最重要的综合性指标,建立正确的效能指标体系是进行效能分析与评价的前提。在详细研究了激光武器对抗机理、效能指标选用原则的基础上,构建了相对完整的激光武器对抗效能指标体系结构,并提出了在不同作战任务下量度激光武器对抗能力的效能定义。     

Modelling and analysis of 3-D arrangements of particles by point processes with examples of application to biological data obtained by confocal scanning light microscopy

Within the concept of point processes, a review is presented of quantities which can be used in studies of three-dimensional (3-D) aggregates of particles. Suitable characteristics and estimators are given for both unmarked and marked point processes. To demonstrate the feasibility of such quantitative approaches, an application in histology, dealing with 3-D arrangements of cell nuclei in rat liver, is described. Using a confocal scanning light microscope, 3-D images are recorded and image analysis used to obtain the coordinates of the centroid, together with the volume and DNA content, of each cell nucleus. Examples of results are given, using both unmarked and marked point processes. In the latter case, cell type, nuclear volume and ploidy group are suitable marks.     

激光平网雕刻机设计

研制了用于制作平面网版的激光雕刻机，设计了雕刻机用CO2激光器、光路系统及单片机控制系统，探讨了将图像文件转化为控制命令文件的方法。     

采用模数转换技术提高脉冲激光测距的测时精度

针对脉冲激光测距中计数量化误差影响测时精度的问题,本文提出了采用模数转换技术提高测时精度的方法,并进行了可行性与精度分析,理论与实践结果均表明,该方法易于实现,能够容易地将计数量化误差减少若干个数量级。     

激光熔敷合金层组织及腐蚀磨损特性研究

利用ＣＯ＿２连续激光器在４５钢表面进行了激光熔敷镍基合金、镍基Ｃｒ＿２Ｏ＿３合金和镍基ＷＣ合金，以２Ｃｒ１３不锈钢为对比材料，系统地研究了激光熔敷层在不同冲击速度和腐蚀介质浓度下的腐蚀磨损特性，并根据组织分析、显微硬度测试及腐蚀磨损后的表面形貌观察，探讨了激光熔敷层的腐蚀磨损过程。结果表明：激光熔敷层的腐蚀磨损性能均比２Ｃｒ１３不锈钢好。