Improved direct bonding method of Nd:YVO4 and YVO4 laser crystals

We succeeded in the fabrication of bonded laser crystals composed of a neodymium-doped YVO₄ laser crystal (Nd:YVO₄) and its host crystals YVO₄ by a newly developed dry etching technique using an argon ion beam. The optical distortion caused by the bonded interface of size 5 mm × 6 mm was estimated to be 0.05λ at 633 nm. From the comparison of laser performance pumped by a laser diode, the bonded crystals could increase the laser output power by nearly twice that of the non-bonded crystals with the same degree of polarization of 99.2%. To analyze the mechanism of the enhanced reduction of the thermal load in the bonded crystals, numerical simulations with a finite-element method were also performed.     

机械合金化过程中Fe70B30粉末晶粒尺寸和微观应变的研究

用Ｘ射线和电镜研究了Ｆｅ＿（７０）Ｂ＿（３０）粉末经不同时间高能球磨后晶粒尺寸和微观应力的变化。在机械合金化过程中，粉末的Ｘ射线衍射谱的宽度随球磨时间的增加逐渐加宽，这是晶粒细化和内部微观应力共同作用的结果。Ｘ射线衍射结果表明：随着机械合金化的进行，粉末的晶粒尺寸逐渐减小，球磨初期晶粒尺寸下降较快，经１５ｈ球磨，晶粒尺寸为２５ｎｍ，机械合金化进行到一定时间后晶粒尺寸下降缓慢，８０ｈ球磨后晶粒尺寸可达５ｎｍ。在机械合金化过程中球磨所造成的微观应变不大，球磨初期粉末的内应力随球磨时间增加而增加，当粉末粒子尺寸很小时，随球磨的进行粉末中的微观应变显著下降。     

液相添加剂对PTCR陶瓷电性能的影响

液相添加剂ＡＳＴ（Ａｌ２Ｏ３＋ＳｉＯ２＋ＴｉＯ２）对ＢａＴｉＯ３陶瓷材料电性能的影响很大，随着Ａｌ２Ｏ３含量的增加，材料的电性能降低；ＳｉＯ２、ＴｉＯ２的物理特性对材料电性能影响较大；过量ＴｉＯ２对材料ＰＴＣ效应有重要影响，适当过量ＴｉＯ２含量，可得到性能优良的ＰＴＣＲ陶瓷。     

布里奇曼法生长碲镉汞晶体的固液界面形态研究

文中综述了布里奇曼法及加速坩埚旋转技术的布里奇曼法生工碲镉汞晶体过程中固液界面形态的研究结果，简单讨论了固液界面形态对组分分布的影响，并将两种技术所得的组分分布结果进行了比较，在分析影响固液界面形态因素的基础上，认为加速坩埚旋转技术是目前改善固液界面形态的有效方法。     

Separation of di- and tripeptides with solvent extraction and an emulsion liquid membrane

The extraction equilibria of various di- and tripeptides with di-2-ethylhexylphosphoric acid (D2EHPA) were studied at low pH values. The complex extracted to organic phase consisted of one molecule of peptide and two molecules of D2EHPA dimer. The extraction constants of the peptides correlated well with the distribution coefficients of peptides between 1-octanol and water, which is a measure of hydrophobicity. The permeation rates of peptides through an emulsion liquid membrane were examined by using D2EHPA as a carrier, Span 80 as an emulsifier and kerosene as a diluent. The rates varied considerably with peptide type, depending upon the hydrophobicity.     

中温低氰液体碳氮共渗及其应用效果

通过金相、硬度、耐磨性等测试分析表明，在“６０３”液体渗碳基础上研制出的新型中温低氰液体碳氮共渗剂对薄片件进行薄层碳氮共渗．能完全满足技术要求，并且取得了良好经济和社会效益．     

硼酸铝钕(NAB)晶体光学均匀性的测量

NAB晶体是一种综合性能较好的新型激光工作物质,有希望做成高效的小型固体激光器。本文介绍一种测量这种晶体光学均匀性的方法。 一般都采用在干涉仪上观测干涉图样来判定激光棒的光学均匀性。NAB晶体的吸收光谱曲线显示出其在可见光光谱区内有多个吸收峰。我们注意到:通常用做激光干涉仪光源的He-Ne激光器发射的632.8nm谱线正位于NAB晶体的一个吸收峰,并用输出约为45mW     

β—BBO晶体的电光性能

用干涉法测量了β－ＢＢＯ晶体的电光系数：γ２２＝２．６，γ３３＝０．２３，γ３１＝０．２５，γ５１＝－３．５×１０－１２ｍ／Ｖ。结果表明如果在Ｙ方向加电场，Ｚ方向通光，β—ＢＢＯ晶体可能制作成有应用价值的光开关。     

Sixty years of dislocations

It is well-known that with the appearance of three independent papers by Taylor, Polanyi and Orowan in the year 1934, the concept of crystal dislocations was born. Since then, dislocation theory has had many spectacular successes. It is quite appropriate therefore to be aware of the state of development of this exciting subject, sixty years after its discovery. A flavour for the vast subject of the applications of dislocation mechanisms to real materials is presented by choosing three examples, one each, drawn from metallurgy, physics and electronics. The topic of ‘Strength of metals and alloys’ is the first one, as this is also the author’s area of research. The phenomenon of solidification and crystal growth forms the next topic, especially in view of the seminal contributions made by A R Verma and his school from India. Dislocations play a useful role in the strengthening of solids, but how influential are they in affecting the performance of modern semiconductor devices? In the third example, the interesting and painstaking work done to settle this question is reviewed. Can we regard carbon fibre as thetransistor of dislocation theory? How shall we understand the long-established effects such as corrosion-fatigue, superplasticity and shape memory as well as the electrochemical and electro-mechanical properties of dislocations in semiconductor and non-metallic crystals? Answers to these questions belong to the realms of the future developments in dislocations. The talk is concluded with a discussion of these topics.     

Crystallization and Drying in Thin Sucrose Films During Panning

Sucrose crystallization in thin films (50–55 μm) was studied, using a videomicroscopy technique, at conditions encountered during hard panning processes. No nucleation occurred in unseeded films, while a linear increase in seeded crystals occurred during drying. Crystal growth rate increased with temperature (25–30°C) and with air velocity (2.4–12.5 m/sec), but did not change with varying sucrose concentrations (70–76% w/w) and relative humidities (0–66% at 30°C). FD & C Yellow No. 5 food coloring in the dye form (0.05–0.5 g/100 mL) showed no effects while similar concentrations in the lake form inhibited crystal growth rate.