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61.
分子动力学模拟测得熔融(RbCl)108离子簇在300K至600K温度时凝固的成核速率大于10^35m^-3s^-1,用均相成核的经典理论加以分析,估算得氯化铷离子簇的固液界面自由能σalT^1.4,用Grunasy提出的扩散界面理论加以分析,估算得扩展界面厚度约为0.195nm,σalT^0.97,2个理论在实验温度范围内没有明显判别,且均能较好地分子动力学模型的结果,但预测的较高温度下的成核速率有比较显著区别,因此进一步地研究将有助于鉴别它们。 相似文献
62.
This work is the first part of an overall project the aim of which is the development of general mix design rules for concrete containing different kinds of mineral admixtures. The separation of the different physical effects responsible for the modification of cement hydration, when chemically inert quartz powders are used in mortars, is presented. The phenomenological approach, based on semi-adiabatic calorimetry, is only associated with first-order phenomena, and the study excludes the complex physicochemical details involved in the chemistry of cement. The results, obtained for a wide range of fineness (between 180 and 2000 m2/kg) and replacement rates (up to 75%), show that short-term degrees of hydration in mortars containing a chemically inert mineral admixture (quartz) are always higher than for a reference mortar. This study confirms that cement hydration is enhanced by inert mineral admixtures. The two main physical effects responsible for the modification of the hydration of cement are identified as the dilution effect and heterogeneous nucleation. The dilution effect of the cement is highlighted with a coarse mineral admixture. The heterogeneous nucleation effect, although it increases with fineness of mineral admixtures, presents an optimum depending on the replacement rate. In the following part of this work, these results will be used for the development of an empirical model allowing us to quantify both physical effects. 相似文献
63.
M.E. Biancolini C. Brutti G. Paparo A. Zanini 《International Journal of Fatigue》2006,28(12):1820-1825
In this paper, a new acoustic emission (AE) diagnostic technique, for the study of fatigue cracks nucleation and propagation on steel, was investigated. Using the fractal analysis, and the box-counting method (BCM) in particular, it is possible to characterize the spatial distribution of the prime AE sources through the fractal dimension (D) that evolve with the number of fatigue cycles (N) of the specimen. D–N curves were found useful to identify the condition of incipient collapse due to the nucleation and propagation of fatigue cracks on steel. It is possible to use the fractal dimension as a damage parameter. In all tested specimens, the crisis occurs within the same range of values of fractal dimension. The results suggest that it is possible to anticipate the detection of crack beginning relating to the other theoretical or experimental techniques. 相似文献
64.
Fretting is associated with small amplitude oscillatory movements between two surfaces in contact. One possible consequence of fretting is the formation and subsequent growth of cracks at the edges of the contact. This paper presents an experimental investigation of the cracking behaviour under fretting loading of two different aluminium alloys: 2024-T351 and 7075-T651. Systematic and controlled experiments with a cylinder-flat contact under partial slip fretting conditions were carried out. A model which combines both crack nucleation and propagation processes is used to predict the crack extension throughout the life of the component. The direction of crack propagation experimentally observed was taken into account by the model. Furthermore, an analytical prediction of crack nucleation based on the process volume approach is made. The predictions of both crack extension and nucleation are compared with the experimental results, and show good agreement. 相似文献
65.
66.
Coating of SiC Powder with Nano YAG Phase 总被引:5,自引:0,他引:5
SiCceramiccompositeshavefoundextensiveap plicationsinmodernindustryduetotheirexcellentchemicalstabilityandwear resistance .Rodeghieroetal.[1~ 3 ] investigatedthefabricationofSiC Al2 O3 ce ramiccompositematerialsviaco precipitationcoatingandsol gelmethods… 相似文献
67.
The use of thermodynamic, statistical, and light and electron‐optical microscopic methods has made it possible to analyse the course of reactions during steel‐plant‐internal hot metal desulphurisation. The theoretical dependence between oxygen and sulphur activity has been used to develop an EMF‐measurement‐based technique for determining the sulphur content as the hot metal is desulphurised. The absence of magnesium sulphide from the collection of phases in the final slag because of the greater stability and secondary formation of calcium sulphide has been explained with the aid of thermo‐chemical calculations. 相似文献
68.
A sort of special dislocation configuration was deformation-induced in an Fe-Ni-V-C alloy by in-situ elongation tests of TEM. The cooling in-situ observations, as well as the SADPs from the region of the special dislocation configurations, proved that they are martensitic nuclei. In martensitic transformation, a nucleus changed into a small martensitic sub-plate, and a group of parallel sub-plates that formed from a group of parallel nuclei made up a big martensitic plate Martensitic transformation involved opposite shear between adjacent martensitic nuclei. By using the reduced-cell method, the crystallographic structure of observed martensitic nuclei was indexed as a face-centered orthogonal (FCO) lattice, which was explained by the nucleation mechanism proposed by the present authors. The crystallographic analysis confirmed that the defect faulting involved in martensitic nucleation took place among three close pakked planes, instead of between two adjacent planes as an ordinary stacking fault. 相似文献
69.
The propagation of short cracks in the neighbourhood of grain boundaries have been investigated using a technique were the crack is modelled by distributed dislocation dipoles and the plastic deformation is represented by discrete dislocations. Discrete dislocations are emitted from the crack tip as the crack grows. Dislocations can also nucleate at the grain boundaries. The influence on crack growth characteristics of the distance between the initial crack tip and the grain boundary has been studied. It was found that crack growth rate is strongly correlated to the dislocation pile-ups at the grain boundaries. 相似文献
70.
During the solidification of the AZ91D-alloys, the Al8(Mn, Fe)5 phase is generally precipitated in the melt in advance of the precipitation of the primary α-Mg. The basic principle for manufacturing AZ91D-alloy slurries for semi solid forming is to use the Al8(Mn, Fe)5 precipitates as the heterogeneous nucleation sites for primary α-Mg phases. Microscopic analysis for the location of the Al8(Mn, Fe)5 precipitate explains that the Al8(Mn, Fe)5 precipitate is the effective heterogeneous nucleation site for the primary α-Mg phase. It was also observed that increase of the Mn content in the melt and the cooling rate below to the solid/liquid two-phase region resulted in smaller and more globular primary α-Mg due to the increase of heterogeneous nucleation sites. It was found that the average α-Mg diameter grew as a function of t0.278, where t is the holding time at the solid/liquid two-phase region. This would be attributed to the Ostwald type ripening and coalescence between primary α-Mg phases. The cooling rate below to the solid/liquid two-phase region, Mn content in AZ91D alloy, and the holding time and temperature affected on the quality of slurry. 相似文献