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101.
The results of conversion determinations on the products from Powhatan No.5 coal liquefied in an autoclave and in a high-pressure, high-temperature e.s.r. cavity are reported. Oil, asphaltene and preasphaltene yields, and overall conversion have been determined for Powhatan No.5 coal samples liquefied in tetralin, SRC-11 heavy distillate, and naphthalene at temperatures from 400 to 480 ° C in both reactor systems. The concept of reaction severity is introduced and used to formalize the relation between the effect of temperature and reaction time on oil yield and conversion. Oil is the predominant product in liquefaction in tetralin or naphthalene, asphaltene is the major product of liquefaction in SRC-II heavy distillate. Retrogressive reaction (THF-insoluble product formation) becomes severe when SRC-II heavy distillate is the liquefaction solvent and residence time of >10 min are used at temperatures >450 °C. Preasphaltenes appear to be the only intermediate species in Powhatan No.5 liquefaction. 相似文献
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Rajib Bandyopadhyay Mahuya Bandyopadhyay Yoshihiro Kubota Yoshihiro Sugi 《Journal of Porous Materials》2002,9(2):83-95
AlPO4-5 and AlPO4-11 were synthesized by dry-gel conversion (DGC) method. Steam-assisted conversion (SAC) and vapor-phase transport (VPT) techniques were applied for this purpose. The synthesis was successful in presence of a certain minimum amount of external bulk water, without which the crystallization failed. Crystallization by VPT method was slower than corresponding SAC and HTS method. SAPO analogs of the samples, SAPO-5 and SAPO-11 were also synthesized by DGC method. Samples made by DGC methods had higher yield than the conventional hydrothermal synthesis (HTS); otherwise the samples showed similar characteristics as that made by HTS. XRD, SEM and N2-adsorption results showed high crystallinity and purity of the samples made by DGC, and 27Al MAS NMR spectra indicated the tetrahedral framework nature of Al. SAPO-5 and SAPO-11 were tested for their catalytic activity in isopropylation of biphenyl, and in terms of conversion and selectivity, SAPO-5 was found to be suitable for this application. 相似文献
104.
Polypropylene/poly(methyl acrylate)‐grafted glass wool (PMA‐g‐GW) mixes were prepared. The polymerization process was carried out using potassium persulfate (PPS) and PPS/acetone sodium bisulfite (ASBS) as a redox‐pair initiation system at 60 and 70°C. The effect of using PPS or PPS/ASBS on the grafting percent and conversion percent reveals that the conversion percent values on using PPS as an initiator are higher than those of PPS/ASBS, while in the case of grafting, the inverse is true, that is, using PPS as an initiator gives grafting percent values lower than those that can be obtained using PPS/ASBS. The dielectric properties, thermal diffusivity, specific heat capacity, and thermal conductivity of PP loaded with modified glass wool as a function of different types and concentrations of initiators—used in the grafting polymerization process, namely, PPS and the redox initiating system—were also studied. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 87: 723–732, 2003 相似文献
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随着遥感应用技术的不断发展,对ESRI Shapefile格式图像文件的处理需求变得日益紧迫。目前能对它进行处理的软件有很多,但是这些软件运行时占用大量系统资源,而直接将商业软件嵌入到自主开发的软件中也是不可取的。因此,能够在自主开发的遥感图像处理软件中实现对ESRI Shapefile格式文件的操作已经变得非常重要。通过对ESRI Shapefile格式的影像数据结构特征分析,提出基于GDAL实现ESRI Shapefile格式文件到png文件格式的转换和处理方法,包括地理信息获取、坐标系统转换和文件格式转换。通过试验验证了该方法的可行性。 相似文献
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新型开关磁阻发电机具有发电容量大、效率高、起动和发电组合容易等优点,三电平逆变器具有能减少开关损耗和滤波电感损耗并有降低开关应力等特点。利用三电平逆变器转换效率高的优势,结合新型开关磁阻发电机低风速发电特点,降低开关损耗和开关器件电压应力,提高装置可靠性。仿真实验结果表明:用三电平逆变器能够很好的实现开关磁阻发电机的逆变要求。 相似文献
110.
王慧 《自动化技术与应用》2014,33(9):103-105
设计了直流电机运行电流的硬件采集电路,解决了高速下电枢绕组电流的采集问题。利用霍尔电流传感器ACS712通过AD转换将采集到的绕组电流数据,通过串口和上位机进行通信,实现了本机LCD液晶显示和基于LabVIEW的软件界面显示电流数据,具有实际的工程意义。 相似文献